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Behaviour of Polymer Filled Composites for Novel Polymer Railway Sleepers - MDPI
polymers
Article
Behaviour of Polymer Filled Composites for Novel Polymer
Railway Sleepers
Wahid Ferdous 1, * , Allan Manalo 1 , Choman Salih 1 , Peng Yu 1 , Rajab Abousnina 2 , Tom Heyer 3
and Peter Schubel 1

                                           1   Centre for Future Materials (CFM), University of Southern Queensland, Toowoomba, QLD 4350, Australia;
                                               Allan.Manalo@usq.edu.au (A.M.); Choman.Salih@usq.edu.au (C.S.); Peng.Yu@usq.edu.au (P.Y.);
                                               Peter.Schubel@usq.edu.au (P.S.)
                                           2   School of Engineering, Macquarie University, Macquarie Park, NSW 2113, Australia;
                                               rajab.abousnina@mq.edu.au
                                           3   Austrak Pty. Ltd., Brisbane, QLD 4001, Australia; Tom.Heyer@vossloh.com
                                           *   Correspondence: Wahid.Ferdous@usq.edu.au; Tel.: +61-7-4631-1331

                                           Abstract: A novel concept of polymer railway sleeper is proposed in this study that has the potential
                                           to meet static performance requirements within the cost of hardwood timber. The existing challenges
                                           of composite sleepers, such as low performance or high cost, can be overcome using this innovative
                                           concept. Such a proclamation is proven through limit state design criteria and a series of experimen-
                                           tations. Results show that polyurethane foam as an infill material can provide sufficient strength and
                                           stiffness properties to the sleeper, but the inadequate screw holding capacity could be a problem.
                                           This limitation, however, can be overcome using a particulate filled resin system. The findings of this
                                           study will help the railway industry to develop a timber replacement sleeper.
         
         
                                           Keywords: composite sleeper; timber replacement sleeper; GFRP; structural performance; sustain-
Citation: Ferdous, W.; Manalo, A.;
                                           able development
Salih, C.; Yu, P.; Abousnina, R.; Heyer,
T.; Schubel, P. Behaviour of Polymer
Filled Composites for Novel Polymer
Railway Sleepers. Polymers 2021, 13,
1324. https://doi.org/10.3390/             1. Introduction
polym13081324                                   The global railway industry is looking for an alternative material railway sleeper
                                           that can replace traditional timber sleeper which is suffering from premature deteriora-
Academic Editor: Vincenzo Fiore            tion [1,2]. To take this as an opportunity, a number of research institutions and railway
                                           sleeper manufacturing companies in different parts of the world are developing innovative
Received: 28 February 2021                 polymer-based technologies. These alternative sleepers are mainly developed from recy-
Accepted: 15 April 2021
                                           cled plastics and fibre reinforced synthetic foam materials. Recycled plastic sleepers are
Published: 18 April 2021
                                           made of waste tyres, plastic bottles and other similar materials which is highly beneficial
                                           from the environmental viewpoint [3]. Moreover, this type of sleeper can be manufactured
Publisher’s Note: MDPI stays neutral
                                           within the cost of hardwood timber due to the use of high volume of waste materials. How-
with regard to jurisdictional claims in
                                           ever, they are suffering from low pull-out resistance, low stiffness, high thermal expansion
published maps and institutional affil-
                                           causing plastic deformation and subsequently loosening of fasteners, low fire resistance
iations.
                                           and poor dimensional stability at service temperatures [4]. On the other hand, the Fibre-
                                           reinforced Foamed Urethane (FFU) sleeper has very similar mechanical properties but
                                           superior durability than traditional timber sleepers [5–7]. However, their high cost (around
                                           5–10 times more expensive than standard timber sleepers [8]), limited shear strength due to
Copyright: © 2021 by the authors.
                                           the absence of transverse fibres and increasing concern for occupational health, safety, and
Licensee MDPI, Basel, Switzerland.
                                           environment (OHSE) [7] due to the generation of polyurethane dust during screw drilling
This article is an open access article
                                           are restricting their applications. Therefore, an alternative polymer-based material that
distributed under the terms and
                                           meets both cost and performance criteria for sleeper is inevitable.
conditions of the Creative Commons
                                                Ferdous et al. [9] investigated high performance polymer sleeper manufactured from
Attribution (CC BY) license (https://
                                           fibre composite sandwich panels and bonded with epoxy polymer matrix. The dog bone
creativecommons.org/licenses/by/
4.0/).
                                           shape of this sleeper was designed based on shape optimisation that reduced the volume

Polymers 2021, 13, 1324. https://doi.org/10.3390/polym13081324                                            https://www.mdpi.com/journal/polymers
Behaviour of Polymer Filled Composites for Novel Polymer Railway Sleepers - MDPI
Polymers 2021, 13, 1324                                                                                                      2 of 13

                               of materials by up to 50% with respect to the rectangular shaped sleeper and was able to
                               be manufactured within target price range. A similar approach for shape optimisation
                               was considered for KLP (Kunststof Lankhorst Product) plastic sleepers which reduced the
                               volume of plastics by 35% compared with rectangular shaped solid sleeper [10]. However,
                               the railway industry prefers to replace timber sleeper by an alternative sleeper that looks
                               alike timber sleepers, i.e., the rectangular shaped sleeper is the preferred choice [11]. The
                               reason could be the rectangular shaped sleeper is easier to push into the ballast bed during
                               spot replacement (i.e., track maintenance work). Therefore, the key scientific research
                               challenge is how to develop an alternative material sleeper that will be rectangular in
                               shape and perform satisfactorily within the target price range. To achieve this goal, the
                               authors recently proposed three new concepts of internally reinforced rectangular shaped
                               composite sleepers [4]. However, the manufacturing process of internally reinforced
                               sleepers is complex and time consuming. Therefore, this study proposed a design concept
                               for an externally reinforced polymer railway sleeper to address the scientific challenge.
                               Moreover, a higher strength and stiffness can be achieved if the reinforcement is applied
                               externally. The outcome of this study will guide sleeper manufacturers to design a polymer
                               railway sleeper that is cheaper and faster in construction.

                               2. Development of the Sleeper Concept and Performance Evaluation
                               2.1. Selection of Suitable Polymer
                                    The commonly used polymeric resins for structural applications are epoxy, polyester,
                               vinyl ester, phenolic, polyurethane foam and some others. Several classes of synthetic resins
                               manufactured by the esterification of organic compounds are available. The advantage and
                               disadvantage of different resins are summarised in Table 1 to justify the selection of the most
                               suitable one for manufacturing railway sleepers. One of the major considerations is the cost
                               of resin which limits the choice among polyester, phenolic and polyurethane foam. The
                               quick and ease of application of resin for large scale sleeper manufacturing is an essential
                               requirement. Since the resin will be used as an infill material, moisture and UV are not of
                               major concern. Considering this fact, polyurethane foam was selected for this study.

                                Table 1. Advantage and Disadvantage of Different Resins [12].

         Types of Resin                          Advantage                                        Disadvantage

                           •     High mechanical and thermal properties
                           •     High water resistance                           •   More expensive than vinyl esters
             Epoxy         •     Long working times available                    •   Mixing is critical
                           •     High temperature resistance
                           •     Low cure shrinkage

                                                                                 •   Limited mechanical properties
                           •     Easy to use                                     •   High styrene emissions in open moulds
            Polyester      •     Low cost                                        •   Limited range of working times
                                                                                 •   High cure shrinkage

                                                                                 •   Postcure required for high properties
                           •     Very high chemical resistance                   •   High styrene content
           Vinyl ester     •     Higher mechanical properties than polyesters    •   Expensive than polyesters
                                                                                 •   High cure shrinkage

                           •     Good mechanical properties
                           •     Heat and impact resistant                       •   Very low toughness
            Phenolic       •     High chemical and moisture resistance           •   Brittle nature
                           •     Low cost                                        •   Humidity badly affects its resistance
                           •     Low smoke emission

                           •     Low cost
                           •     High thermal insulation properties              •   Spray foam insulation method might be
       Polyurethane foam   •     Quick and easy application                          expensive
                           •     Highly adhesive and extremely lightweight
                           •     Does not create dust or release harmful gases
Behaviour of Polymer Filled Composites for Novel Polymer Railway Sleepers - MDPI
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                            Highly adhesive and extremely lightweight
Polymers 2021, 13, 1324     Does not create dust or release harmful gases                                                                          3 of 13

                                   2.2. Design of PU Foam Core FRP Sleeper (Concept-1)
                                         This concept
                                   2.2. Design          of sleeper
                                                of PU Foam              is based
                                                                 Core FRP            on (Concept-1)
                                                                               Sleeper  a glass fiber reinforced polymer (GFRP) rectangu-
                                   lar hollow   pultruded      section     filled
                                         This concept of sleeper is based on a glasswith   polyurethane        (PU) foam
                                                                                                  fiber reinforced     polymer as shown
                                                                                                                                   (GFRP)in      Figure 1.
                                                                                                                                              rectangular
                                   Inspired  by  the  sleeper    concept      developed      on   the  geopolymer        concrete
                                   hollow pultruded section filled with polyurethane (PU) foam as shown in Figure 1. Inspired        filled  GFRP    tubes
                                   [13],
                                   by the sleeper concept developed on the geopolymer concrete filled GFRP tubes [13],geo-
                                         the proposed     concept      is  advantageous         from   screw    drilling   perspectives.      While     the
                                   polymer
                                   proposedconcrete
                                               concept is is non-drillable,
                                                              advantageousthe       fromPUscrew
                                                                                             foamdrilling
                                                                                                     core allows       on-site drilling
                                                                                                                perspectives.                which is an
                                                                                                                                   While geopolymer
                                   important
                                   concrete iscriterion    for spot
                                                non-drillable,       thereplacement
                                                                           PU foam core    of allows
                                                                                               deteriorated
                                                                                                         on-sitesleepers.
                                                                                                                   drilling Moreover,
                                                                                                                               which is anthe     exterior
                                                                                                                                               important
                                   polymer
                                   criterion coated
                                              for spot GFRP      offers better
                                                         replacement               thermal andsleepers.
                                                                              of deteriorated        fire resistance
                                                                                                                 Moreover,compare      to recycled
                                                                                                                                 the exterior         plas-
                                                                                                                                                 polymer
                                   tics which   was  identified      a  weakness       for  recycled    plastic    sleepers.
                                   coated GFRP offers better thermal and fire resistance compare to recycled plastics which     The   cost  of  the GFRP
                                   profile is dependent
                                   was identified    a weaknesson thefor  wall    thickness.
                                                                              recycled    plasticTosleepers.
                                                                                                     determine    The thecost
                                                                                                                           minimum
                                                                                                                               of the GFRPrequired    wall
                                                                                                                                                 profile  is
                                   thickness,
                                   dependentthe  onsectional
                                                     the wallanalysis
                                                                   thickness.  is conducted
                                                                                   To determine  (Figure
                                                                                                       the 1).  It is worth
                                                                                                             minimum           noting wall
                                                                                                                            required     that the  contri-
                                                                                                                                                thickness,
                                   bution  of PU core
                                   the sectional         is ignored
                                                   analysis               in the analysis
                                                                is conducted        (Figure 1). dueItto
                                                                                                      is its low noting
                                                                                                         worth      strength.thatThe
                                                                                                                                   thestrain   and stress
                                                                                                                                         contribution    of
                                   profiles
                                   PU core are    plotted in
                                             is ignored      inthe
                                                                 Figure     1 where
                                                                      analysis     due totheitssymbols     have their
                                                                                                 low strength.       The usual
                                                                                                                           strain meanings.       Table 2
                                                                                                                                    and stress profiles
                                   listed the properties
                                   are plotted   in Figure of     GFRP the
                                                               1 where       laminates
                                                                                  symbols  fabricated
                                                                                              have their  with
                                                                                                             usualtenmeanings.
                                                                                                                        layers of fibres
                                                                                                                                      Table oriented
                                                                                                                                             2 listed thein
                                   longitudinal
                                   properties of(60%)
                                                   GFRPand        45-degree
                                                            laminates             diagonal
                                                                            fabricated    with (40%)   directions
                                                                                                  ten layers           withoriented
                                                                                                                of fibres     a fibre volume      fraction
                                                                                                                                         in longitudinal
                                   (60%)
                                   of 55%.and 45-degree diagonal (40%) directions with a fibre volume fraction of 55%.

     Figure 1. Sectional
               Sectional analysis
                          analysisofofsleeper
                                        sleeperConcept-1
                                                Concept-1   (ignoring
                                                         (ignoring  thethe contribution
                                                                        contribution     of low
                                                                                     of low      strength
                                                                                             strength infillinfill material
                                                                                                             material thus athus a linear
                                                                                                                             linear strain
     strain and distribution
     and stress stress distribution  for exterior
                              for exterior        Fiber Reinforced
                                            Fiber Reinforced  PolymerPolymer
                                                                        (FRP)).(FRP)).

                                   Table 2. Nominal
                                   Table 2. Nominal Properties of GFRP
                                                    Properties of GFRP Laminates.
                                                                       Laminates.

                                                          Properties                                          Value                     Unit
                                              Properties                                   Value                                    Unit
                                                    Tensile failure strain                                    0.035                      -
                                         Tensile failure  strain
                                                    Tensile  failure stress                 0.035              425                   - MPa
                                         Tensile failure  stressmodulus
                                                      Tensile                                425               16.5                 MPa GPa
                                           Tensile modulus                                  16.5                                    GPa
                                                Compressive failure strain                                    0.025                      -
                                       Compressive failure strain                           0.025                                    -
                                                Compressive
                                       Compressive               failure stress
                                                     failure stress                          280               280                  MPa MPa
                                                  Compressive
                                        Compressive    modulus modulus                       11.5              11.5                 GPa GPa
                                        The increase of sectional modulus and moment capacity with the increase of tube
                                   thickness  from 1 mm
                                        The increase         to 10 mm
                                                        of sectional      are summarised
                                                                      modulus     and moment in Table   3. The
                                                                                                  capacity    withmoment    capacity
                                                                                                                     the increase     and
                                                                                                                                  of tube
                                   modulus
                                   thicknessoffrom
                                                 elasticity
                                                     1 mm(MOE)      of the
                                                             to 10 mm       composite
                                                                          are          sleepers
                                                                               summarised         can be
                                                                                             in Table   3. as lowmoment
                                                                                                            The     as 25 kN-m  [4] and
                                                                                                                            capacity    4
                                                                                                                                      and
                                   GPa  [14], of
                                   modulus    respectively.   Basedof
                                                 elasticity (MOE)    onthe
                                                                         thecomposite
                                                                              compressive   failure
                                                                                        sleepers  canatbe
                                                                                                        theastop
                                                                                                              lowside   ofkN-m
                                                                                                                    as 25  GFRP,[4]
                                                                                                                                  Table
                                                                                                                                    and 34
                                   suggested   that a thin layer
                                   GPa [14], respectively.        of GFRP
                                                              Based  on thetube    (even 1 mm)
                                                                               compressive        canatmeet
                                                                                             failure           the side
                                                                                                         the top    requirements  of mo-3
                                                                                                                         of GFRP, Table
                                   ment  capacity,
                                   suggested   that however,   a minimum
                                                    a thin layer of GFRP tube thickness
                                                                                 (even 1of 4 mm
                                                                                         mm)   canismeet
                                                                                                     required    to meet the target
                                                                                                           the requirements         MOE
                                                                                                                              of moment
                                   capacity,
                                   of 4 GPa. however, a minimum thickness of 4 mm is required to meet the target MOE of
                                   4 GPa.
Behaviour of Polymer Filled Composites for Novel Polymer Railway Sleepers - MDPI
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                                  Table 3. Increase of Sleeper Capacity with Tube Thickness.

                                      Table
                                    Tube    3. Increase ofNeutral
                                         Thickness         Sleeper Axis
                                                                   Capacity with Tube Thickness.
                                                                        Depth          I                        Moment                  MOE
        Tube Thickness         Neutral Axis
                                         mm  Depth                   mmI                     mm4Moment            kN-m          MOE      GPa
             mm                       mm 1                           mm4
                                                                    61.09                        kN-m
                                                                                           29490994                 89          GPa      2.01
               1                      61.092                       29490994
                                                                    61.08                  2948909889              175          2.01     2.73
               2                      61.083                       29489098
                                                                    61.06                         175
                                                                                           29485321                258          2.73     3.41
               3                      61.064                       29485321
                                                                    61.04                         258
                                                                                           29481565                339          3.41     4.07
               4                      61.045                       29481565
                                                                    61.02                         339
                                                                                           29477830                416          4.07     4.70
               5                      61.026                        61.00
                                                                   29477830                29474117
                                                                                                  416              491          4.70     5.30
               6                      61.007                        60.98
                                                                   29474117                29470424
                                                                                                  491              563          5.30     5.86
               7                      60.988                        60.96
                                                                   29470424                29466753
                                                                                                  563              633          5.86     6.40
               8                      60.969                        60.93
                                                                   29466753                29461286
                                                                                                  633              699          6.40     6.92
               9                      60.9310                       60.91
                                                                   29461286                29457667
                                                                                                  699              763          6.92     7.41
              10                         60.91                     29457667                       763                           7.41
                                  2.3. Materials and Manufacturing of Sleeper Concept-1
                                   2.3. Materials
                                  2.3.1.  PU Foam     and Manufacturing
                                                        and   GFRP Laminates of Sleeper Concept-1
                                   2.3.1.APU    Foam
                                             solid      and GFRPmade
                                                     component        Laminates
                                                                              with polyurethane (PU) based resin was used as a core
                                  material    of sleeper
                                         A solid            (Figure
                                                     component        2a). with
                                                                   made     The typical    compressive
                                                                                 polyurethane               strength
                                                                                                    (PU) based    resinand
                                                                                                                         wascompressive
                                                                                                                              used as a core modulus
                                                                                                                                                ma-
                                   terial
                                  of PU of    sleeper
                                           foam     are 1(Figure
                                                          MPa and  2a).16
                                                                        The   typical
                                                                            MPa,       compressive
                                                                                   respectively          strength
                                                                                                     [15]. Two typesand compressive
                                                                                                                         of GFRP fabrics  modulus
                                                                                                                                              such as
                                   of PU foam
                                  uniaxial          are 1 MPa
                                              (0 direction    andand60016gsm)
                                                                            MPa,and
                                                                                  respectively     [15]. Two
                                                                                      triaxial (0/+45/      −45types   of GFRP
                                                                                                                 directional      fabrics
                                                                                                                               fibres  andsuch    as
                                                                                                                                             823 gsm)
                                   uniaxial
                                  were    used (0 to
                                                  direction
                                                      fabricateandouter
                                                                    600 gsm)
                                                                           layerand   triaxial
                                                                                  of the   core.(0/+45/−45
                                                                                                   Two layers directional   fibres
                                                                                                                   (first and  lastand    823 gsm)
                                                                                                                                     layers)   of non-
                                   were usedchopped
                                  structural       to fabricate   outermat
                                                              strand      layer  of the
                                                                              (CSM)       core. Two
                                                                                       fibreglass       layers
                                                                                                      were      (first
                                                                                                             used      and last
                                                                                                                    together      layers)
                                                                                                                               with    GFRPof non-
                                                                                                                                               fabrics.
                                   structural    chopped      strand   mat   (CSM)   fibreglass     were   used   together
                                  The very first layer of CSM was provided to ensure sufficient resin to the main GFRP layer with  GFRP     fabrics.
                                   The better
                                  and   very first    layer ofThe
                                                 bonding.       CSM    waslayer
                                                                     final   provided
                                                                                   of CSMto ensure    sufficient to
                                                                                              was provided        resin to the
                                                                                                                     avoid  themain
                                                                                                                                 dropGFRP     layer
                                                                                                                                         of resin  due
                                   and   better   bonding.     The  final  layer  of CSM    was    provided    to  avoid
                                  to gravity and also for cosmetic elegance to the sleeper. The fibre stacking sequence   the  drop   of resin  duewas
                                   to gravity and also for cosmetic elegance
                                  CSM/U/T/U/U/U/T/U/CSM,                       where Utoand  the Tsleeper.   The unidirectional
                                                                                                    represents    fibre stacking sequence
                                                                                                                                    and triaxialwasfab-
                                   CSM/U/T/U/U/U/T/U/CSM,
                                  rics, respectively. The lamination    where    U andwas
                                                                               process    T represents
                                                                                               done at the unidirectional    and triaxial
                                                                                                              Buchanan Advanced             fabrics,
                                                                                                                                         Composites
                                   respectively.
                                  (BAC)               The lamination process was done at the Buchanan Advanced Composites
                                            in Toowoomba.
                                   (BAC) in Toowoomba.

                                                             (a)                                                    (b)
                                   Figure2.
                                  Figure 2. Manufacturing
                                            Manufacturing process.
                                                          process. (a)
                                                                    (a)Prefabricated
                                                                       PrefabricatedPU
                                                                                     PUfoam
                                                                                        foamcore.
                                                                                             core.(b)
                                                                                                    (b)Applying
                                                                                                        ApplyingGFRP
                                                                                                                 GFRPfabrics onon PU
                                                                                                                       fabrics
                                   PU core.
                                  core.

                                   2.3.2. Manufacturing
                                  2.3.2.  Manufacturing Method
                                                           Method
                                         The
                                        The PUPU core  was  prepared
                                                            prepared ininaaclosed
                                                                             closedmould
                                                                                    mouldbefore
                                                                                            beforeapplying
                                                                                                    applying     laminates.
                                                                                                                   laminates.  The PUPU
                                                                                                                                 The    core
                                                                                                                                           core
                                   waswrapped
                                  was    wrapped with
                                                    with GFRP laminates
                                                                 laminates using
                                                                              usinghand
                                                                                     handlamination
                                                                                           laminationprocess.
                                                                                                           process.The   Thewrapping
                                                                                                                               wrapping waswas
                                   done by
                                  done    by two
                                              two steps
                                                  steps to avoid
                                                            avoid sagging
                                                                    saggingdueduetotogravity
                                                                                      gravity(a)
                                                                                               (a)applied
                                                                                                   appliedonon    two
                                                                                                                    two sides  and
                                                                                                                           sides    thethe
                                                                                                                                  and    toptop
                                   surface and
                                  surface   and (b) flipped over
                                                              over and
                                                                    andrepeat
                                                                         repeatthethesame
                                                                                      sameprocess
                                                                                            process(i.e.,
                                                                                                       (i.e.,applied
                                                                                                              applied  twotwosides and
                                                                                                                                sides andthethe
                                   othersurface).
                                  other   surface). The
                                                    The fibres
                                                        fibres were
                                                                were overlapped
                                                                      overlappedatattwotwosides
                                                                                            sidesofofthe
                                                                                                       thesleeper
                                                                                                             sleeper forfor
                                                                                                                          full depth.
                                                                                                                            full depth.
                                        AA particulate
                                           particulate filled
                                                        filledresin
                                                                resinmix
                                                                       mixwaswasprepared  using
                                                                                   prepared      polyester
                                                                                             using    polyester resinresin
                                                                                                                      (Polyplex    1472 In-
                                                                                                                              (Polyplex   1472
                                   fusion  Resin  25, density  1.10 g/cm 3), NOROX
                                                                              3        CHM-50    hardener      (density
                                  Infusion Resin 25, density 1.10 g/cm ), NOROX CHM-50 hardener (density 1.06 g/cm )       1.06 g/cm 3) and 3

                                  and fly ash with a mixing ratio of Resin: Hardener: Fly ash = 2000:40:200 g. The resin and
Behaviour of Polymer Filled Composites for Novel Polymer Railway Sleepers - MDPI
Polymers 2021, 13, 1324                                                                                                                      5 of 13

                          Polymers 2021, 13, x FOR PEER REVIEW                                                                                           5 of 1

                                    hardener were mixed before the fly ash added to the mix. The gel time (working time) of
                                    the resin mix wasflyaround   1 h.
                                                           ash with   The samples
                                                                    a mixing           were post
                                                                              ratio of Resin:      curedFly
                                                                                              Hardener:       80 =◦ C
                                                                                                           atash       for 3 h. The
                                                                                                                    2000:40:200        overall
                                                                                                                                  g. The resin and hard
                                    casting process areener  werein
                                                         shown    mixed  before
                                                                     Figure       the fly ashthe
                                                                             2. Although      added
                                                                                                 GFRPto the mix. Thewere
                                                                                                         laminates      gel time  (working
                                                                                                                              applied   usingtime) of the
                                                       resin mixfor
                                    hand lamination process      wasthe
                                                                      around   1 h. The
                                                                         research       samples were
                                                                                      purpose,         post curedwas
                                                                                                 the approach       at 80 used
                                                                                                                          °C for to
                                                                                                                                 3 h.simulate
                                                                                                                                      The overall casting
                                    pultruded hollow process    are shown
                                                        rectangular         in Figure
                                                                      profiles          2. Although
                                                                                for large           the GFRP laminates were applied using hand
                                                                                           scale manufacturing.
                                                           lamination process for the research purpose, the approach was used to simulate pultruded
                                                       hollow rectangular profiles
                                    2.4. Results and Discussion—Performance        for largeofscale
                                                                               Evaluation           manufacturing.
                                                                                                Sleeper Concept-1
                                    2.4.1. Density
                                                           2.4. Results and Discussion—Performance Evaluation of Sleeper Concept-1
                                         The dimensions of the PU foam core sleeper were 243 mm (W) × 120 mm (D) ×
                                                      2.4.1. Density
                                    2130 mm (L). The overall weight of the sleeper was 39 kg that provided an equivalent
                                                             The dimensions of the PU foam core sleeper were 243 mm (W) × 120 mm (D) × 2130
                                    density of 640 kg/m3 . This density is lower than the density of traditional softwood timber
                                                      mm     (L). The overall weight of the sleeper was 39 kg that provided an equivalent density
                                    sleepers (855 kg/m3 ) and able         to overcome the limitation of heavy weight for concrete
                                                      of 3640 kg/m3. This density is lower than the density of traditional softwood timber sleeper
                                    sleepers (2000 kg/m    ). Moreover,
                                                      (855 kg/m ) and able
                                                                     3       the density  is alsothe
                                                                                  to overcome      slightly lower
                                                                                                      limitation of than
                                                                                                                     heavythe  recycled
                                                                                                                             weight      plastic sleeper
                                                                                                                                     for concrete
                                    sleepers (850–1150(2000
                                                        kg/m     3 ) and close to FFU (fibre-reinforced foamed urethane) synthetic
                                                              kg/m ). Moreover, the density is also slightly lower than the recycled plastic sleeper
                                                                       3
                                                       3 ) [10]. The lower
                                    sleeper (740 kg/m(850–1150        kg/m3) anddensity
                                                                                  close toof
                                                                                           FFUthe(fibre-reinforced
                                                                                                   proposed concept      is due
                                                                                                                     foamed       to the synthetic
                                                                                                                              urethane)   use of sleepe
                                    lightweight foam (740
                                                       core.    The
                                                             kg/m        lowThe
                                                                    3) [10].  density
                                                                                lower is preferable
                                                                                      density           for ease concept
                                                                                                of the proposed   of handling
                                                                                                                           is due sleepers   but
                                                                                                                                  to the use of lightweigh
                                    might create trackfoam
                                                       stability
                                                              core.issue.
                                                                        The low density is preferable for ease of handling sleepers but might create
                                                           track stability issue.
                                    2.4.2. Bending Modulus of Elasticity (MOE)
                                                        2.4.2. Bending
                                          Bending modulus               Modulus
                                                                of elasticity      of Elasticity
                                                                               is an   important (MOE)
                                                                                                    property on which the deflection
                                    characteristics of sleeper are dependent. The MOE isanthe
                                                              Bending  modulus   of elasticity is   important
                                                                                                      functionproperty  on which
                                                                                                                of the initial     theof
                                                                                                                               slope    deflection
                                                                                                                                          the      char
                                                        acteristics of sleeper are  dependent.    The MOE  is the function
                                    load-displacement curve obtained from midspan bending test. Therefore, a non-destructiveof the  initial slope of the
                                                        load-displacement curve obtained from midspan bending test. Therefore, a non-destruc
                                    test (Figure 3a) up to 50 kN was carried out under three-point bending with a span of
                                                        tive test (Figure 3a) up to 50 kN was carried out under three-point bending with a span o
                                    1130 mm (same as narrow gauge length of sleeper).
                                                           1130 mm (same as narrow gauge length of sleeper).

                                    Figure 3. Non-destructive
                                       Figure 3. Non-destructivethree-point
                                                                  three-pointbending
                                                                              bending test (a) test
                                                                                      test (a) testsetup
                                                                                                    setupand
                                                                                                          and(b)
                                                                                                              (b)load-displacement
                                                                                                                  load-displacement  behaviour.
                                                                                                                                   behaviour.

                                         Figure 3b plotted Figure
                                                            the load-displacement         curve where itcurve
                                                                     3b plotted the load-displacement         can where
                                                                                                                    be seen    thatbe
                                                                                                                            it can  the  bending
                                                                                                                                      seen  that the bending
                                    behaviour is almost linear upistoalmost
                                                      behaviour         50 kN linear
                                                                                load. The
                                                                                       up toeffective   modulus
                                                                                              50 kN load.           of elasticity
                                                                                                              The effective        of theof
                                                                                                                               modulus     sleeper
                                                                                                                                              elasticity of the
                                    was found 5.15 GPa   as determined
                                                      sleeper   was foundby     Equation
                                                                             5.15           (1), where a,
                                                                                   GPa as determined            I and ∆P/∆δ
                                                                                                          byL,Equation           are shear
                                                                                                                          (1), where   a, L, Ispan,
                                                                                                                                               and ΔP/Δδ are
                                                      shear span,
                                    span, effective moment           span,ofeffective
                                                             of inertia                moment
                                                                              the sleeper,   andof   inertia
                                                                                                   slope      of the
                                                                                                          of the      sleeper, and slope curve,
                                                                                                                   load–displacement         of the load–dis
                                                      placement
                                    respectively. The MOE           curve, respectively.
                                                            for softwood                   The MOE
                                                                              timber sleeper     can beforas
                                                                                                           softwood
                                                                                                             low as 7.4timber
                                                                                                                           GPa.sleeper   can bethe
                                                                                                                                  Moreover,       as low as 7.4
                                                      GPa.  Moreover,    the  MOE    for recycled   plastic sleeper  varies
                                    MOE for recycled plastic sleeper varies between 1.5 GPa and 1.8 GPa while it is 8.1 GPa   between   1.5 GPa   and 1.8 GPa
                                                      while  it is 8.1 GPa  for  FFU  synthetic  sleeper  [10]. The  American
                                    for FFU synthetic sleeper [10]. The American Railway Engineering and Maintenance-of-          Railway   Engineering    and
                                                      Maintenance-of-Way Association (AREMA) specification indicated that the MOE for pol
                                    Way Association (AREMA) specification indicated that the MOE for polymer composite
                                                      ymer composite sleeper should be at least 1.17 GPa [16]. The incorporation of fibres in PU
                                    sleeper should be at least 1.17 GPa [16]. The incorporation of fibres in PU foam core sleeper
                                    provided higher modulus than recycled plastic materials. However, the stiffness is slightly
                                    lower than softwood timber and FFU due its lower density.

                                                                                  a  2              ∆P 
                                                                                                  2
                                                                     MOE =             3L − 4a                                                   (1)
                                                                                 48I                    ∆δ
Behaviour of Polymer Filled Composites for Novel Polymer Railway Sleepers - MDPI
Polymers 2021, 13, x FOR PEER REVIEW                                                                                           6 of 13

Polymers 2021, 13, 1324                                    foam core sleeper provided higher modulus than recycled plastic materials. However,
                                                                                                                                         6 of 13 the
                                                           stiffness is slightly lower than softwood timber and FFU due its lower density.
                                                                                                                               ∆
                                                                                                   =        (3   −4       )(     )                        (1)
                                                                                                       48                      ∆
                                    2.4.3. Compression Modulus of Elasticity
                                                     2.4.3. Compression
                                          The compression    modulus ofModulus      of Elasticity
                                                                           elasticity  of sleeper indicates the deformation charac-
                                    teristics when the sleeper   is being compressed.
                                                           The compression                 A non-destructive
                                                                             modulus of elasticity                rail-seat
                                                                                                    of sleeper indicates the compression
                                                                                                                             deformation charac-
                                                     teristics
                                    test was conducted         when the sleeper
                                                         to determine            is being compressed.
                                                                         these properties.              A non-destructive
                                                                                               The compression              rail-seat4a)
                                                                                                                   load (Figure       compression
                                                                                                                                         was
                                                     test which
                                    applied up to 72 kN   was conducted   to determine
                                                                  is the design         these
                                                                                 rail-seat     properties.
                                                                                            load           The compression
                                                                                                  for narrow-gauge           load (Figure
                                                                                                                       rail-track          4a) was
                                                                                                                                    [9]. The
                                                     applied up to 72 kN which is the design rail-seat load for narrow-gauge rail-track [9]. The
                                    sleeper was supported by two steel plates. The load was applied at mid-span due to the
                                                     sleeper was supported by two steel plates. The load was applied at mid-span due to the
                                    homogeneous property       along the length of the sleeper.
                                                     homogeneous property along the length of the sleeper.

                                    Figure 4. Rail-seat  compression
                                              Figure 4. Rail-seat      test (a)
                                                                  compression   test
                                                                              test (a) setup   andand
                                                                                       test setup  (b)(b)
                                                                                                       load-displacement     behaviour.
                                                                                                          load-displacement behaviour.

                                          The compressionThe  load-displacement          behaviour is
                                                                  compression load-displacement           plotted is
                                                                                                        behaviour   inplotted
                                                                                                                        Figurein4b.  The4b.
                                                                                                                                  Figure    compres-
                                                                                                                                              The compres-
                                    sion test providedsion  test provided
                                                         a non-linear         a non-linear load-displacement
                                                                          load-displacement         curve withcurve      with increasing
                                                                                                                  increasing     slope. Theslope. The initial
                                                                                                                                               initial
                                    slope up to 10 kN was linear and lower than other portions of the curve. This implies the
                                                       slope  up  to 10 kN    was  linear and  lower  than  other portions  of the curve.   This implies
                                    the specimen wasspecimen        was locally compressed at the initial stage and the slope started to increase
                                                         locally compressed          at the initial stage and the slope started to increase
                                                       thereafter due to stopping local compression. Therefore, the maximum slope in the entire
                                    thereafter due to stopping local compression. Therefore, the maximum slope in the entire
                                                       load-displacement curve was used to determine the compressive modulus of elasticity
                                    load-displacement     curve
                                                       using        was used
                                                              Equation    (2). Into   determine
                                                                                   this equation, D,theA compressive
                                                                                                         and ΔP/Δδ are modulus
                                                                                                                           the depth of ofsleeper,
                                                                                                                                            elasticity
                                                                                                                                                    effective
                                    using Equation (2).    In  this   equation,     D,  A  and   ∆P/∆δ     are  the  depth
                                                       compression area and maximum slope of the load-displacement curve. Theof sleeper,    effective
                                                                                                                                               compressive
                                    compression areamodulus
                                                        and maximum            slope
                                                                   of elasticity  was of  the load-displacement
                                                                                       obtained  450 MPa which is highercurve.than
                                                                                                                                Thethecompressive
                                                                                                                                         same property for
                                                       recycled
                                    modulus of elasticity    wasplastic    sleepers
                                                                    obtained      450(176–269
                                                                                       MPa whichMPa) isbuthigher
                                                                                                            lower than
                                                                                                                   than timber   sleepers
                                                                                                                          the same          (650 MPa)
                                                                                                                                      property     for [17].
                                                       Understanding      the   compressive    modulus   of  sleeper  is important
                                    recycled plastic sleepers (176–269 MPa) but lower than timber sleepers (650 MPa) [17].           as the  screw   holding
                                                       ability of sleeper   is dependent    on this property.
                                    Understanding the compressive modulus of sleeper is important as the screw holding
                                    ability of sleeper is dependent on this property.                               ∆
                                                                                                             = ×                                         (2)
                                                                                                                      ∆
                                                                                           D ∆P
                                                                              MOEcom =       ×                                                     (2)
                                                           2.4.4. Modulus of Rupture (MOR) A   ∆δ
                                                                 Modulus of rupture measures the load carrying capacity of sleeper in bending. The
                                    2.4.4. Modulus oftest
                                                       Rupture     (MOR) following the procedure described in the AS 1085.22 [18]. Two speci-
                                                           was conducted
                                          Modulus of rupture
                                                      mens were measures    the load
                                                                   tested under  centrecarrying  capacity
                                                                                        point bending  at a of sleeper
                                                                                                            span  of 600 in
                                                                                                                         mm  bending.
                                                                                                                               until the The   test
                                                                                                                                          failure  (Figure
                                    was conducted following the procedure described in the AS 1085.22 [18]. Two specimens The
                                                      5a). It was observed  that the specimens  were  failed in skin buckling   and   compression.
                                    were tested under specimens   failed bending
                                                         centre point    in skin buckling  due to
                                                                                    at a span  ofthe
                                                                                                   600discontinuation
                                                                                                        mm until theoffailure
                                                                                                                            fibres in(Figure
                                                                                                                                       the hand5a).
                                                                                                                                                  lamina-
                                                      tion manufacturing process. This could be avoided if the GFRP rectangular hollow profile
                                    It was observed that the specimens were failed in skin buckling and compression. The
                                    specimens failed in skin buckling due to the discontinuation of fibres in the hand lamination
                                    manufacturing process. This could be avoided if the GFRP rectangular hollow profile is
                                    made in a pultrusion process. The maximum load and displacement (Figure 5b) observed
                                    from calibrated equipment were 325 kN at 11.1 mm for specimen-1 and 405 kN at 13 mm
                                    for specimen-2, respectively, provided an average MOR of 94 MPa according to Equation
                                    (3) where M is the average ultimate moment and c is the distance of outer fibre from the
                                    neutral axis. The MOR obtained for this sleeper is significantly higher than the MOR of
                                    softwood timber (22–34 MPa) and hardwood timber sleepers (55 MPa) [4].

                                                                                                 Mc
                                                                                     MOR =                                                         (3)
                                                                                                  I
Behaviour of Polymer Filled Composites for Novel Polymer Railway Sleepers - MDPI
Equation (3) where M is the average ultimate moment and c is the distance of outer fibre
                                                          from the neutral axis. The MOR obtained for this sleeper is significantly higher than the
                                                          MOR of softwood timber (22–34 MPa) and hardwood timber sleepers (55 MPa) [4].

                                                                                                                                                              =                                     (3)
Polymers 2021, 13, 1324                                                                                                                                                                   7 of 13

                                                                                                                                                  450
                                                                                                                                                            Specimen-1
                                                                                                                                                  400

                                                                                                                     Ultimate bending load (kN)
                                                                                                                                                            Specimen-2
                                                                                                                                                  350
                                                                                                                                                  300
                                                                                                                                                  250
                                                                                                                                                  200
                                                                                                                                                  150
                                                                                                                                                  100
                                                                                                                                                  50
                                                                                                                                                   0
                                                                                                                                                        0           5           10         15
                                                                                                                                                                  Displacement (mm)

                                                               (a)                                                                                                      (b)
                                                        Figure
                                    Figure 5. Ultimate test    5. Ultimate
                                                            results.       test
                                                                     (a) Test   results.
                                                                              setup  and (a)failure
                                                                                             Test setup and(b)
                                                                                                    mode.   failure mode. (b) Load-displacement
                                                                                                               Load-displacement    behaviour. behaviour.

                                                      2.4.5. Pull-Out Resistance
                                    2.4.5. Pull-Out Resistance
                                       Pull-out resistancePull-out
                                                            measuresresistance
                                                                         the screwmeasures
                                                                                     holding  the  screw holding
                                                                                                capacity              capacity
                                                                                                            of sleeper.   This isofan
                                                                                                                                    sleeper.  This is an im
                                                                                                                                       important
                                                     portant  property    that ensures   rail alignment     in  correct gauge.
                                  property that ensures rail alignment in correct gauge. The pull-out resistance is determined   The   pull-out  resistance is
                                                     determined based on the force required to pull-out the screw. Three standard 16 × 105 rai
                                  based on the force required to pull-out the screw. Three standard 16 × 105 rail screws
                                                     screws (shank diameter 16 mm, underhead length 105 mm and shank length 35 mm) sup
                                  (shank diameter 16 mm, underhead length 105 mm and shank length 35 mm) supplied
                                                     plied by Cold Forge Pty Ltd (Caringbah, NSW, Australia) were inserted into the sleeper
                                  by Cold Forge Pty Ltd (Caringbah, NSW, Australia) were inserted into the sleeper. The
                                                     The test setup is shown in Figure 6a and the pull-out force and crosshead displacement is
                                  test setup is shown    in Figure
                                                     plotted          6a and
                                                              in Figure         themaximum
                                                                           6b. The   pull-out pull-out
                                                                                                 force and       crosshead
                                                                                                             resistance       displacement
                                                                                                                         provided                is
                                                                                                                                      by three screws    were
                                  plotted in Figure 15.57
                                                     6b. The     maximum       pull-out   resistance     provided      by  three   screws
                                                            kN, 12.78 kN, and 11.29 kN with an average of 13.2 kN (standard deviation 2.17)  were
                                  15.57 kN, 12.78 kN,   and
                                                     This     11.29 kN
                                                           resistance       withthan
                                                                       is lower   an average
                                                                                       the minimumof 13.2    kN (standard
                                                                                                         pull-out   resistancedeviation
                                                                                                                               of 22.2 kN 2.17).
                                                                                                                                             required as per
                                  This resistance isAREMA
                                                      lower than     the minimum
                                                                specification            pull-out
                                                                               [16]. Moreover,    theresistance
                                                                                                      resistance isofalso
                                                                                                                        22.2  kN required
                                                                                                                           significantly   lowerasthan the 40
                                  per AREMA specification
                                                     kN pull-out [16].  Moreover,
                                                                   resistance         the for
                                                                                required   resistance
                                                                                               traditionalis also
                                                                                                              timbersignificantly
                                                                                                                      sleeper as per lower   than standard
                                                                                                                                        AS1085.18
                                  the 40 kN pull-out [19]. The low pull-out
                                                        resistance    required resistance  is due to the
                                                                                  for traditional          low transverse
                                                                                                       timber     sleeper asshear
                                                                                                                               percapacity    of the PU core
                                                                                                                                      AS1085.18
 Polymers 2021, 13, x FOR PEER REVIEW                                                                                                         8 of 13
                                  standard [19]. The low pull-out resistance is due to the low transverse shear capacity of the
                                  PU core.

                                                                                                                18
                                                                                                                                                        Screw-1
                                                                                                                16                                      Screw-2
                                                                                       Pull-out strength (KN)

                                                                                                                14                                      Screw-3
                                                                                                                12
                                                                                                                10
                                                                                                                8
                                                                                                                6
                                                                                                                4
                                                                                                                2
                                                                                                                0
                                                                                                                     0                                     2           4              6
                                                                                                                                                    Crosshead displacement (mm)

                                       (a)                                                                                                                        (b)
                           Figure6.6.Pull-out
                          Figure      Pull-outbehaviour.
                                               behaviour.(a)
                                                          (a)Pull-out
                                                              Pull-outtest
                                                                       testsetup.
                                                                            setup.(b)
                                                                                   (b)Pull-out
                                                                                       Pull-outforce
                                                                                                forcevs
                                                                                                      vsdisplacement.
                                                                                                         displacement.

                                     2.5.Findings
                                    2.5.  Findingsfrom
                                                   FromSleeper
                                                        SleeperConcept-1
                                                                Concept-1
                                          ItItisisobvious
                                                   obviousthat
                                                             thatthe
                                                                  thealternative
                                                                      alternativesleeper
                                                                                    sleeperhashastotoperform
                                                                                                      performsatisfactorily
                                                                                                                satisfactorilyas
                                                                                                                               asper
                                                                                                                                   perstandard
                                                                                                                                       standard
                                    requirements.
                                     requirements. The   The performance
                                                               performanceofofthethesleeper
                                                                                        sleeper  Concept-1
                                                                                               Concept-1       obtained
                                                                                                            obtained     from
                                                                                                                      from   the the extensive
                                                                                                                                 extensive  test-
                                    testing   program
                                     ing program       is is tabulated
                                                          tabulated  ininTable
                                                                          Table4.4.ItItcan
                                                                                        canbe
                                                                                            beseen
                                                                                               seenthat
                                                                                                      that the
                                                                                                           the bending modulus
                                                                                                                         modulusof  ofelasticity
                                                                                                                                       elasticity
                                    and
                                     andmodulus
                                           modulusof    ofrupture
                                                            ruptureofofthe
                                                                        thePU
                                                                            PUfoam
                                                                                foamcore coreFRP
                                                                                               FRPsleeper
                                                                                                     sleeper(Concept-1)
                                                                                                              (Concept-1)satisfactorily
                                                                                                                            satisfactorilymeet
                                                                                                                                            meet
                                    the  performance        criteria while  density     and  rail-seat  compression    modulus
                                     the performance criteria while density and rail-seat compression modulus are slightly         are  slightly
                                     lower than timber. However, the screw pull-out resistance is lower than the minimum
                                     requirement as per AREMA specification for polymer composite sleeper. Therefore, a fur-
                                     ther investigation is necessary to overcome the limitations of PU foam core FRP sleeper.
                                     The next section highlighted how to improve screw pull-out resistance without sacrificing
                                     other requirements.
Behaviour of Polymer Filled Composites for Novel Polymer Railway Sleepers - MDPI
Polymers 2021, 13, 1324                                                                                                     8 of 13

                                   lower than timber. However, the screw pull-out resistance is lower than the minimum
                                   requirement as per AREMA specification for polymer composite sleeper. Therefore, a
                                   further investigation is necessary to overcome the limitations of PU foam core FRP sleeper.
                                   The next section highlighted how to improve screw pull-out resistance without sacrificing
                                   other requirements.

                              Table 4. Performance Comparison of PU Foam Core FRP Sleeper (Concept-1).

                                                                                      AREMA
                 Properties                   Concept-1         Softwood                                      Observation
                                                                                    Requirements
 Density (kg/m3 )                                640               855              Not available         Lighter than timber
 Bending modulus of elasticity (GPa)             5.15              7.4                  1.17                 Satisfactory
 Rail-seat compression modulus (MPa)             450               650              Not available         Lower than timber
 Modulus of rupture (MPa)                         94              22–34                 13.8                 Satisfactory
 Screw pull-out resistance (kN)                  13.2               40                  22.2                Unsatisfactory

                                   3. Overcoming Challenges of Sleeper Concept-1
                                   3.1. Development of PFR Core FRP Sleeper Concept (Concept-2)
                                         The low strength capacity of PU foam core in sleeper Concept-1 is the main issue
                                   identified for low screw holding capacity as no crack was observed on the FRP. Therefore,
                                   the strength properties of core material need to be improved. One approach to improve
                                   the core properties is to use the particulate filled resin (PFR) system. Ferdous et al. and
                                   Khotbehsara et al. [20–22] developed a PFR that has superior strength properties and could
                                   be suitable for manufacturing polymer railway sleepers. However, the PFR is expensive
                                   compared to PU core since the latter one is a foam that can add volume without increasing
                                   cost. Therefore, a minimum volume of PFR should be used to minimise the cost of sleeper.
                                   Since the purpose of introducing PFR is to improve the screw holding capacity, they can
                                   be filled at the rail-seat region only while the other parts of the hollow FRP tube can be
                                   filled with low cost material such as ordinary portland cement (OPC) concrete which is
                                   even cheaper than PU foam core. This approach may increase the overall weight of the
                                   sleeper as both PFR and OPC concrete are heavier than PU core. However, the density of
                                   sleeper Concept-1 is lower than timber (Table 4) and thus a further increase of density may
                                   not create problem. Moreover, it is expected that the density of timber replacement sleeper
                                   should be similar to the density of timber. While lighter sleepers are easy to handle, they
                                   are however less effective to provide lateral stability of the rail-track. A schematic diagram
                                   of the whole concept is provided latter.

                                   3.2. Materials and Manufacturing of Sleeper Concept-2
                                         The 5.2 mm thick FRP tubes used in Concept-2 were fabricated by pultrusion process
                                   and were made of E-glass fibre and vinyl-ester resin with a fibre volume fraction of 60%.
                                   The hollow pultruded section is a preferred choice over the laminates overlapping method
                                   discussed in Concept-1 as the latter one was failed due to skin buckling (Figure 5a). The
                                   PFR in this study was prepared by mixing polyester resin and methyl ethyl ketone peroxide
                                   (MEKP) hardener with a mixing ratio of 100:1.5 g and filled the resin matrix with short
                                   polypropylene (PP) fibres and fly ash fillers. The fillers were mixed together prior to mixing
                                   resin and hardener. Once prepared a homogeneous resin and hardener mix, the mixed
                                   fillers were added to the resin system. The bottom of the FRP tubes were sealed and placed
                                   vertically to fill the tubes from the top end. When tubes were filled with OPC and PFR, the
                                   pouring was done in separate days for each mix. Before testing, the samples were cured in
                                   normal temperature and humidity for more than 28 days.

                                   3.3. Results and Discussion—Performance Evaluation of Sleeper Concept-2
                                   3.3.1. Pull-Out Resistance
                                        Six standard screws were inserted in the PFR core FRP sleeper (Concept-2) as shown
                                   in Figure 7a. The results are plotted in Figure 7b. The first major drop of load for Screw-1,
Behaviour of Polymer Filled Composites for Novel Polymer Railway Sleepers - MDPI
vertically to fill the tubes from the top end. When tubes were filled with OPC and PFR,
                                  the pouring was done in separate days for each mix. Before testing, the samples were
                                  cured in normal temperature and humidity for more than 28 days.

                                  3.3. Results and Discussion—Performance Evaluation of Sleeper Concept-2
Polymers 2021, 13, 1324                                                                                                                             9 of 13
                                  3.3.1. Pull-Out Resistance
                                       Six standard screws were inserted in the PFR core FRP sleeper (Concept-2) as shown
                                  in Figure 7a. The results are plotted in Figure 7b. The first major drop of load for Screw-1,
                                  Screw-2
                                  Screw-2 and
                                            and Screw-3
                                                Screw-3 were
                                                         were observed
                                                               observed at
                                                                         at 40.47
                                                                            40.47 kN,
                                                                                  kN, 43.20
                                                                                      43.20 kN
                                                                                             kN and
                                                                                                 and 39.81
                                                                                                     39.81 kN
                                                                                                           kN with
                                                                                                               with an
                                                                                                                    an average
                                                                                                                        average
                                  of 41.16 kN (standard deviation of 1.8). Only three screws were tested as the ultimate
                                  of 41.16 kN (standard deviation of 1.8). Only three screws were tested as the ultimate
                                  pullout resistance for the first three screws were consistent. It can be seen that the PFR
                                  pullout resistance for the first three screws were consistent. It can be seen that the PFR
                                  core (41.16 kN) in sleeper Concept-2 significantly improved the pull-out resistance when
                                  core (41.16 kN) in sleeper Concept-2 significantly improved the pull-out resistance when
                                  compare to PU foam core (13.2 kN only) in sleeper Concept-1. Moreover, the average screw
                                  compare to PU foam core (13.2 kN only) in sleeper Concept-1. Moreover, the average
                                  holding capacity of PFR core sleeper is very similar to the minimum required capacity for
                                  screw holding capacity of PFR core sleeper is very similar to the minimum required ca-
                                  timber sleepers (40 kN as per AS1085.18 standard). Therefore, PFR core has potential for
                                  pacity for timber sleepers (40 kN as per AS1085.18 standard). Therefore, PFR core has po-
                                  manufacturing polymer railway sleepers.
                                  tential for manufacturing polymer railway sleepers.
                                                                                                          60
                                                                                                                   Screw-1
                                                                                                          50       Screw-2

                                                                                    Pull-out force (kN)
                                                                                                                   Screw-3
                                                                                                          40

                                                                                                          30

                                                                                                          20

                                                                                                          10

                                                                                                          0
                                                                                                               0     2        4     6      8   10
                                                                                                                         Displacement (mm)

                                   (a)                                                                                       (b)
      Figure 7.
      Figure 7. Pull-out
                Pull-out test
                         test of
                              of the
                                 the PFR
                                     PFR core
                                         core FRP
                                              FRP sleeper
                                                  sleeper (Concept-2).
                                                           (Concept-2). (a)
                                                                        (a) Pull-out
                                                                            Pull-out test
                                                                                     test setup.
                                                                                          setup. (b)
                                                                                                 (b) Pull-out
                                                                                                     Pull-out force
                                                                                                              force vs
                                                                                                                    vs displacement.
                                                                                                                       displacement.

                                  3.3.2. Effect of the Joint between OPC and PFR
                                        Since the
                                        Since  theprimary
                                                   primarycomponent
                                                             componentofofdrillable
                                                                              drillablePFR
                                                                                        PFRis is resin,
                                                                                              resin,     it more
                                                                                                     it is  is more  expensive
                                                                                                                  expensive       than
                                                                                                                               than     nor-
                                                                                                                                    normal
                                  mal OPC
                                  OPC         concrete
                                         concrete  whichwhich   is non-drillable.
                                                          is non-drillable.         Therefore,
                                                                               Therefore,         an optimal
                                                                                           an optimal            usePFR
                                                                                                            use of    of PFR
                                                                                                                          onlyonly   at rail-
                                                                                                                                at rail-seat
                                  seat region
                                  region   wherewhere  the screws
                                                  the screws         are drilled
                                                               are drilled couldcould   significantly
                                                                                   significantly          minimise
                                                                                                   minimise           the of
                                                                                                                the cost   cost of sleepers.
                                                                                                                             sleepers.  The
                                  The other
                                  other   partsparts should
                                                should        be filled
                                                        be filled       with normal
                                                                  with normal           OPC concrete.
                                                                                 OPC concrete.     In such In asuch
                                                                                                                case,a several
                                                                                                                        case, several  bond
                                                                                                                                bond areas
                                  between PFR and OPC concrete are obvious which could create weak zones due to the
                                  variation of their elastic modulus properties. To address this concern, one of the two FRP
                                  tubes was filled with PFR and the other one was filled with a combination of normal OPC
                                  concrete and PFR by equal volume (Figure 8a,b). Centre-point bending test was conducted
                                  to create maximum moment at the bond area as shown in Figure 8b. Both beams were
                                  failed in a similar manner due to the longitudinal shear cracks appeared in FRP tubes
                                  (Figure 8c). The FRP tubes were opened after ultimate failure and it was observed that the
                                  in-fill concrete was cracked at the load point for both beams, particularly the in-fill concrete
                                  in the second beam was failed at the OPC-PFR interface (Figure 8c). However, the joint
                                  between OPC and PFR did not affect the overall behaviour as shown in Figure 8d. The
                                  load-displacement behaviour of both beams were very similar in terms of strength, stiffness
                                  and post-cracking behaviour. This is because the overall behaviour of the beam is governed
                                  by FRP tubes and the type of in-fill materials has less impact due to the confinement
                                  effect. Therefore, it can be said that the PFR is compatible with OPC as in-fill material for
                                  manufacturing polymer railway sleepers.
Behaviour of Polymer Filled Composites for Novel Polymer Railway Sleepers - MDPI
in-fill concrete was cracked at the load point for both beams, particularly the in-fill con-
                                      crete in the second beam was failed at the OPC-PFR interface (Figure 8c). However, the
                                      joint between OPC and PFR did not affect the overall behaviour as shown in Figure 8d.
                                      The load-displacement behaviour of both beams were very similar in terms of strength,
Polymers 2021, 13, 1324
                                      stiffness and post-cracking behaviour. This is because the overall behaviour of the beam
                                                                                                                             10 of 13
                                      is governed by FRP tubes and the type of in-fill materials has less impact due to the con-
                                      finement effect. Therefore, it can be said that the PFR is compatible with OPC as in-fill
                                      material for manufacturing polymer railway sleepers.
                          400 mm                    400 mm                               400 mm                400 mm
                            PFR                       PFR                                 OPC                    PFR

                            300 mm                  300 mm                                                     300 mm            300 mm
                                           (a)                                                                           (b)

                                                                                                      60

                                                                                                      50

                                                                                                      40

                                                                                         Load, (kN)
                                                                                                      30

                                                                                                      20

                                                                                                      10                Filled with PFR only
                                                                                                                        Filled with PFR and OPC
                                                                                                       0
                                                                                                           0           5          10              15
                                                                                                                 Midspan displacement, (mm)

                                           (c)                                                                           (d)
          Figure
      Figure       8. Effect
               8. Effect     of joint
                         of joint     between
                                   between OPCOPC and
                                                and   PFR.
                                                    PFR. (a)(a)
                                                             FRPFRP tube
                                                                  tube    filled
                                                                       filled    with
                                                                               with   PFR
                                                                                    PFR   only.
                                                                                        only. (b)(b)
                                                                                                  FRPFRP tube
                                                                                                       tube    filled
                                                                                                            filled    withPFR
                                                                                                                    with   PFRand
                                                                                                                               andOPC.
                                                                                                                                   OPC.(c)
          (c) Failure mode. (d) Load-displacement plot.
      Failure mode. (d) Load-displacement plot.
                                       3.3.3. Full Length Sleeper Deflection Behaviour
                                    3.3.3. Full Length Sleeper Deflection Behaviour
                                             There still remains the question of how the full-scale sleeper will behave in rail-track.
                                       To There   still remains
                                           understand               the question
                                                           the in-track  deflectionofbehaviour
                                                                                      how the full-scale   sleeper
                                                                                                of full-scale        willa behave
                                                                                                               sleeper,    five-pointin bending
                                                                                                                                        rail-track.
                                    Totest
                                         understand     the  in-track  deflection   behaviour   of full-scale  sleeper,   a five-point
                                             was conducted. The justification of the five-point bending test setup for railway           bending
                                    test  was   conducted.     The  justification of the five-point bending     test setup
                                       sleeper is discussed in [4]. The load was applied until the ultimate failure at 143 kNfor railway   sleeper
                                                                                                                                                of
                                    is total
                                       discussed   in [4].72The
                                              load (i.e.,     kNload    wasrail-seat).
                                                                   at each   applied until
                                                                                       The the ultimate
                                                                                            specimen   wasfailure
                                                                                                             failedatdue
                                                                                                                      143 to
                                                                                                                           kNtheof total load (i.e.,
                                                                                                                                   longitudinal
                                    72shear
                                        kN atcrack
                                                each in
                                                      rail-seat).  Theupper
                                                          FRP at the    specimen
                                                                               end. was
                                                                                    The failed dueshape
                                                                                         bending    to theoflongitudinal
                                                                                                              the beam is shear     crack
                                                                                                                              plotted      in FRP
                                                                                                                                       in Figure
                                    at 9b.
                                        theItupper  end.
                                               can be  seen The  bending
                                                              that          shape
                                                                    a positive     of the (sagging
                                                                                bending   beam is plotted
                                                                                                    moment) in Figure
                                                                                                                occurred9b.atItrail-seat
                                                                                                                                can be seen    that
                                                                                                                                          region
                                    a positive bending (sagging moment) occurred at rail-seat region while negative bending
                                    (hogging moment) observed at mid-span. This is the generalbehaviour observed in real
                                    rail-track condition [23]. The maximum deflection observed at rail-seat location is 5.73 mm
                                    which is larger than the theoretical deflection of 2.66 mm determined in [4]. This is because
                                    a smaller section of 100 × 100 mm instead of the actual sleeper section (230 × 115 mm2 )
                                    was tested to understand whether the concept is suitable for manufacturing sleeper. In this
                                    study, 2.15 times larger (i.e., 5.73/2.66) deflection of the beam than the deflection of the
                                    actual size sleeper is expected as the dimensions of the actual sleeper are 2.3 times wider
                                    (i.e., 230/100) and 1.15 times deeper (i.e., 115/100).

                                    3.4. Findings from Sleeper Concept-2
                                         Sleeper Concept-2 was introduced to overcome the challenge of low screw holding
                                    capacity in sleeper Concept-1. Replacing PU foam core by PFR can significantly improve
                                    and meet the requirements of pull-out resistance for polymer sleepers. Since PFR is an
                                    expensive material, its optimal use is important to minimise the cost of sleepers. Therefore,
                                    the rail-seats region of the FRP tube need to be filled with drillable PFR while other parts
Polymers 2021, 13, 1324                                                                                                          11 of 13

                                   can be filled with non-drillable OPC concrete. It was found that the joint between PFR and
                                   OPC concrete does not affect the overall behaviour. Figure 10 proposed the distribution of
                                   infill materials along the sleeper length. Only 600 mm at the two rail-seat locations11need
Polymers 2021, 13, x FOR PEER REVIEW                                                                                          of 13
                                   PFR as an infill material based on the stress distribution pattern described in [9]. This
                                   concept can save almost 50% volume of PFR. Moreover, the FRP tube with a thickness
                                   of 4 mm can provide sufficient strength and stiffness properties. It is estimated that the
                                  while negative bending (hogging moment) observed at mid-span. This is the generalbe-
                                   materials cost of the proposed sleeper concept would be approximately AU$100 per sleeper
                                  haviour observed in real rail-track condition [23]. The maximum deflection observed at
                                   which is quite below than the target final sleeper cost of AU$160 indicated by Queensland
                                  rail-seat location is 5.73 mm which is larger than the theoretical deflection of 2.66 mm
                                   Rail (excluding sleeper reprocessing cost at the end of their life). Although the final product
                                  determined in [4]. This is because a smaller section of 100 × 100 mm instead of the actual
                                   cost of $160 is twice the cost of traditional timber sleeper ($80), however, the life cycle
                                  sleeper section (230 × 115 mm2) was tested to understand whether the concept is suitable
                                   cost of composite sleeper (50 years design life) is expected to be lower than timber sleeper
                                  for manufacturing sleeper. In this study, 2.15 times larger (i.e., 5.73/2.66) deflection of the
                                   (15 years design life). Therefore, manufacturing a high performance and cost effective
                                  beam than the deflection of the actual size sleeper is expected as the dimensions of the
                                   polymer composite railway sleeper is possible using the proposed concept.
                                  actual sleeper are 2.3 times wider (i.e., 230/100) and 1.15 times deeper (i.e., 115/100).

                          500 mm                               1130 mm                                  500 mm

                            700 mm                            730 mm                          500 mm           200 mm
                              PFR                           OPC concrete                        PFR              PFR
                                                                   (a)

 Polymers 2021, 13, x FOR PEER REVIEW                                                                                              12 of 13

                                    the final product cost of $160 is twice the cost of traditional timber sleeper ($80), however,
                                    the life cycle cost of composite sleeper (50 years design life) is expected to be lower than
                                                                    (b)
                                    timber sleeper (15 years design life). Therefore, manufacturing a high performance and
           Figure
           Figure 9.
                  9. Full-scale
                     Full-scaledeflection  behaviour.
                                    cost effective
                                deflection            (a)
                                                       (a) Five-point
                                                   polymer
                                           behaviour.                 bending
                                                                composite
                                                           Five-point         (5-PB)
                                                                           railway
                                                                      bending        test
                                                                                     test setup.
                                                                              (5-PB)sleeper      (b)
                                                                                                  (b) Bending
                                                                                              is possible
                                                                                          setup.              profile
                                                                                                           using
                                                                                                      Bending    theof
                                                                                                              profile    sleeper.
                                                                                                                      proposed
                                                                                                                      of sleeper. concept.

                                   3.4. Findings From Sleeper Concept-2
                                        Sleeper Concept-2 was introduced to overcome the challenge of low screw holding
                                  capacity in sleeper Concept-1. Replacing PU foam core by PFR can significantly improve
                                  and meet the requirements of pull-out resistance for polymer sleepers. Since PFR is an
                                  expensive material, its optimal use is important to minimise the cost of sleepers. There-
                                  fore, the rail-seats region of the FRP tube need to be filled with drillable PFR while other
                                  parts can be filled with non-drillable OPC concrete. It was found that the joint between
                                Figure10.
                               Figure  10.Proposed
                                           Proposedfinal
                                                     finaldesign
                                                           designofofpolymer
                                                                      polymersleeper
                                                                              sleeper(based
                                                                                      (basedononConcept-2).
                                                                                                 Concept-2).
                                  PFR and    OPC concrete     does not affect  the overall behaviour.   Figure 10 proposed the dis-
                                  tribution of infill materials along the sleeper length. Only 600 mm at the two rail-seat lo-
                                    4. Conclusions
                                  cations need PFR as an infill material based on the stress distribution pattern described in
                                          This
                                  [9]. This    study proposed
                                             concept   can save aalmost
                                                                     new concept   for manufacturing
                                                                           50% volume                   fibre reinforced
                                                                                           of PFR. Moreover,              polymer
                                                                                                                the FRP tube   withrail-
                                                                                                                                     a
                                    way   sleeper. The   systematic    design approach    and  experimental   program   identified
                                  thickness of 4 mm can provide sufficient strength and stiffness properties. It is estimated      new
                                    materials
                                  that         and method
                                        the materials   cost offor
                                                                thedeveloping    composite
                                                                     proposed sleeper         sleeper
                                                                                         concept      concept.
                                                                                                  would         The following
                                                                                                          be approximately      conclu-
                                                                                                                             AU$100
                                    sions
                                  per      are made:
                                       sleeper  which is quite below than the target final sleeper cost of AU$160 indicated by
Polymers 2021, 13, 1324                                                                                                        12 of 13

                                  4. Conclusions
                                       This study proposed a new concept for manufacturing fibre reinforced polymer
                                  railway sleeper. The systematic design approach and experimental program identified new
                                  materials and method for developing composite sleeper concept. The following conclusions
                                  are made:
                                  •    Filled FRP tube is a promising concept for developing polymer railway sleepers. To
                                       meet the strength and stiffness requirements, a minimum tube thickness of 4 mm is
                                       necessary.
                                  •    Polyurethane foam as an infill material can provide sufficient bending and compres-
                                       sion properties. However, it cannot provide sufficient resistance to hold screws.
                                  •    Particulate filled resin (PFR) system as an infill material can overcome the limitation
                                       of low screw holding capacity that was observed in polyurethane foam.
                                  •    The expensive and drillable infill PFR material can be replaced by the inexpensive and
                                       non-drillable OPC concrete except rail-seat locations.
                                  •    The joint between PFR and OPC concrete does not affect the overall performance of
                                       the sleeper as the behaviour of the sleeper is governed by an external FRP tube and
                                       the type of in-fill materials have only minimal impact due to the confinement effect.
                                  •    The proposed design of sleeper only requires 50% volume of PFR as infill material that
                                       lead to manufacture a high performance and cost effective railway sleeper technology.
                                       Railway sleepers are often subjected to impact and fatigue loading due to flat wheel
                                  and repeated movements of the train. Therefore, an in-depth understanding of the impact
                                  and fatigue behaviour of the polymer sleeper will ensure its suitability to replace existing
                                  timber sleepers. To understand the fatigue behaviour of a polymer sleeper, the author
                                  attempted to investigate the fatigue behaviour of GFRP laminates [24,25].

                                  Author Contributions: W.F.: conceptualization, methodology, data curation, formal analysis, inves-
                                  tigation, writing—original draft preparation; A.M.: supervision, writing—review & editing; C.S.:
                                  writing—review & editing; P.Y.: writing—review & editing; R.A.: methodology; T.H.: writing—
                                  review & editing; P.S.: supervision. All authors have read and agreed to the published version of the
                                  manuscript.
                                  Funding: This research was funded through Cooperative Research Centres Projects, grant number
                                  [CRC-P57360-CRC-P Round 3] and The APC was waived by MDPI.
                                  Institutional Review Board Statement: Not applicable.
                                  Informed Consent Statement: Not applicable.
                                  Data Availability Statement: Not applicable.
                                  Acknowledgments: This study is supported by the Cooperative Research Centres Projects (CRC-
                                  P57360-CRC-P Round 3) grant.
                                  Conflicts of Interest: The authors declare no conflict of interest.

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