Instruction Manual Model FU20-FTS Differential pH/ORP sensor - Helpjuice
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Model FU20-FTS Instruction Differential pH/ORP sensor Manual IM 12B06J03-05E-E 3rd edition
2 (BG) (E) Всички улътвания за продукти от серията Todos los manuales de instrucciones para ATEX Ex ce лредлагат на английски los productos antiexplosivos de ATEX están език. Ако се нуждаете oт улътвания за disponibles en inglés. Si desea solicitar las продукти oт серията Ex на родния ви instrucciones de estos artículos antiexplosivos eзик, ce свържете c най-близкия oфис или en su idioma local, deberá ponerse en contacto представителство на фирма Yokogawa. con la oficina o el representante de Yokogawa más cercano. (CZ) Všechny uživatelské příručky pro výrobky, na (F) něž se vztahuje nevýbušné schváleni ATEX Tous les manuels d’instruction des produits Ex, jsou dostupné v angličtině. Požadujete-li ATEX Ex sont disponibles en langue anglaise. pokyny týkající se výrobků s nevýbušným Si vous nécessitez des instructions relatives schválením ve vašem lokálním jazyku, aux produits Ex dans votre langue, veuillez kontaktujte prosím vaši nejbližší reprezentačni bien contacter votre représentant Yokogawa le kancelář Yokogawa. plus proche. (D) (GB) Alle Betriebsanleitungen für ATEX Ex All instruction manuals for ATEX Ex related bezogene Produkte stehen in den Sprachen products are available in English. Should you Englisch. Sollten Sie die Betriebs- anleitungen require Ex related instructions in your local für Ex-Produkte in Ihrer Landessprache language, you are to contact your nearest benötigen, setzen Sie sich bitte mit Ihrem Yokogawa office or representative. örtlichem Yokogawa-Vertreter in Verbindung. (GR) (DK) Ολα τα εγχειριδια λειτουργιας των Alle brugervejledninger for produkter relateret προιοντων με ATEX Ex διατιθενται στα til CE er tilgængelige på engelsk. Skulle De Αγγλικα. Σε περιπτωση πον χρειαζεοτε ønske yderligere oplysninger om håndtering οδηγιεξ σχετικα με Ex στην τοπικη af CE produkter på eget sprog, kan De rette γλωσσα παρακαλονμε επικοινωνηστε με henvendelse herom til den nærmeste Yokogawa το πλησιεστερο γραφειο τηζ Yokogawa η afdeling eller forhandler. αντιπροσωπο τηξ. (EST) (H) Kõik ATEX Ex toodete kasutamisjuhendid on Az ATEX Ex mûszerek gépkönyveit angol esitatud inglise keeles. Ex seadmete muukeelse nyelven adjuk ki. Amennyiben helyi nyelven dokumentatsiooni saamiseks pöörduge lähima kérik az Ex eszközök leírásait, kérjük keressék lokagava (Yokogawa) kontori või esindaja fel a legközelebbi Yokogawa irodát, vagy poole. képviseletet. (I) Tutti i manuali operativi di prodotti ATEX contrassegnati con Ex sono disponibili in inglese. Se si desidera ricevere i manuali operativi di prodotti Ex in lingua locale, mettersi in contatto con l’ufficio Yokogawa più vicino o con un rappresentante. IM 12B06J03-05E-E
3 (LV) (PL) Visas ATEX Ex kategorijas izstrâdâjumu Wszystkie instrukcje obsługi dla urządzeń Lietoðanas instrukcijas tiek piegâdâtas w wykonaniu przeciwwybuchowym Ex, angïu valodâs. Ja vçlaties saòemt Ex ierîèu zgodnych z wymaganiami ATEX, dostępne dokumentâciju citâ valodâ, Jums ir jâsazinâs ar są w języku angielskim. Jeżeli wymagana firmas Jokogava (Yokogawa) tuvâko ofisu vai jest instrukcja obsługi w Państwa lokalnym ję pârstâvi. zyku, prosimy o kontakt z najbliższym biurem Yokogawy. (LT) Visos gaminiø ATEX Ex kategorijos (RO) Eksploatavimo instrukcijos teikiami anglø Toate manualele de instructiuni pentru kalbomis. Norëdami gauti priestaisø Ex produsele ATEX Ex sunt in limba engleza. dokumentacijà kitomis kalbomis susisiekite su In cazul in care doriti instructiunile in limba artimiausiu bendrovës Yokogawa biuru arba locala, trebuie sa contactati cel mai apropiat atstovu. birou sau reprezentant Yokogawa. (M) (S) Il-manwali kollha ta’ l-istruzzjonijiet għal Alla instruktionsböcker för ATEX Ex prodotti marbuta ma’ ATEX Ex huma (explosionssäkra) produkter är tillgängliga disponibbli bl-Ingliż. Jekk tkun teħtieģ på engelska. Om Ni behöver instruktioner struzzjonijiet marbuta ma’ Ex fil-lingwa för dessa explosionssäkra produkter på annat lokali tiegħek, għandek tikkuntattja lill-eqreb språk, skall Ni kontakta närmaste Yokogawa rappreżentan jew uffiććju ta’ Yokogawa. kontor eller representant. (NL) (SF) Alle handleidingen voor producten die te Kaikkien ATEX Ex-tyyppisten tuotteiden maken hebben met ATEX explosiebeveiliging käyttöhjeet ovat saatavilla englannin-. Mikäli (Ex) zijn verkrijgbaar in het Engels. Neem, tarvitsette Ex-tyyppisten tuotteiden ohjeita indien u aanwijzingen op het gebied van omalla paikallisella kielellännne, ottakaa explosiebeveiliging nodig hebt in uw eigen taal, yhteyttä lähimpään Yokogawa-toimistoon tai contact op met de dichtstbijzijnde vestiging van -edustajaan. Yokogawa of met een vertegenwoordiger. (SK) (P) Všetky návody na obsluhu pre prístroje s Todos os manuals de instruções referentes aos ATEX Ex sú k dispozícii v jazyku anglickom. produtos Ex da ATEX estão disponíveis em V prípade potreby návodu pre Ex-prístroje vo Inglês. Se necessitar de instruções na sua língua Vašom národnom jazyku, skontaktujte prosím relacionadas com produtos Ex, deverá entrar miestnu kanceláriu firmy Yokogawa. em contacto com a delegação mais próxima ou com um representante da Yokogawa. (SLO) Vsi predpisi in navodila za AEX Ex sorodni pridelki so pri roki v anglišèini. Èe so Ex sorodna navodila potrebna v vašem tukejnjem jeziku, kontaktirajte vaš najbliši Yokogawa office ili predstaunika. IM 12B06J03-05E-E
4 IM 12B06J03-05E-E
5 CONTENTS 1. PREFACE 6 1.1 Introduction 6 1.2 Unpacking and Checking 6 1.3 Warranty and Service 6 1.4 Serial number 7 2. GENERAL SPECIFICATIONS 8 2.1 Measuring elements 8 2.2 Wetted parts 8 2.3 Functional specifications (at 25°C) 8 2.4 Dynamic specifications 8 2.5 Operating range 8 2.6 Regulatory standards (only for sensor with Pt1000 temp. element) 9 2.7 Shipping details 9 2.8 Environmental conditions 9 3. INSTALLATION OF FU20 10 3.1 Typical installation 10 3.1.1 Preparing the sensor for use 10 3.1.2 Mounting the sensor 10 3.2 Mounting FU20-FTS using quick removal adapters 11 3.3. Mounting the FU20-FTS in PR10 retractable 12 4. DIMENSIONS 14 5. WIRING 15 5.1 Connections of VP dual coax cable 15 5.2 Connections 16 5.3 Definition EXA/FLXA terminal numbers to FU20-FTS sensor 16 5.4 Settings for Yokogawa pH analyzer 16 6. G ENERAL CALIBRATION & MAINTENANCE PROCEDURE 17 6.1 Buffer calibration 17 6.2 Process calibration 17 6.3 Calibration of ORP and rH measurements 18 6.4 Maintenance of the FU20-FTS sensor 18 7. MODEL CODE 19 8. SPARE PARTS 19 9. EU DECLARATION OF CONFORMITY 20 10. Chemical Compatibility Chart 21 IM 12B06J03-05E-E
6 1. PREFACE 1.1 Introduction 1.3 Warranty and Service This instruction manual provides Yokogawa products and parts are information for the installation and use of guaranteed free from defects in the FU20-FTS, four-in-one wide body pH workmanship and material under normal sensors. Like the other members of the use and service for a period of (typically) 12 FU20 family the FU20-FTS is the choice months from the date of shipment from the for the majority of typical waste water manufacturer. Individual sales organizations and process applications. The FU20-FTS can deviate from the typical warranty uses a salt sensitive reference technology period, and the conditions of sale relating to eliminate problems of conventional to the original purchase order should be reference systems. consulted. Damage caused by wear and The Model FU20-FTS offers a simple and tear, inadequate maintenance, corrosion, cost effective solution for a wide variety of or by the effects of chemical processes are waste water and process applications. This excluded from this warranty coverage. In all-in-one sensor provides simultaneous the event of warranty claim, the defective measurement of pH, pNa, redox (ORP) and goods should be sent (freight paid) to the temperature if desired. Service Department of the relevant sales Organization for repair or replacement (at The rugged body is designed for easy Yokogawa’s discretion). installation into on-line and immersion applications via the 3/4” NPT threaded The following information must be included connections provided on both ends of in the letter accompanying the returned the sensor. Like the conventional FU20 goods: sensors the salt sensitive sensor fits with • Model Code and Serial Number. the PR10 retractable fitting for installation • Original Purchase Order and Date. in continuous processes where minimum • Length of time in service and description process interruption is required. Optional of the process. quick-removal adapters in both stainless • Description of the fault and circumstances steel and titanium are available to make of the failure. calibration and maintenance even easier. • Process/environmental conditions that may be related to the failure of the sensor The FU20-FTS comes with a multipole VP • Statement as to whether warranty or non- connector and requires seperate cable warranty service is requested. type WU10-V-D that is available in 5 fixed • Complete shipping and billing instructions lengths. for return of material, plus the name and phone number of a contact person that 1.2 Unpacking and Checking can be reached for further information. Upon delivery, unpack the sensor carefully • Clean Statement and inspect it to ensure it was not Returned goods that have been in damaged during shipment. If damage is contact with process fluids must be found, retain the original packing materials decontaminated and disinfected prior and then immediately notify the carrier and to shipment. Goods should carry a the relevant Yokogawa sales office. Make certificate to this effect, for the health and sure the Model Code and Serial Number on safety of our employees. Material Safety the sensor are the same as on the packing Data sheets must be included for all list. Also, check any option(s) that were components of the process to which the ordered are included and correct. sensor(options) have been exposed. IM 12B06J03-05E-E
7 1.4 Serial number The Serial number is defined by nine (9) alphanumeric characters: X1X2 Production location X3X4 Year/Month code X5X6 X7X8 X9 Tracking number Example: N3P600028 Method used for year/month numbering Table 1: Production Year code Table 2: Production Month code Year Year code Year Year code Month Month code 2014 P 2026 3 January 1 2015 R 2027 4 February 2 2016 S 2028 5 March 3 2017 T 2029 6 April 4 2018 U 2030 7 May 5 2019 V 2031 8 June 6 2020 W 2032 9 July 7 2021 X 2033 A August 8 2022 Y 2034 B September 9 2023 Z 2035 C October A 2024 1 2036 D November B 2025 2 2037 E December C IM 12B06J03-05E-E
8 2. GENERAL SPECIFICATIONS 2.1 Measuring elements : Na-glass electrode : pH-glass electrode : Silver chloride reference : Solid platinum electrode : Pt1000 temperature sensor. 2.2 Wetted parts Sensor body : PVDF-(GF25+TZ4) Earthing pin : Solid Platinum Measuring sensor : L-glass, pNa-glass LE glass tube : AR-glass O-ring : Viton Body insert : PVDF 2.3 Functional specifications (at 25°C) Isothermal point : pH7, pNa 0 Reference system : Salt sensitive, Ag/AgCl in 1M KCl Glass impedances : Nominal: 750 MΩ Liquid outlet : Non-flow no junction Temperature element : Pt1000 to IEC 751 Asymmetry potential : 0 ± 15 mV Slope : > 90% in pH 2-12 with pH = pNa+2 NOTE: T he temperature sensor included in the FU20-FTS is designed for cell compensation and for indication. It is NOT designed for process temperature control. 2.4 Dynamic specifications Response time pH : t90 < 15 sec. (for 7 to 4 pH step) Response time temp. : t90 < 120 sec. (for 10 °C step) Stabilization time pH : < 2 min. (for 0.02 pH unit during 10 sec.) 2.5 Operating range pH : 2 to 14 ORP : -1500 to 1500 mV Temperature : 0 to 105 ºC (14 to 221 ºF) Pressure : p(bar) p(bar) 10 5 FSM 0 -10 0 25 50 105 Temp. (ºC) Conductivity : > 10 µS/cm NOTE: T he pH operating range at room temperature is 2-14 pH, but at high temperatures or range outside 2-12 pH the lifetime will be seriously shortened. IM 12B06J03-05E-E
9 2.6 Regulatory standards (only for sensor with Pt1000 temp. element) CE : Decision 768/2008/EC - ATEX : Directive 94/9/EC, as amended by Regulation (EC) no. 1882/2003 - Certificate no. :D EKRA 11ATEX0014 X II 1 G Ex ia IIC T3...T6 Ga - Electrical data : For sensor input circuit connected to a certified intrinsically safe circuit with the following maximum values: Ui = 18 V; Ii = 170 mA; Pi = 0.4 W; Li = 0 mH; Ci = 0 nF (VP type) or Certified intrinsically safe Yokogawa pH/ORP transmitter Model FLXA21 series or Model FLXA202 series. - Special conditions (X): T 6 for Tamb. -40 °C to +40 °C T4 and T5 for Tamb. -40 °C to +55 °C T3 for Tam. -40 °C to +105 °C : Electrostatic charges on the sensor enclosure shall be avoided. -ROHS II : Directive 2011/65/EU Applying article category 9; Industrial monitoring and control instruments; ion selective electrodes - Pressure : Directive 97/23/EC, as amended by Regulation (EC) no. 1882/2003 - Applying article : 3.3 (Sound Engineering Practice) : Damaging the screw thread of the sensor might influence the maximum process pressure. : Sensor contains glass parts which if broken can cause cutting injuries. WEEE : Directive 2002/96/EC IECEx Applying standards : IEC 60079-0: 2007 IEC 60079-11: 2006 IEC 60079-26: 2006 Certificate no. : IECEx DEK 11.0064X Ex ia IIC T3...T6 Ga Note: When the sensor has been connected to none intrinsically safe equipment which exceeds the restrictions regarding the sensor input circuit (see electrical data), the sensor is not suitable anymore for intrinsically safe use. 2.7 Shipping details FU20-FTS Package size (L x W x H) : 300 x 100 x 75 mm 11.8 x 3.9 x 3.0 inch Package weight (max.) : 0.33 kg (0.73 lbs) 2.8 Environmental conditions Storage temperature : -10 to 50 ºC (14 to 122 ºF) Water proof : IP67 (conform IEC 60529) IM 12B06J03-05E-E
10 3. INSTALLATION OF FU20-FTS For optimum measurement results, the 3.1.1 Preparing the sensor for use FU20-FTS should be installed in a location Remove the sensor from its shipping box that offers an acceptable representation of and slide of the so-called ‘wet pocket’, the the process composition and DOES NOT tube filled with solution to prevent drying out exceed the specifications of the sensor. of the measuring elements during shipment The FU20-FTS is designed with 3/4” NPT or storage. threaded connections on both ends of the Although the sensor is factory calibrated, sensor to allow installation in a wide variety it is recommended to calibrate the sensor of applications. before first use. A general calibration procedure is described 3.1 Typical installation in Section 6 of this Instruction Manual. The FU20-FTS sensor is designed for versatile in-line, immersion or off-line installation. 3.1.2 Mounting the sensor For best results the FU20-FTS should be The simplest mounting is to use one of mounted with the process flow coming the 3/4” NPT threaded connection of the towards the sensor, and positioned at least sensor. Apply Teflon tape to the appropriate 15° above the horizontal plane to eliminate air threaded end, then install the sensor in the bubbles in the pH glass bulb (see Figure 1). process (see Figure 2). FU20 Horizontal plane TeflonTape FU20 Figure 1: Sensor installation Figure 2: Simple mounting of sensor IM 12B06J03-05E-E
11 3.2 M ounting FU20-FTS using quick 3A pply Teflon tape to the appropriate removal adapters threaded end of the sensor; The FU20-FTS can also be mounted using 4P lace the O-ring and screw the mating one of the optional quick-removal adapters part of the adapter on the sensor; (/NSS, /NTI, /BSS, /BTI, see Figure 3). For 5M ount the sensor in the adapter, making a detailed description of these adapters see sure that the O-ring seals properly; Sections 4 and 7 of this Instruction Manual. 6H and-tighten the adapter nut. 1A pply Teflon tape to the threaded end of Other mounting examples of the FU20-FTS this adapter; are given in Figure 4. 2 Install the adapter in the process connection. Tighten the adapter using a O NOT over tighten the adapter to Note: D wrench on the adapter flats. prevent damage; 1 2 3 4 5 6 Figure 3: Mounting of sensor with option /NSS, /NTI, /BSS or /BTI IM 12B06J03-05E-E
12 3.3. Mounting the FU20-FTS in PR10 5 Lead the sensor cable through the tube retractable of the fitting, from the side where the 1 Take the sensor out of the box and apply knurled knob has been removed. Attach Teflon tape to the appropriate threaded the sensor and cable as usual. end. 6 Hold the sensor still and turn the metal 2 Bind the separate wires of the cable tube onto the sensor. Don’t rotate the together with a piece of tape. cell, but rotate the tube of the fitting, 3 Take the fitting out of the box and remove because the cable can be disconnected the option(s), if necessary. from the cell, when rotating it. 4 Release the pigtail (cable gland) 7 Lead the loose part of the pigtail onto the completely. Do not undo the part in the cable and screw it onto the fixed part. metal tube! 8 Remove the tape. unit mm (inches) FIG. 4 Dimensional drawing PR10...-D32 with mounted FU20 sensor IM 12B06J03-05E-E
13 FU20-FTS + FD40 FU20-FTS + ADAPTER Fitting Process Flow O-ring /HCNF, SPRAY CLEANER Cleaning Adapter Solution ( /FPS ) (water, acid, etc.) FU20 O-ring Figure 5. Installation examples for the FU20 IM 12B06J03-05E-E
14 4. DIMENSIONS Dimensions in mm (inches) TYPE: VP8 (FTS) A H G B F ø22(0.87") C E D ¾" - 14 NPT ¾" - 14 NPT FU20-VP- ø25.9 19.6(0.78") 19.6(0.78") 10(0.39") 137.5(5.4") 201.2(7.92") Figure 6. Dimensions FU20-FTS /NSS, /NTI, /BSP, /BTI /FPS ø35.5 (1.4”) 10.0 (0.4”) 5.0 (0.2”) ø30.0 (1.18”) 20.0 (0.8”) 99.0 (3.9”) 5.0 (0.2”) ø36.0 (1.42”) 25.0 (1”) 1” NPT or ISO 7/1-R1 ø39.0 (1.54”) Figure 6. D imensions 1” FU20-FTS adapter Stainless Steel & Titanium and FU20-FTS adapter for FF40, FS40 and FD40 fittings IM 12B06J03-05E-E
15 5. WIRING 5.1 Connections of VP dual coax cable The numbers in the table refer to the numbers of the terminals in a Yokogawa pH instrument. Transparent (Brown core) Transparent (White core) Jumper Brown Yellow Green White Black Blue Red A B C D E F G H (63) Differential pH + pNA + ORP(rH) 15 16 13 17 11 12 14 - (3) none (63) FU24/FU20: pH + ORP(rH) 15 13 16 14 11 12 - - (3) - (63) FU24/FU20: pH / ref 15 13 16 14 11 12 - - (3) - (63) FU24/FU20: ORP / ref - 13 16 15 11 12 - - (3) 13-14 (63) FU24/FU20: ORP / pH 13 - 16 15 11 12 - - (3) 15-14 Table 4 The numbers (11- 17) in the table refer to the numbers on the terminals in EXA Instruments. Other instruments are indicated in the following tables Blue (F) Red (E) Black White (D) Brown (B) green brown A H G yellow Transparant (C) Transparant (A) brown B F blue C E D Green (H) Yellow (G) white red white Connector Cable Figure 7 Figure 9 IM 12B06J03-05E-E
16 5.2 Connections The FU20-FTS is provided with a Variopin connector. The connections for the sensors together with the WU10 cable is given in below section. F E Gr ee n 14 Yell ow 63 Blac G D 17 White k Core coax White White 13 H C 15 Core coax Brown Brown n Brow A B 16 11 Re d ue Bl Indication groove 12 Figure 10: Top view of sensor Variopin Figure 11: WU10 dual coax cable connector with gold plated contacts 5.3 Definition EXA/FLXA terminal numbers to FU20-FTS sensor FU20-VP with WU10-V wire color pH ORP EXA/FLXA terminal # pH+ORP ORP pH compensated pH+rH 11 Red Red Red 12 Blue Blue Blue 13 Brown Brown Clear 14 Yellow 15 Clear Yellow Yellow 16 Black 17 Black Note: F or ORP measurement the EXA/FLXA terminals 13 and 14 should be interconnected. For ORP pH compensated measurement the EXA/FLXA terminals 14 and 15 should be interconnected. 5.4 Settings for Yokogawa pH analyzer Function pH pH compensated pH&ORP pH&rH ORP Setting (default) ORP sensor setup pH pH+ORP pH+ORP ORP ORP measurement pH+ORP pH+rH setup Impedance setting input1 High High High Low Low input 2 High High High High High jumper input 1 No No No Yes Yes jumper input 2 No No No No No IM 12B06J03-05E-E
17 6. GENERAL CALIBRATION & MAINTENANCE PROCEDURE Calibration of the FU20-FTS sensor has to 4. Rinse sensor thoroughly with tap water; be done with the pH analyzer connected. 5. Immerse the sensor in the second buffer Normally the pH standards that are (pH 4.00 is recommended); preprogrammed in the pH analyzer can be Wait until the pH reading is stable. Adjust used for calibration with the pH analyzer set the pH reading in the pH analyzer to the to “AUTOCAL”. The FU20-FTS however value indicated on the bottle (in this case is a differential pH sensor which needs pH 4.00). buffers that have the same ionic strength Quit the manual calibration routine by because the sodium reference will change accepting the new calculated calibration as the ionic strength changes. These pH data of zero and slope. buffers are not preprogrammed in the pH After calibration, re-install the sensor into analyzer, which means the calibration has the process. to be done with specific buffer solutions (see Section 6.1) and the pH analyzer set Note: It is important to understand it is to “MANUAL” calibration. Refer to the possible the FU20-FTS differential analyzer Instruction Manual for details. sensor does not show the correct Calibration data of the sensor is stored into pH value in process after buffer the pH analyzer. calibration. The reason is that the ionic strength of the buffers is 1 mol 6.1 Buffer calibration NaCl, which can deviate from the To calibrate the FU20-FTS sensor, two ionic strength of the process. For an buffer solutions with known pH values accurate pH reading an extra 1 point are required. It is recommended that one process calibration has to be done buffer solution has a value near to pH (see Section 6.2) to compensate for 7.00. Depending on the process value to differences in ionic strength. be measured, the second buffer solution should be either acidic 6.2 Process calibration (below pH 7.00) or alkaline (above pH 7.00). The following is a specific 1-point manual Buffers which are available are: pH 4.00, calibration procedure for the process to pH 7.00 and pH 9.00. measure: See Section 8 for ordering information. Set the pH analyzer to “MANUAL” calibration. Wait until the pH reading is The following is a very general 2-point manual stable. calibration procedure with buffer solution: Adjust the pH reading in the pH analyzer 1. Clean the sensor using a 5% solution of to the value of the process sample that is HCl; analyzed using a laboratory measurement. 2. Rinse sensor thoroughly with tap water For the laboratory measurement, we advice (DO NOT use demineralized water); to use the Yokogawa PH72 personal pH 3. Immerse the sensor in the first buffer meter. solution (pH 7.00 is recommended); Quit the manual calibration routine by Set the pH analyzer to “MANUAL” accepting the new calculated calibration calibration. Wait until the pH reading is data of zero. Slope value will be unchanged. stable. Adjust the pH reading in the pH analyzer to the value indicated on the bottle (in this case 7.00). Go to solution 2 to do a 2-point calibration; IM 12B06J03-05E-E
18 6.3 C alibration of ORP and rH 6.4 Maintenance of the FU20-FTS sensor measurements A pH sensor requires routine maintenance For calibration of ORP and rH, the to keep the measuring elements clean and procedure for MANUAL CALIBRATION can functioning. Because the FU20-FTS sensor be used as described in the Instruction does not have an open reference junction Manual of the analyzer. and is hermetically sealed from the process, it does not suffer from poisoning, diffusion The rH value is a function of the reference and fouling. This means the FU20-FTS system and the pH value of the buffer sensor requires very little maintenance. solution. The FU20-FTS sensor has a reference system of 1molal Silver/Silver In most cases cleaning with water, iso- Chloride (Ag/AgCl). The commonly used propanol or methanol is sufficient. In other standards for ORP and rH calibration are cases the measuring elements of the sensor made from Chinhydron (Quinhydrone) have to be cleaned with specific solutions. powder dissolved in pH buffer solutions (1 Examples: g / 200 ml). In Table 5 the measurement 1. Deposits of limes, hydroxides or values are given as function of the used pH carbonates can be removed by buffer solution with Chinhydron powder. The immersing the bottom part of the sensor accuracy of the standards is approximately in a solution containing dilute hydrochloric ± 10 mV. acid (5% is recommended). Afterwards rinse the sensor with water. Table 5: ORP, pH compensated ORP and 2. Deposits of oil and fat can be removed rH as function of pH buffer solution with with hot water with a detergent. When Chinhydron powder. the results are unsatisfactory, a mild (carbonate based) abrasive can be used. pH ORP (mV) Na ORP (mV) pH rH (mV) 3. Protein deposits should be removed with buffer compensated compensated a protein enzymatic solution, for instance 4.00 228 51 23.6 a solution containing 8.5 ml concentrated 7.00 51 51 23.6 hydrochloric acid and 10 grams of pepsin 9.00 -67 51 23.6 in 1 liter of water. A soft toothbrush may be used to The accuracy of the standard values is accelerate the cleaning process. approximately +/- 10 mV. Note: A void cleaning with non-polar solvent like tri-chloro ethylene, toluene or hexane. The non-polar solvents will break up the gel-layer on the measuring glass elements and requires that the sensor has to be soaked in water for at least 12 hours before it will function again. IM 12B06J03-05E-E
19 7. MODEL CODE Model Suffix Code Option code Description FU20 Wide Body sensor Cable length -03 3 m cable -05 5 m cable Not available -10 10 m cable for model FTS and FTD -20 20 m cable -VP No Cable; Vario Pin connector Temperature -T1 Pt1000 Sensor Model -NPT Ryton, Tapered thread, Dome Shaped -FSM Ryton, Tapered thread, Flat Surface Model -FTD PVDF, Tapered thread, Dome Shaped -FTS PVDF, Tapered thread, Salt sensitive membrane Options /HCNF Complete Hastelloy cleaning system /FPS Adapter F*40 from PPO /NSS 1” NPT, SS316 /NTI 1” NPT, Titanium /BSS 1” BSP, SS316 /BTI 1” BSP, Titanium 8. SPARE PARTS Spare part Description FU20 K1523DD /FPS Adapter for FF40, FS40 and FD40 fittings (PPO) K1547PK /NSS 1” NPT, Stainless Steel adapter (Viton O-ring) K1547PL /BSS ISO 7/1-R1, Stainless Steel adapter (Viton O-ring) K1547PM /NTI 1” NPT, Titanium adapter (Viton O-ring) K1547PN /BTI ISO 7/1-R1, Titanium adapter (Viton O-ring) K1500FR Viton O-rings 29.82*2.62 (5 pcs) for 1” adapter K1500FS EPDM O-rings 29.82*2.62 (5 pcs) for 1” adapter K1500FT Silicone O-rings 29.82*2.62 (5 pcs) for 1” adapter Cleaning system for FU20 K1547PJ Hastelloy cleaning system (HCNF) K1547PG Hastelloy nozzle and mounting set (HCNF) K1547PH Nylon tube (10 metre) and tube mounting set for c hemical cleaning system Connection equipment BA10 Junction box for longer cable runs WF10-xxx-F Extension cable with terminated ends. Specify length in whole meters (e.g. XXX = 005, 010, 025, 050 meter) WU10-V-D-02 Cable for Variopin, dual coax, 2 meter WU10-V-D-05 Cable for Variopin, dual coax, 5 meter WU10-V-D-10 Cable for Variopin, dual coax, 10 meter WU10-V-D-15 Cable for Variopin, dual coax, 15 meter WU10-V-D-20 Cable for Variopin, dual coax, 20 meter Buffer solutions K1520BF Buffer solution pH 4/7/9 + PNa 0 (500 ml each), ionic strength 1 mol NaCl K1520BH Buffer solution pH 4 + pNa 0 (3 x 500 ml), ionic strength 1 mol NaCl K1520BJ Buffer solution pH 7 + pNa 0 (3 x 500 ml), ionic strength 1 mol NaCl K1520BK Buffer solution pH 9 + pNa 0 (3 x 500 ml), ionic strength 1 mol NaCl * Note: Adapter K1523JB or K1523JD needed to fit the sensor. IM 12B06J03-05E-E
20 9. EU DECLARATION OF CONFORMITY EU DECLARATION OF CONFORMITY We: Yokogawa Process Analyzers Europe B.V. Euroweg 2 3825 HD Amersfoort The Netherlands herewith declare under our sole responsibility that the product, model: FU20 further specified with model suffix- and option codes: As listed in Annex-1 in this document is manufactured in accordance with the requirements for CE-marking of products as stated in EC Decision: 768/2008/EC on a common framework for the marketing of products by applying the following standards: EN-ISO 9001: 2008 Quality management systems - Requirements Subject product is: In compliance with the essential requirements of the specific product legislation: - Pressure Equipment Directive 97/23/EC (PED) As amended by Regulation (EC) no. 1882/2003, by applying: Article 3.3: Sound Engineering Practice - RoHS 2 Directive 2011/65/EU by applying: Category 9: Industrial monitoring and control instruments, ion selective electrode - Explosive atmospheres Directive 94/9/EC (ATEX) As amended by Regulation (EC) no. 1882/2003, by applying the following standards: EN 60079-0: 2009 Explosive atmospheres – Part 0: Equipment – General requirements EN 60079-11: 2007 Explosive atmospheres – Part 11: Equipment protection by intrinsic safety “i” EN 60079-26: 2007 Explosive atmospheres – Part 26: Equipment with equipment protection level (EPL) Ga The provisions fulfilled are: II 1 G Ex ia IIC T3...T6 Ga Number of the EC-type Examination Certificate: DEKRA 11 ATEX 0014 X Name of the notified body: DEKRA Certification B.V. Identification number of the notified body: 0344 Address of the notified body: Meander 1051, 6825 MJ Arnhem, The Netherlands Produced according to appropriate quality control procedures. The CE-mark has been affixed on the product in 2012 for the first time. If applicable, the product is checked against the latest official released revision of the standards mentioned above; differences do not affect the certified product identified on this declaration. Amersfoort - March 01, 2016 H. Leijten 1/2 IM 12B06J03-05E-E
21 ANNEX-1 Model Suffix Code Option code Description FU20 Wide Body sensor Cable length -03 3 m cable -05 5 m cable Not available -10 10 m cable for model FTS and FTD -20 20 m cable -VP No Cable; Vario Pin connector Temperature -T1 Pt1000 Sensor Model -NPT Ryton, Tapered thread, Dome Shaped -FSM Ryton, Tapered thread, Flat Surface Model -FTD PVDF, Tapered thread, Dome Shaped -FTS PVDF, Tapered thread, Salt sensitive membrane Options /HCNF Complete Hastelloy cleaning system /FPS Adapter F*40 from PPO /NSS 1” NPT, SS316 /NTI 1” NPT, Titanium /BSS 1” BSP, SS316 /BTI 1” BSP, Titanium IM 12B06J03-05E-E
22 10. CHEMICAL COMPATIBILITY CHART Material PVDF S.S. 316 VITON PEEK PP PVC PFA (Kynar) Temp. % ºC 100 100 100 100 100 Conc. 20 60 20 60 20 60 20 60 20 60 20 60 20 60 Sulfiric acid 10 OOO XXX OOO OOO OO OX OOO 50 OOO XXX OOO OOX OO OO OOO 95 OX - XXX OOO - - - X - XX OOO fuming - - - - - - OOO - - - - - - - OOO Hydrochloric acid 10 OOO - - - OOO OOX OO OX OOO sat. OOO - - - OOX OO OO OOO Inorganic acid Nitric acid 25 OOX XXX OOX OOO OO OX OOO 50 OOX XXX - - - XXX X - OX OOO 95 OX - OOO - - - - - - - - - - OOO fuming - - - OOO - - - - - - - - - - OOO Phosphoric acid 25 OOO - - - OOO OOO OO OX OOO 50 OOO XXX OOO OOO OO OO OOO 95 OOO OOO XX - OOO OO OO OOO Hydrofluoric acid 40 OOO - - - OOO - - - OO OX OOO 75 OOO - - - OOO - - - OO XX OOO Acetic acid 10 OOO OOX - - - OOO OO OX OOO Organic acid glacial O X - OOX - - - OOX OX XX OOO Formic acid 80 OOO XXX - - - XXX OO O- OOX Citric acid 50 OOO OOO OOO OOO OO OO OOO Calcium hydroxide sat. OOO OOO OOO OOO OO OO OOO Potassium hydroxide 50 OOX OOO OOO OOO OO OO OOO Alkali Sodium hydroxide 40 OOX OOO XXX OOO OO OX OOO Ammonia in water 30 OOO OOO XXX OOO OO OX OOO Ammonium chloride sat. OOO XXX OOO OOO OO OO OOO Acid Zinc chloride 50 OOO XXX OOO OOO OO OO OOO salt Iron (III) chloride 50 OOO - - - OOO OOO OO OO OOO O = can be used, X = shortens useful life, - = cannot be used Sodium sulfite sat. OOO OOO - - - OOO OO OO OOO Basic salt Sodium carbonate sat. OOO OOO OOO OOO OO OO OOO Potassium chloride sat. OOO XXX OOO OOO OO OO OOO Sodium sulfate sat. OOO OOO OOO OOO OO OO OOO Calcium chloride sat. OOO XXX OOO OOO OO OO OOO Neutral salt Sodium chloride sat. OOO XXX OOO OOO OO OO OOO Sodium nitrate 50 OOO XXX OOO OOO OO OO OOO Aluminium chloride sat. OOO - - - OOO OOO OO OO OOO Hydrogen peroxide 30 OOO OOO OOO OOO OO OO OOO Oxidizing Sodium hypochloride 50 OOO XXX OOX OOO XX XX OOO agent Potassium dichromate sat. OOO OOO OOO OOO OO OO OOO Chlorinated lime OX - X X X XXX - - OO OOO Ethanol 80 OOX OOO X - - OOO OO OX OOO Cyclohexane OOX OOO OOO OOO - - OO OOO Organic solvent Toluene OOO OOO - - - OOO X - - - OOO Trichloroethane XXX OOX XXX OOO - - - - OOO Water OOO OOO OOO OOO OO OO OOO Note: Information in this list is based on our general experience and literature data and given in good faith. However Yokogawa is unable to accept responsobility for claims related to this information. IM 12B06J03-05E-E
23 IM 12B06J03-05E-E
YOKOGAWA ELECTRIC CORPORATION YOKOGAWA ELECTRIC ASIA Pte. LTD. Yokogawa has an extensive sales and World Headquarters 5 Bedok South Road 9-32, Nakacho 2-chome, Musashino-shi Singapore 469270 distribution network. Tokyo 180-8750 Singapore Japan www.yokogawa.com/sg Please refer to the European website www.yokogawa.com (www.yokogawa.com/eu) to contact your YOKOGAWA CORPORATION OF AMERICA YOKOGAWA CHINA CO. LTD. nearest representative. 2 Dart Road 3F Tower D Cartelo Crocodile Building Newnan GA 30265 No.568 West Tianshan Road Changing District USA Shanghai, China www.yokogawa.com/us www.yokogawa.com/cn YOKOGAWA EUROPE BV YOKOGAWA MIDDLE EAST B.S.C.(c) Euroweg 2 P.O. Box 10070, Manama 3825 HD AMERSFOORT Building 577, Road 2516, Busaiteen 225 The Netherlands Muharraq, Bahrain www.yokogawa.com/eu www.yokogawa.com/bh IM 12X0X0-E-E Subject to change without notice Printed in The Netherlands, 00-000 (A) I Copyright © IM 12B06J03-05E-E Printed in The Netherlands, 03-1706 Subject to change without notice Copyright ©
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