On Separation Science - 16th International Symposium FINAL PROGRAM - Invitation to 16th ISSS
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16th International Symposium
on Separation Science
Recent Advancements in Chromatography and Capillary Electromigration Techniques
FINAL PROGRAM
September 6-10, 2010
National Research Council, P.le Aldo Moro 7, Rome, Italy
FINAL PROGRAM
16th International Symposium on
Separation Science
Recent Advancements in Chromatography and
Capillary Electromigration Techniques
September 6-10, 2010
National Research Council, P.le Aldo Moro 7, Rome, Italy
1
Organizers of the Symposium
Interdivisional Group of Separation Science of the Italian Chemical Society
The 16th ISSS is organized under the auspices of the
Central European Group for Separation Sciences
Division of Analytical Chemistry of the Italian Chemical Society
Division of Chemistry for Environment and Cultural Heritage
of the Italian Chemical Society
European Society for Separation Sciences
National Research Council (CNR)
2
Welcome to Rome and the 16th International Symposium on
Separation Science
Recent Advancements in Chromatography and Capillary
Electromigration Techniques
On behalf of the Scientific and Organizing Committees and Symposium
Co-chairman Prof. Corrado Sarzanini, it is my great pleasure and honor to welcome you to the 16th
International Symposium on Separation Science – New Advancements in Chromatography and
Capillary Electromigration Techniques. I am delighted to notice that our invitation to the 16th
ISSS has been accepted by more than 200 registered delegates, coming from 29 different
European, Asian, African and American countries, which clearly demonstrates the worldwide
interest of academia and industry for separation science.
The scientific program includes 56 oral communications in plenary and parallel sessions, 8 short
presentations of posters from podium and 122 poster communications, which constitute the
primary vehicle for scientific communications in the tradition of this symposium series. Posters
make the symposium a comprehensive site for face-to-face exchange of information and for
facilitating contact with practitioners and innovators in the different areas of separation science.
Plenary session V is in Memoriam of Prof. Csaba Horváth, the greater pioneer of HPLC, who
would have celebrated his 80th birthday this year. All lectures of this session are delivered by
separation scientists who had the privilege to work at Yale University with him.
The scientific program of the symposium is complemented by an attractive social program to
facilitate meeting friends and exchanging with colleagues, including welcome reception and
lunches that will be served in the Congress site. The high-light of the social program will
definitely be the visit to Vatican Museum and Sistine Chapel, followed by a raid by bus to
Janiculum (a hill in western Rome not comprised among the proverbial Seven Hills) to enjoy the
beautiful view of Rome at sunset. The view of san Peter and Rome by night will be enjoyed by the
terrace of Villa Aurelia where an evening of traditional Italian food will be held as the social
dinner.
I thank all persons who have made possible the organization of this Symposium, in particular all
sponsors and exhibitors for providing generous financial support and the members of the Scientific
Committee for having successfully promoted the 16th ISSS. Special thanks go to all colleagues
who have submitted excellent abstracts covering many areas of separation sciences, to the
Interdivisional Group of Separation Science of the Italian Chemical Society and all other
Organizing Partners, and to the members of the Organizing Committee for their valuable effort in
making the Symposium possible.
I wish all attendees of the 16th ISSS an intellectually stimulating and awarding meeting as well
as a pleasant and unforgettable time in Rome.
Danilo Corradini
Chairman 16th ISSS
3
Honorary Committe
Giuseppe Arena, President Division Analytical Chemistry SCI, University of Catania, Italy
Luigi Campanella, President SCI, Sapienza University, Rome, Italy
Luciano Maiani, President CNR, Rome, Italy
Chairman
Danilo Corradini, CNR - Institute of Chemical Methodologies, Montelibretti, Rome, Italy
Co-Chairman
Corrado Sarzanini, University of Turin, Italy
International Scientific Committee
Dŭsan Berek*, Polymer Institute, Bratislava, Slovak Republic
Günther Bonn, Leopold-Franzes University, Innsbruck, Austria
Wolfgang Buchberger*, Johannes-Kepler University, Linz, Austria
Boguslaw Buszewski*, Nicolaus Copernicus University, Toruń, Poland
Virginia Coman*, Babeş-Bolyai University, Cluj-Napoca, Romania
Danilo Corradini, CNR - Institute of Chemical Methodologies, Montelibretti, Rome, Italy
Francesco Dondi, University of Ferrara, Italy
Attila Felinger, University of Pécs, Hungary
Modest Gertsiuk*, Institute of Geochemistry of Environment, Kiev, Ukraine
Pavel Jandera*, University of Pardubice, Czech Republic
Imre Klebovich*, Semmelweis University, Budapest, Hungary
Aldo Laganà, Sapienza University, Rome, Italy
Jozef Lehotay*, Slovak University of Technology, Bratislava, Slovak Republic
Luigi Mondello, University of Messina, Italy
Nikola Šegudović*, INA-Industrija Nafte d.d., Zagreb, Croatia
Corrado Sarzanini*, University of Turin, Italy
Lucija Zupančič-Kralj*, University of Ljubljana, Slovenia
*permanent members of CEGSS
Organizing Committee
Maria Concetta Bruzzoniti, University of Turin, Italy
Danilo Corradini, CNR - Institute of Chemical Methodologies, Montelibretti, Rome, Italy
Antonella De Rossi, CNR - Institute of Chemical Methodologies, Montelibretti, Rome, Italy
Imre Molnár, Molnár-Institute for Applied Chromatography, Berlin, Germany
Isabella Nicoletti, CNR - Institute of Chemical Methodologies, Montelibretti, Rome, Italy
Claudio Ricci, CNR – Research Area Rome 1, Montelibretti, Italy
Corrado Sarzanini, University of Turin, Italy
The 16th ISSS has received the patronage of the University of Turin, Sapienza University of
Rome, Governor of Regione Lazio, Province of Rome and City of Rome
4
The Organizing Committee acknowledges with gratitude the support of the
following Sponsors and Exhibitors
Advanstar Communications
Agilent Technologies Italia S.p.A.
Avantech Group srl
CPS Analitica
CHIRAL Technologies Europe
Chromatographia
Dionex SpA
LabService Analytica Srl
LECO Italy S.r.l.
Molnár-Institute
Shimadzu
Superchrom
Thermo Fisher Scientific S.p.A.
5.
.
6General Information
Venue Conference Halls of the CNR Headquarters in Piazzale Aldo Moro, 7
Rome (Italy), entrance at Via dei Marrucini.
Registration Lobby “Aula Convegni”
Monday: 14.00 – 16.30
Tuesday: 8.00 – 16.30
Wednesday: 8.00 – 16.30
Thursday: 8.00 – 13.00
Friday: 8.00 – 11.00
Badges A name badge must be worn by each registered participant and
accompanying person to enter the CNR building and to attend the
scientific sessions, exhibition, coffee breaks, lunches and all social events.
Tickets Each participant will receive nominative tickets which must be presented
in order to gain admittance to social events.
Symposium language The Symposium language will be English. No simultaneous translation
will be provided.
Key to lectures KL Keynote Lectures
& posters L Lectures
HML Csaba Horváth Memorial Lectures
P Posters
PP Posters from podium
Exhibition Conference site
Monday: 14.00 – 18.40
Tuesday: 8.00 – 18.40
Wednesday: 8.00 – 18.30
Thursday: 8.00 – 15.00
Friday: 8.00 – 11.20
Social program Monday, September 6: Welcome reception (17.40 – 19.00).
Thursday, September 9: visit to Vatican Museum and Sistine Chapel
(15.30 – 18.00, with departure of busses from CNR Headquarter at 15.00
sharp).
Thursday, September 9: Gala Banquette (20.00).
Friday, September 10: Farewell Reception (13.00).
Internet connection Free-of-charge wireless internet access will be available in the
Symposium area for all registered participants.
Weather September is a good time of year to visit Rome. Average temperatures are
26°C (70°F) maximum and 16°C (61°F) minimum and the weather is
usually dry.
7.
.
.
.
8How to get to CNR Headquarters
The CNR Headquarters are in Piazzale Aldo Moro at walking distance from the main railway
station (Roma Termini), served by metro ("A" and "B" Lines) and several buses. You can take at
Termini Station bus number 310 and get off at Viale dell'Università. The entrance to the
Conference Halls is at Via dei Marrucini. Two train lines connect Fiumicino airport with Rome.
The Leonardo Express is a direct service from the airport to Roma Termini station. Ticket cost
€ 14.00, and the journey into Rome takes approximately 35 minutes. Trains run every 30 minutes
from 6.23 am to 11.23 pm (from Termini to Fiumicino 5.50 am to 10.52 pm). Alternatively the
FM1 regular rail service runs from the airport to either Fara Sabina or Orte, making central stops
at Trastevere, Ostiense, Tuscolana, and Tiburtina stations. Tickets cost € 8.00, and the journey
takes approximately 45 minutes. Trains run approximately every 15 minutes (less often on
Sundays and public holidays). The bus line number 492 connects Tiburtina Station to CNR (get
off at Via dei Marrucini). If you want to use taxi from Fiumicino Airport you are strongly advised
to use white licensed taxi only.
CNR
Rome has an integrated public transport system, the tickets work on all metro, buses, trams and
city trains in the urban area. Regular tickets cost € 1 and are valid for 75 minutes from the
moment they are first stamped. Within those 75 minutes you are entitled to use one Metro
journey and any combination of buses and trams. Tickets are not on sale on buses, trams or trains.
You must buy tickets (biglietti) from tobacco shops (Tabacchi) recognizable by the "T" sign,
newsstands, and at metro stations.
More information on public transportation: http://www.atac.roma.it
Information on Fiumicino Airport: http://www.adr.it
Information on the Italian Raylway: http://www.ferroviedellostato.it
910
Scientific Information
Oral communications Lectures will last 30 and 20 minutes. It is essential that anyone adhere to
the time allotted for her/his communication. Presentations should be
prepared as PowerPoint file saved on USB sticks. The symposium‘s PCs
and laptops are equipped with Windows XP and PowerPoint version 2003.
Speakers are kindly requested to provide their presentation on USB sticks
to the registration desk by 16.30 of the day before their lecture is
scheduled. Speakers presenting their communication on Friday,
September 10 should provide their presentation on USB sticks to the
registration desk by 13.00 of Tuesday, September 9. Under no
circumstances the use of your own computer will be possible. It is
helpful for the speakers to introduce themselves to the chair persons
before the session begins in order to reduces delay at the start of the
session and facilitate the smooth transfer from one speakers to the next.
Poster presentations Each poster board measures 100 cm high by 70 cm wide. Pushpins will be
available at the registration desk. Your poster number and poster session
will be e-mailed to you. If you do not receive an e-mail by August 31,
please check the final program at http://www16ISSSRome2010.it.
Authors must be in attendance during the hours listed in the final program.
Posters should be removed at the end of each poster session. The
poster sessions are scheduled for:
- Tuesday, September 7 17.10 – 18.40
- Wednesday, September 8 17.00 – 18.30
- Thursday, September 9 13.30 – 15.00
Poster from podium The presenting Author illustrates her/his poster in the lecture hall from
podium in 5 minutes plus 3 minutes for discussion, using few slides to
illustrating her/his work as it is presented in the poster. Poster from
podium presentations should be prepared as PowerPoint file saved on
USB sticks, as it is reported above for the oral communications. Speakers
are kindly requested to provide their presentation on USB sticks to the
registration desk by 16.30 of Monday, September 7. Under no
circumstances the use of your own computer will be possible.
Poster awards All posters presented at the 16th ISSS will be evaluated by an international
panel of scientists and valuable awards will be presented on Friday,
September 10 at the Poster Award Ceremony preceding the Closing
Remarks.
16th ISSS Proceedings All papers presented at the 16th ISSS, either as lecture or poster or poster
from podium, will be considered for publication in a special issue of
Chromatographia. You are cordially invited to submit your paper for
inclusion in this issue. Manuscripts are to be submitted online directly to
the Editor by October 15, following the instructions that are available in
the Chromatographia website http://www.editorialmanager.com/chro/
The submitted manuscript will be subjected to the usual process of peer
review. All registered delegates will receive a copy of the 16th ISSS
special issue free of charge.
11Program Overview
12SCIENTIFIC PROGRAM
13Monday, September 6
Aula Convegni
16.30 OPENING CEREMONY
OPENING PLENARY LECTURE
17.00 – 17.40 Recent Progress in Column Technology
KL1 Georges Guiochon and Fabrice Gritti
Department of Chemistry, University of Tennessee, Knoxville, USA and Division
of Chemical and Analytical Sciences, Oak Ridge National Laboratory
17.40 – 19.00 WELCOME RECEPTION
Tuesday, September 7
Aula Convegni
9.30 – 10.00 LIBERTI MEDAL AWARD CEREMONY
PLENARY SESSION I
Chairpersons Danilo Corradini, Georges Guiochon
10.00 – 10.30 Environmental Problems and Chromatographic Solutions
KL2 Corrado Sarzanini
University of Turin, Department of Analytical Chemistry, Turin, Italy
10.30 – 11.00 Determination of Ionic Liquids in Natural Samples by Separation
KL3 Techniques. Problems and Solutions?
Bogusław Buszewski, Sylwia Studzińska
Chair of Environmental Chemistry and Bioanalytics, Nicolaus Copernicus
University, Faculty of Chemistry, Toruń, Poland
11.00 – 11.30 COFFEE BREAK & EXHIBITION
14Tuesday, September 7
Aula Convegni
PLENARY SESSION II
Chairpersons Pavel Jandera, Pat Sandra
11.30 – 12.00 A Novel Chip-Based Flow Modulator for Comprehensive Two-dimensional
KL4 Gas Chromatography
Luigi Mondello1,2, Peter Quinto Tranchida1, Giorgia Purcaro1, Paola Dugo1,
Giovanni Dugo1, Peter Dawes3
1
Dipartimento Farmaco-chimico, Università di Messina, Messina; 2Università
Campus Bio-Medico, Roma,Italy, 3SGE Analytical Science, Ringwood, Australia
12.00 – 12.20 Potential of Very Fast Quadrupole Mass Spectrometry (20000 amu/sec) for
L1 Analysis of Perfume Allergens Using Comprehensive Two-Dimensional Gas
Chromatography
Giorgia Purcaro1,2, Peter Quinto Tranchida1, Lanfranco Conte2, Paola Dugo1,
Giovanni Dugo1, and Luigi Mondello1,3
1
Dipartimento Farmaco-Chimico, Università di Messina, Messina; 2Dipartimento
di Scienze degli Alimenti, Università di Udine; 3Università Campus Bio-Medico,
Roma, Italy
12.20 – 12.40 Analysis of Fatty Acids (cis/trans) with Comprehensive GCMS
L2 Margit Geissler1, Shuichi Kawana2, Haruhiko Miyagawa2
1
Shimadzu Europa GmbH, Albert-Hahn-Str. 6-10, Duisburg, Germany,
2
Shimadzu Corporation, Kyoto, Japan
12.40 – 14.10 LUNCH & EXHIBITION
15Tuesday, September 7
Aula Convegni
PARALLEL SESSION I
Chairpersons Wolfgang Buchberger, Bernd Trathnigg
14.10 – 14.40 Optimization of Selectivity, Peak Capacity and Separation Time in Two-
KL5 Dimensional HPLC by Matching Separation Systems and Adjusting
Gradient Conditions in the Two Dimensions
Pavel Jandera, Tomáš Hájek, Petr Česla
Department of Analytical Chemistry, Faculty of Chemical Technology, University
of Pardubice, Czech Republic
14.40 – 15.10 Comprehensive LC Analysis of Real Samples
KL6 Paola Dugo1,2, Paola Donato2, Giovanni Dugo1, and Luigi Mondello1,2
1
Dipartimento Farmaco-Chimico, Università di Messina, Messina;2Università
Campus Bio-Medico, Roma, Italy
15.10 – 15.40 Two-Dimensional Liquid Chromatography of Synthetic Polymers
KL7 Dŭsan Berek
Polymer Institute, Slovak Academy of Sciences, Bratislava, Slovakia
15.40 – 16.00 Sample Solvent Strength and Viscous Fingering Effects in Two-Dimensional
L3 Liquid Chromatography
Michel Martin1, Manoranjan Mishra2, Anne De Wit3, Candice Grivel4, Sabine
Heinisch4
1
Ecole Supérieure de Physique et de Chimie Industrielles, Laboratoire de
Physique et Mécanique des Milieux Hétérogènes, Paris, France; 2Nonlinear
Physical Chemistry Unit and Center for Nonlinear Phenomena and Complex
Systems, Service de Chimie Physique et Biologie Théorique, Université Libre de
Bruxelles, Belgium; 3Indian Institute of Technology Ropar, Rupnagar, India;
4
Laboratoire des Sciences Analytiques, Université de Lyon ,Villeurbanne Cedex,
France
16.00 – 16.30 COFFEE BREAK & EXHIBITION
16Tuesday, September 7
Aula Marconi
PARALLEL SESSION II
Chairpersons Virginia Coman, Imre Klebovich
14.10 – 14.40 New Roles for the Separation Scientist
KL8 Lois A. Beaver
LAB Enterprise, Chevy Chase, MD, USA
14.40 – 15.10 Infrared Spectroscopy - A Novel Tool for the Physicochemical
KL9 Characterisation of Particulate, Monolithic and Coated Stationary Phases
Christian Huck
Institute of Analytical Chemistry and Radiochemistry, Leopold-Franzens
University, Innsbruck, Austria
15.10 – 15.30 Methods of Separation and Definition of Amino Acids by Mass Spectrometer
L4 and Chromatographic Methods on Carbon Sorbents
Elena S. Kuznetsova, Aleksey K. Buryak, Galina A. Petukhova
A.N. Frumkin Institute of Physical Chemistry and Electrochemistry, Russian
Academy of Sciences, Moscow, Russia
15.30 – 15.50 Determination of the Molar Mass Distribution of Ultra-High Viscosity
L5 Alginates
Henning Storz1, Derek Lohmann1, Werner-Michael Kulicke1, Ulrich
Zimmermann2, Heiko Zimmermann3
1
Institute for Technical and Macromolecular Chemistry, University of Hamburg;
2
Biozentrum, University of Würzburg; 3Fraunhofer-Institute for Biomedical
Technique, St. Ingbert, Germany
16.00 – 16.30 COFFEE BREAK & EXHIBITION
17Tuesday, September 7
Aula Convegni
PARALLEL SESSION III
Chairpersons Christian Huck, Josef Lehotay
16.30 – 16.50 Molecularly Imprinted Polymers in Capillary Electrophoresis: Drawbacks
L6 and Solutions
Cristina Giovannoli, Cinzia Passini, Patrizia Baravalle, Laura Anfossi, Claudio
Baggiani
Laboratory of Bioanalytical Chemistry, Department of Analytical Chemistry,
University of Torino, Italy
16.50 – 17.10 Multiplexed Detection of Small Analytes by Structure-Switching Aptamer-
L7 based Capillary Electrophoresis
Zhenyu Zhu1, Corinne Ravelet1, Sandrine Perrier1, Valérie Guieu1, Béatrice Roy2,
Christian Perigaud2, Eric Peyrin1
1
Département de Pharmacochimie Moléculaire, Université Grenoble I, Campus
universitaire, Saint-Martin d’Hères, France; 2Institut des Biomolécules Max
Mousseron, Université Montpellier 2, Place Eugène Bataillon, Montpellier,
France
Aula Marconi
PARALLEL SESSION IV
Chairpersons Massimo Castagnola, Claudio Corradini
16.30 – 16.50 Advances in Capillary Ion Chromatography Systems Using On-line
L8 Electrolytic Eluent Generation and Suppressed Conductivity Detection
Khalil Divan, Yan Liu, Victor Barreto, Chris Pohl
Dionex Corporation, Sunnyvale, CA, USA
16.50 – 17.10 Recent Developments in Quaternary Ultra High Performance Liquid
L9 Chromatography
Sergio A. Guazzotti1 ,Guenter Boehm2, Thomas Preiswerk2
1
Thermo Fisher Scientific, San Jose, CA, USA, 2 Thermo Fisher Scientific,
Reinach, Switzerland
17.10 – 18.40 POSTER SESSION I & EXHIBITION
18Tuesday, September 7
POSTER SESSION I P1 – P40
Chairperson Isabella Nicoletti
17.10 – 18.40
Stationary phases
Multidimensional & hyphenated techniques
Method development
Advancements in detection methods
Fundamentals I
P1 An Approach to Molecularly Imprinted Polymers for the Separation of Polar
Analytes
Claudio Baggiani, Laura Anfossi, Patrizia Baravalle, Cristina Giovannoli, Cinzia
Passini
Laboratory of Bioanalytical Chemistry, Department of Analytical Chemistry,
University of Torino, Torino, Italy
P2 Binding Behaviour of Molecularly Imprinted Stationary Phases Prepared by
a Hierarchical Approach in Mesoporous Silica Beads of Varying Porosity
Claudio Baggiani, Laura Anfossi, Patrizia Baravalle, Cristina Giovannoli, Cinzia
Passini
Laboratory of Bioanalytical Chemistry, Department of Analytical Chemistry,
University of Torino, Torino, Italy
P3 Fast LC-MS/MS Procedure Based on Fused-CoreTM Packing Material:
Application to Doping Control Analysis
Ilaria Fiacco1, Monica Mazzarino1, Xavier de la Torre1, Francesco Botrè1, David
Cowan2, Nicola Gray2
1
Laboratorio Antidoping, Federazione Medico Sportiva Italiana, Rome, Italy;
2
Drug Control Centre, King’s College London, London, United Kingdom
P4 Stability and Life Time of Slurry Packed Capillary Columns
Martin Franc1, Pavel Coufal1, Zuzana Bosáková1, Eva Tesařová2
1
Charles University in Prague, Faculty of Science, Department of Analytical
Chemistry, Prague; 2Charles University in Prague, Faculty of Science,
Department of Physical and Macromolecular Chemistry, Prague, Czech Republic
P5 Enantioseparation Power of Derivatized Cyclofructan Based CSP
Květa Kalíková1, Eva Tesařová1, Daniel W. Armstrong2
1
Department of Physical and Macromolecular Chemistry, Faculty of Science,
Charles University in Prague, Czech Republic; 2Department of Chemistry and
Biochemistry, University of Texas at Arlington, Arlington, USA
19P6 Utilization of Specific Properties of Supercritical Water in Analytical
Chemistry
Pavel Karásek, Josef Planeta, Michal Roth, Barbora Hohnová, Lenka Šťavíková
Institute of Analytical Chemistry, Brno, Czech Republic
P7 Continuous Reaction on Proline Functionalized Silica Stationary Phase under
Flow Conditions and High Pressure: the Case of Slow and Fast Aldolic
Reactions
Alberto Cavazzini, Alessandro Massi, Luisa Pasti and Francesco Dondi
University of Ferrara, Chemstry Department, Ferrara, Italy
P8 New Monolithic Capillary Columns for Green Chemistry Applications
Anna Kubíčková1, Adéla Svobodová1, Pavel Coufal1, Eva Tesařová2
1
Charles University in Prague, Faculty of Science, Department of Analytical
Chemistry; 2Charles University in Prague, Faculty of Science, Department of
Physical and Macromolecular Chemistry, Prague, Czech Republic
P9 Comparison of Particulate and Monolithic Stationary Phases in HPLC
Analysis of Salicylic Acid and Methylsalicylate in Paste Formulation
Ludmila Matysová1, Lucie Havlíková1, Veronika Šestakova1, Dalibor Šatínský1,
Renata Hájková1, Petr Solich1
1
Charles University in Prague, Faculty of Pharmacy, Department of Analytical
Chemistry, Hradec Králové, Czech Republic
P10 Use of Modern Analytical SPDE and TDAS Methods for the Analysis of
Sulphur Flavors in Beer
Renata Mikulíková1, Zdeněk Svoboda1, Sylvie Běláková1, Karolína Benešová1
1
Research Institute of Brewing and Malting, Malting Institute Brno, Brno, Czech
Republic
P11 Chiral Ligand-Exchange Separation and Resolution of Extremely Rigid
Glutamate Analogs: 1-Aminospiro[2.2]Pentyl-1,4-Dicarboxylic Acids
Benedetto Natalini, Roccaldo Sardella, N. Giacchè, F. Ianni, Emidio Camaioni,
Antonio Macchiarulo, Maura Marinozzi, Roberto Pellicciari
Dipartimento di Chimica e Tecnologia del Farmaco, Perugia, Italy
P12 Analysis of “Czech” beer phenolics by LC-MS
Kateřina Pařilová1, Ivana Márová1, Kateřina Duroňová1, Radana Měřínská1, Pavla
Benešová Pavla1
1
Brno University of Technology, Faculty of Chemistry, Brno, Czech Republic
P13 Preparation of Sulfaguanidine-Imprinted Polymers for the Selective
Extraction from Waters
Dragana Mutavdžić Pavlović1, Sara Livazović2, Ivan Brnardić3, Sandra Babić1,
Marija Kaštelan-Macan1
1
Department of Analytical Chemistry; 2BSc student; 3Department of Physical
Chemistry, Faculty of Chemical Engineering and Technology, University of
Zagreb, Zagreb, Croatia
20P14 Preparation and Application of Capillary Silica-Monolithic Columns
Josef Planeta, Dana Moravcová, Michal Roth, Pavel Karásek
Institute of Analytical Chemistry of the ASCR, Brno, Czech Republic
P15 Achievement of Separation for Steroids Including Geometrical Isomers
Using Carbazole-based Polymeric Organic Phase
Kaori Shingo, Abul K. Mallik, Tsuyoshi Sawada, Makoto Takafuji, and Hirotaka
Ihara
Department of Applied Chemistry and Biochemistry, Kumamoto University, Japan
P16 Optimization of Separation Conditions for Polar Compounds in HILIC
Veronika Škeriková1 and Pavel Jandera1
1
Department of Analytical Chemistry, Faculty of Chemical-Technology, University
of Pardubice, Czech Republic
P17 Optimization of Modern Analytical SPME and SPDE Methods for
Determination of trans-2-Nonenal in Barley, Malt and Beer
Zdeněk Svoboda1, Renata Mikulíková1, Sylvie Běláková1, Karolína Benešová1
1
Research Institute of Brewing and Malting, Malting Institute Brno, Brno, Czech
Republic
P18 CLC and CEC on Poly(styrene-divinylbenzene-methacrylic acid) Monolith as
a Stationary Phase
Adéla Svobodová1, Tomáš Křížek1, Pavel Coufal1, Jana Sobotníková1, Eva
Tesařová2
1
Charles University in Prague, Faculty of Science, Department of Analytical
Chemistry; 2Charles University in Prague, Faculty of Science, Department of
Physical and Macromolecular Chemistry, Prague, Czech Republic
P19 Comparative Study on the Separation of Structural and Geometrical Isomers
of Carotenoids on C18 and C30 Stationary Phases
Erika Turcsi1, József Deli1
1
University of Pécs, Medical School, Department of Biochemistry and Medicinal
Chemistry, Pécs, Hungary
P20 Simultaneous Determination of Various Isothiocyanates by HPLC following
Precolumn Derivation with Mercaptoethanol
Eli A. Wilson1, Saïd Ennahar1, Minjie Zhao1, Martine Bergaentzle1, Eric
Marchioni1, Françoise Bindler1
1
Laboratoire de Chimie Analytique et Sciences de l'Aliment, IPHC-LC4, UMR
7178, Faculté de Pharmacie, Illkirch, France
P21 Biogenic Amines in Traditional Sheep Cheeses: Assessment, Validation and
Application of a RP-HPLC-DAD Method
Claudia Zazzu1, Margherita Addis2, Maria Francesca Scintu2, Giovanni Piredda2,
Gavino Sanna1
1
Università degli Studi di Sassari, Dipartimento di Chimica, Sassari, Italy;
2
AGRIS Sardegna, Dipartimento per la Ricerca nelle Produzioni Animali, Olmedo
(SS), Italy
21P22 Monitoring of Fat Removal Capacity of Some Wastewater Plants Using
GCxGC-MS
Mihail Simion Beldean-Galea1, Jerôme Vial2, Didier Thiébaut2, Alexia Surchamp2,
Virginia Coman3
1
Faculty of Environmental Science, Babeş-Bolyai University, Cluj-Napoca,
Romania; 2LSABM, UMR-CNRS PECSA 7195, École Supérieure de Physique et de
Chimie Industrielles, ParisTech, Paris, France; 3Raluca Ripan Institute for
Research in Chemistry, Babeş-Bolyai University, Cluj-Napoca, Romania
P23 Capillary Electrophoresis Coupled with Mass Spectrometry for the
Evaluation of Substance P Enzymatic Degradation by Osteoblasts
Antonella Cavazza1,Claudio Corradini1, Mario Marini2, Luigi G. Roda2, Angela
Valenti3
1
Università degli Studi di Parma, Dipartimento di Chimica Generale ed
Inorganica, Chimica Analitica, Chimica Fisica, Parma, Italy; 2Università degli
Studi di Roma “Tor Vergata”, Dipartimento di Neuroscienze, Roma Italy;
3
Università degli Studi di Roma “Tor Vergata”, Dipartimento di Chirurgia 1,
Roma, Italy.
P24 Stable isotope dimethyl labeling coupled with multidimesional liquid
chromatography techniques for phosphopeptides identification in rat
cardiomyocytes
Eleonora Corradini1, Albert J.R. Heck2, Christian Priesinger2, Arjen Scholten2,
Aldo Laganà1
1
Department of Chemistry, La Sapienza University of Rome, Italy, 2 Biomolecular
Mass Spectrometry & Proteomics Group, Utrecht University, Netherlands
P25 Combination of Chemical and Electron-Impact Ionisation with GC×GC–qMS
for Characterization of Fatty Alcohol Alkoxylate Polymers in the Low-
Molecular-Weight Range up to 700 Da
Roman Dück1, Volker Wulf1, Margit Geißler2, Hans-Ulrich Baier2, Michaela
Wirtz3, Hans-Willi Kling3, Siegmar Gäb1 and Oliver J. Schmitz1
1
Department of Analytical Chemistry, University of Wuppertal; 2Shimadzu Europa
GmbH, Duisburg; 3Cognis GmbH, Düsseldorf, Germany
P26 Comprehensive Two-Dimensional Chromatography (LCxLC and GCxGC) of
Extracts from Matcha tea and Radix Angelicae sinensis
Roman Dück1, Alexandra von Trotha1, Margit Geißler2, Hans-Ulrich Baier2 and
Oliver J. Schmitz1
1
Department of Analytical Chemistry, University of Wuppertal; 2Shimadzu Europa
GmbH, Duisburg, Germany
P27 Development and Validation of a Multiresidual Method for Analysis of Major
Mycotoxins in Cereal Samples by Liquid Chromatography/Photoionization -
Tandem Mass Spectrometry
Eleonora Corradini, Patrizia Foglia, Riccardo Gubbiotti, Claudia Roccia, Roberto
Samperi, Aldo Laganà
Department of Chemistry, Sapienza University of Rome, Italy
22P28 Determination of Brominated Flame Retardants in Environmental Water by
Liquid Chromatography-Negative Ion Atmospheric Pressure
Photoionization-Tandem Mass Spectrometry
Piero Giansanti, Alessandro Bacaloni, Eleonora Corradini, Patrizia Foglia,
Riccardo Gubbiotti, Aldo Laganà
Department of Chemistry, Sapienza University of Rome, Italy
P29 Comprehensive Two-dimensional Liquid Chromatography: Comparison of
Different Second Dimension Gradients
Tomáš Hájek, Petr Česla, Pavel Jandera
Department of Analytical Chemistry, Faculty of Chemical Technology, University
of Pardubice, Pardubice, Czech Republic
P30 Determinatioon of Geographical Origin of Acacia Honeys Based on SPME-
GCxGC-TOF-MS Analysis
Ivan Špánik, Antónia Janáčová
Institute of Analytical Chemistry, Slovak University of Technology, Slovakia
P31 Gas Chromatographic Analyses For Second Generation Fuels
Katja Wilke and Matthias Otto
TU Bergakademie Freiberg, Institute of Analytical Chemestry, Germany
P32 Solvent Excess Adsorption on Stationary Phases with Cholesterol Derivatives
Szymon Bocian1, Urszula Balcerek1, Maria Matyska2, Joseph Pessek2, Bogusław
Buszewski1
1
Department of Environmental Chemistry & Bioanalytics, Faculty of Chemistry,
Nicolaus Copernicus University,Torun, Polan; 2Department of Chemistry, San
Jose State University, San Jose, USA
P33 A Theoretical Approach to Retention on Chemically Bonded Phases
Małgorzata Borówko, Wojciech Rżysko, Stefan Sokołowski, Tomasz Staszewski
Maria Curie - Skłodowska University, Department for the Modelling of Physico-
Chemical Processes, Lublin, Poland
P34 From Ion-Pair Chromatography to Chaotropic Chromatography: a
Theoretical Framework towards a Unified Salt Chromatography
Teresa Cecchi1 , Paolo Passamonti2
1
ITIS Montani, Fermo, Italy; 2UNICAM, Camerino (MC), Italy
P35 Comparison of Retention on Various Stationary Phases and Thermodynamic
Parameters of Retention on RTX-200MS GC Column for Isobutylesters of
Perfluorinated Carboxylic Acids
Veronika Dufková, Radomír Čabala
Department of Analytical Chemistry, Faculty of Science, Charles University in
Prague, Czech Republic
23P36 Simultaneous Analytical Separation of Metal-chelate Complexes, Ligands and
Inorganic Anions Using High Performance Ion Chromatography
Renata Tofalvi1, Peter Hajos1, Krisztian Horvath1, Rosa M. De Carlo2, Corrado
Sarzanini2
1
Department of Analytical Chemistry, University of Pannonia, Veszprem,
Hungary; 2Department of Analytical Chemistry, University of Turin, Italy
P37 Study of Interaction Mechanisms on Zirconia-based Columns
Lucie Janečková1, Eva Tesařová2, Zuzana Bosáková1
1
Department of Analytical Chemistry; 2Department of Physical and
Macromolecular Chemistry, Faculty of Science, Charles University in Prague,
Czech Republic
P38 Totally Porous or Superficially Porous Stationary Phase? Comparison of the
Mass Transfer Kinetics
Ibolya Kiss and Attila Felinger
Department of Analytical and Environmental Chemistry, University of Pécs,
Hungary
P39 Characterization of Stationary Phases for Reversed-Phase Chromatography
Martina Molíková, Pavel Jandera
Department of Analytical Chemistry, Faculty of Chemical Technology, University
of Pardubice, Czech Republic
P40 Estimation of Dividing Ability of Carbon Sorbents by Chromatographic and
Mass Spectrometer Methods
Galina A. Petukhova, Elena S. Kuznetsova, Aleksey K. Buryak
A.N. Frumkin Institute of Physical Chemistry and Electrochemistry, Russian
Academy of Sciences, Leninsky pr. 31, 119991 Moscow, Russia
Aula Marconi
17.10 – 18.30 Meeting of the IUPAC Group
24Wednesday, September 8
Aula Convegni
PLENARY SESSION III
Chairpersons Günther Bonn, Boguslaw Buszewski
8.40 – 9.10 The Power of Selectivity in Chromatography: Principles and Challenger
KL10 Wolfgang Lindner
Institute of Analytical Chemistry, University of Vienna, Austria
9.10 – 9.40 Progress in Atmospheric Pressure Ionization for Mass Spectrometry
KL11 Hyphenated with Liquid-phase Separation Techniques
Walter Eberherr1, Christian Klampfl1, Susanne Beismann1, Wolfgang
Buchberger1, Robert Hertsens2
1
Institute of Analytical Chemistry, Johannes-Kepler-University, Linz, Austria;
2
JEOL Europe, Zaventem, Belgium
9.40 – 10.10 “Green Chemistry“: The Resurgence of Analytical SFC ?
KL12 Heinz Engelhardt
Instrumental Analysis, University of Saarland, Saarbrücken, Germany
25Wednesday, September 8
Aula Convegni
POSTER FROM PODIUM SESSION A
Chairpersons Edouard S. P. Bouvier, Nikola Šegudović
10.20 – 10.28 Optimization of Off-line and Heartcutting On-line LC-MEKC Separation
PP1 Employing Sweeping Preconcentration Step
Petr Česla, Jan Fischer, Pavel Jandera
1
University of Pardubice, Faculty of Chemical Technology, Department of
Analytical Chemistry, Pardubice, Czech Republic
10.28 – 10.36 Improvement of Sensitivity in Identification of Proteins by Capillary
PP2 Electrophoresis-Electrospray Mass Spectrometry
Věra Hezinová 1, 2, Carolina Simó 3, Alejandro Cifuentes 3, Karel Klepárník 1,
František1Foret
1
Institute of Analytical Chemistry of the ASCR, Brno, Czech Republic; 2Brno
University of Technology, Faculty of Chemistry, Brno, Czech Republic; 3Institute
of Industrial Fermentation, Madrid, Spain
10.36 – 10.44 Paleo-Proteomics: Hunting for the Haemolymph Proteome of Limulus
PP3 polyphemus
Alfonsina D’Amato1, Angelo Cereda1, Angela Bachi2, James C. Pierce3, Pier
Giorgio Righetti1
1
Department of Chemistry, Materials and Chemical Engineering “Giulio Natta”,
Politecnico di Milano; 2San Raffaele Scientific Institute, Milano, Italy; 3Department
of Bioinformatics and Computer Science; University of the Sciences in
Philadelphia,USA
10.44 – 10.52 Enantioseparation Systems with Mixtures of Chiral Selectors
PP4 Pavel Dubský, Jana Svobodová, Eva Tesařová, Bohuslav Gaš
Department of Physical and Macromolecular Chemistry, Faculty of Science,
Charles University in Prague, Czech Republic
11.00 – 11.30 COFFEE BREAK & EXHIBITION
26Wednesday, September 8
Aula Marconi
POSTER FROM PODIUM SESSION B
Chairpersons Cristina Giovannoli, Modest Gertsiuk
10.20 – 10.28 Comparing the Biphasic and Triphasic Systems in The Solvent Extraction of
PP5 Olive Mill Wastewater Polyphenols: a HPLC Study.
Jihane Fathi, M. Mimouni
Laboratoire Chimie Matériaux, Faculté des Sciences d’Oujda, Oujda, Maro
10.28 – 10.36 Rapid Method for the Determination of Amino Acids in Milk by High
PP6 Performance Liquid Chromatography with Pre-column Derivatization and
Fluorescence Detection
Rosaria Marino1, Marco Iammarino2, Marilena Muscarella2, Antonella Santillo1,
Mariangela Caroprese1, and Marzia Albenzio1
1
Department of Production and Innovation in Mediterranean Agriculture and
Food System (PrIME) University of Foggia, Foggia, Italy; 2Chemistry
Department, Istituto Zooprofilattico Sperimentale della Puglia e della Basilicata,
Foggia, Italy
10.36 – 10.44 Development of a Fast GC Method for the Separation of Non-Polar, Semi-
PP7 Polar and Polar Volatile Organic Compounds
Dorelia Lipsa, Carmen del Cacho, Paolo Leva, Josefa Mª Barrero-Moreno
European Commission, Joint Research Center, Institute for Health and
Consumer Protection, Chemical Assessment and Testing Unit, Ispra (VA), Italy
10.44 – 10.52 Continuous Online Rapid SEC Monitoring of Polymerizations
PP8 Chheng Ngov, Christophe A. Serra
Laboratoire d’Ingénierie des Polymères pour les Hautes Technologies (LIPHT) –
EAc(CNRS) 4379, Ecole Européenne de Chimie, Polymères et Matériaux
(ECPM), Université de Strasbourg (UdS), Strasbourg, France
11.00 – 11.30 COFFEE BREAK & EXHIBITION
27Wednesday, September 8
Aula Convegni
PLENARY SESSION IV
Chairpersons Lois Beaver, Luigi Mondello
11.30 – 12.00 The Proteome Buccaneers: How To Unearth Your Treasure Chest Via
KL13 Combinatorial Peptide Ligand Libraries
Pier Giorgio Righetti1 and Egisto Boschetti2
1
Politecnico di Milano, Department of Chemistry, Materials and Chemical
Engineering "Giulio Natta", Milano, Italy; 2 Bio-Rad Laboratories, Hercules,
USA
12.00 – 12.30 Top-down HPLC-ESI-MS Strategies for the Proteomic Investigation of
KL14 Human Saliva
Massimo Castagnola1, Rosanna Inzitari1, Chiara Fanali1, Federica Iavarone1,
Tiziana Cabras2, Irene Messana2
1
Istituto di Biochimica e Biochimica Clinica, Facoltà Di Medicina, Università
Cattolica, Roma; 2Dipartimento di Scienze Applicate ai Biosistemi, Università di
Cagliari, Italy
12.30 – 14.00 LUNCH & EXHIBITION
28Wednesday, September 8
Aula Convegni
PLENARY SESSION V – IN MEMORIAM CSABA HORVÁTH
Chairpersons Heinz Hengelhardt, Wofgang Lindner
14.00 – 14.25 Introduction
14.25 – 14.50 Novel Monolithic Stationary Phases in Separation Science
HML1 Günther K. Bonn
Institute of Analytical Chemistry and Radiochemistry, Leopold-Franzens
University, Innsbruck, Austria
14.50 – 15.15 Quality by Design: Monitoring Design Space in Selectivity Exploration of
HML2 HPLC Separations
Imre Molnár*, Hans-Jürgen Rieger
Molnár-Institute for Applied Chromatography, Berlin, Germany
15.15 – 15.40 Rapid Separations of Biomolecule Aggregates by UPLC-SEC
HML3 Edouard S. P. Bouvier, Susan Serpa, Nadya Brady, Kevin D. Wyndham, Nicole
L. Lawrence, Paula Hong, Uwe D. Neue, Tom H. Walter
Waters Corporation, Chemistry Operations R&D, Milford, MA,USA
15.40 – 16.05 High-Throughput Chromatographic Methods for Monoclonal Antibody
HML4 Process Development and Quality Control
Dell Farnan, Tony G. Moreno, Rahul Parikh, Yun Lou, Lisa Vampola and
Jennifer Rea
Protein Analytical Chemistry, Genentech, A Member of the Roche Group, South
San Francisco, CA, U.S.A
16.05 – 16.30 Interactions of Analytes with other Solubilized or Dispersed Species in
HML5 Solution and their Role in Liquid Phase Separation Systems
Danilo Corradini, Antonella De Rossi, Isabella Nicoletti
Institute of Chemical Methodologies, Italian National Council of Research, Area
della Ricerca di Roma I, Monterotondo Scalo (Rome) Italy
16.30 – 17.00 COFFEE BREAK & EXHIBITION
17.00 – 18.30 POSTER SESSION II & EXHIBITION
29Wednesday, September 8
POSTER SESSION II P41 – P80
Chairperson: Maria Concetta Bruzzoniti
17.00 – 18.30
Fundamentals II
Capillary electromigration techniques
Sample preparation
Proteomics, metabolomics, and biomarker discovery
Enantioseparations
P41 Partition Coefficients of Organics in Ionic Liquid–Carbon Dioxide Systems
from Supercritical Fluid Chromatography
Josef Planeta, Pavel Karásek, Lenka Šťavíková, Barbora Hohnová, Michal Roth
Institute of Analytical Chemistry of the ASCR, Brno, Czech Republic
P42 Improvements in Multichromatographic Systems Operating in Isotherm
Mario Vincenzo Russo1, Ivan Notardonato1, Enrico Veschetti2
1
Università degli Studi del Molise, Facoltà di Agraria (DISTAAM), Campobasso,
Italy; 2Isituto Superiore di Sanità, Dipartimento Ambiente e connessa Prevenzione
Primaria, Roma, Italy
P43 Temperature Effects in Chromatography with Chemically Bonded Phases
Małgorzata Borówko, Wojciech Rżysko, Stefan Sokołowski, Tomasz Staszewski
Maria Curie- Skłodowska University, Department for the Modelling of Physico-
Chemical Processes, Lublin, Poland
P44 Density Functional Approach to the Description of Microscopic Structure of
Chemically Bonded Phases
Małgorzata Borówko, Wojciech Rżysko, Stefan Sokołowski, Tomasz Staszewski
Maria Curie-Skłodowska University, Department for the Modelling of Physico-
Chemical Processes, Faculty of Chemistry, Lublin, Poland
P45 Adsorption Equilibria of Proline in Hydrophilic Interaction Chromatography
Péter Vajda1, Alberto Cavazzini2, Attila Felinger1
1
Department of Analytical and Environmental Chemistry, University of Pécs,
Hungary; 2Department of Chemistry, University of Ferrara, Italy
P46 Analysis of Free Amino Acids in Honey by Capillary Zone Electrophoresis
Jan Fischer, Václav Staněk, Hana Weiserová
Department of Analytical Chemistry, Faculty of Chemical Technology, University
of Pardubice, Pardubice, Czech Republic
30P47 Optimization of Chiral Electrokinetic Chromatographic Methods Using Dual
Cyclodextrin Selector Systems
Robert Ivanyi1, Erzsebet Varga1, Zoltan Juvancz2, Gerhardt K.E. Scriba3
1
CycloLab Ltd., Budapest, Hungary,2Universitas Budensis, Budapest, Hungary,
3
Friedrich-Schiller University of Jena, School of Pharmacy, Department of
Pharmaceutical Chemistry, Jena, Germany
P48 Differences in Surface Characteristic of Biofilm-Positive and Biofilm-
Negative Candida parapsilosis Strains
Anna Kubesová1, 2, Marie Horká1, Filip Růžička3,Veronika Holá3
1
Institute of Analytical Chemistry of the ASCR, Brno, Czech Republic,
2
Department of Biochemistry, Faculty of Science, Masaryk University, Brno,
Czech Republic, 3Department of Microbiology, Faculty of Medicine, Masaryk
University, Brno, Czech Republic
P49 An Approach for the Separation of Microorganisms by Capillary
Electrophoresis
Cinzia Passini, Cristina Giovannoli, Patrizia Baravalle, Laura Anfossi, Claudio
Baggiani
Laboratory of Bioanalytical Chemistry, Department of Analytical Chemistry,
University of Turin, Turin, Italy
P50 System Peaks in Capillary Zone Electrophoresis: PeakMaster 6.0
Martina Riesová, Vlastimil Hruška, Bohuslav Gaš
Charles University in Prague, Faculty of Science, Department of Physical and
Macromolecular Chemistry, Prague, Czech Republic
P51 Easy Silica Capillary Coatings and EOF Modulation for Analysis of
Chemicals, Drugs and Biological Molecules in CE and CE-MS
Roberto Sebastiano1, Pier Giorgio Righetti1, Attilio Citterio1, Martha E. Mendieta1,
Radim Knob2 and Jonas Bergquist3
1
Polytechnic of Milan, Department of Chemistry, Materials and Chemical
Engineering “Giulio Natta" Milano, Italy, 2Department of Analytical Chemistry,
Faculty of Science, Palack´y University in Olomouc, Czech Republic, 3Department
of Physical and Analytical Chemistry, Uppsala University, Sweden
P52 Capillary Electrophoretic Determination and Characterization of Negatively
Charged Cyclodextrin Derivatives Using Mass Spectrometric Detection and
Application for Peptides Enantioseparation by CE
Bunleu Sungthong1, Róbert Iványi2, Svenja-Catharina Bunz3, Christian Neusüß3,
Gerhard K. E. Scriba1
1
School of Pharmacy, University of Jena, Germany, 2Cyclolab R&D, Budapest,
Hungary, 3Faculty of Chemistry, Aalen University, Germany
P53 Determination of GB and GD in Micropig Whole Blood
Mei Yee Cheh, T. H. Yeo, W. K. Loke
DSO National Laboratories, Singapore
31P54 Purification of Proanthocyanidins from Chocolate Using Solid-Phase
Extraction
Vesna Glavnik1, Breda Simonovska1, Irena Vovk1
1
Laboratory for Food Chemistry, National Institute of Chemistry, Ljubljana,
Slovenia
P55 The Comparison of Various Sample Treatment Methods for Determination of
Volatile Organic Compounds Presented in Slovakian Plum Brandy.
Antónia Janáčová1, Hana Vasarábová1, Solomyia Pysarevska1,2 Ivan Špánik1
1
Institute of Analytical Chemistry, Slovak University of Technology, Slovakia;
2
Department of Analytical Chemistry, Ivan Franko National University, Lviv,
Ukraine
P56 Highly Selective Sorbents for the Determination of Estrogens
David Matějíček1, Jan Přibyl 2
1
Department of Chemistry and Biochemistry, Mendel University in Brno,
Zemedelska 1, Czech Republic; 2National Center for Biomolecular Research,
Masaryk University, Brno, Czech Republic
P57 Polycyclic Aromatic Hydrocarbons & Fatty Fish Safety: Application of
Microwave-assisted Extraction and Liquid Chromatography With
Fluorescence Detection
Maria J. Ramalhosa1,2, Paula Paíga1, Simone Morais1, Cristina Delerue-Matos1 and
Maria B. P.P. Oliveira2
1
Requimte, Instituto Superior de Engenharia do Porto, Porto, Portugal;2Requimte,
Serviço de Bromatologia, Faculdade de Farmácia, Universidade do Porto, Porto,
Portugal
P58 An Influence of Chemical SPME Fibers Modification for Extraction Abilities
of Medically Important Drugs
P. Olszowy1, M. Szultka1, J. Nowaczyk2, T. Ligor1, B. Buszewski1
1
Department of Environmental Chemistry and Bioanalytics, Faculty of Chemistry,
Nicolaus Copernicus University, Torun, Poland, 2Chair of Physical Chemistry and
Physicochemistry of Polymers, Department of Chemistry, Nicolaus Copernicus
University, Torun, Poland
P59 Optimization Study of SPE-HPLC Pharmaceuticals Determination from
Water Samples
Dragana Mutavdžić Pavlović1, Danijela Ašperger1, Dijana Tolić2, Sandra Babić1,
Marija Kaštelan-Macan1
1
Department of Analytical Chemistry, 2BSc student, Faculty of Chemical
Engineering and Technology, University of Zagreb, Zagreb, Croatia
P60 Liquid Phase Microextraction for High Sample Preconcentration and
Determination of Steroids in Surface Waters
Dalibor Satinsky, Karolina Skraskova, Lucie Novakova
Department of Analytical Chemistry, Faculty of Pharmacy, Charles University,
Hradec Kralove, Czech Republic
32P61 Comparison of Different Caps Used for Gaseous Sample Preparation
Agnieszka Ulanowska1, Tomasz Ligor1, Anton Amann2, Bogusław Buszewski1
1
Chair of Environmental Chemistry and Bioanalytics, Faculty of Chemistry,
Nicolaus Copernicus University, Toruń, Poland, 2Department of Anesthesiology
and Critical Care Medicine, Medical University of Innsbruck, Innsbruck, Austria
P62 Approaching the Complexity of Escherichia Coli Proteome Using Off-Gel
IEF/nLC-MS/MS and TPP Data Analysis
Ruedi Aebersold1-4, Luciano Callipo5, Aldo Laganà5, Alex Schmidt6
1
Institute of Molecular Systems Biology, The Swiss Federal Institute of Technology
(ETH Zurich), Zurich, Switzerland; 2Institute for Systems Biology, Seattle,
Washington, US; 3Faculty of Science, University of Zurich, Zurich, Switzerland;
4
Center for Systems Physiology and Metabolic Diseases, Zurich, Switzerland;
5
Department of Chemistry, Sapienza University of Rome, Rome, Italy; 6Proteomics
Core Facility Biozentrum, University of Basel, Basel, Switzerland
P63 Analysis of Plasma Proteins Adsorption onto DC-Chol–DOPE Cationic
Liposomes by HPLC-Chip Coupled to a QTOF Mass Spectrometer
Chiara Cavaliere, Giulio Caracciolo, Giuseppe Caruso, Daniela Pozzi, Roberto
Samperi, Aldo Laganà
Department of Chemistry, Sapienza University of Rome, Italy
P64 Les Maîtres de l’Orge: How to Nail Down the Beer Proteome Via
Combinatorial Peptide Ligand Libraries
Elisa Fasoli and Pier Giorgio Righetti
Politecnico di Milano, Department of Chemistry, Materials and Chemical
Engineering "Giulio Natta", Milan, Italy
P65 Differential Plasma Protein Binding onto Lipsomes and Liploplexes by SDS-
PAGE
Anna Laura Capriotti, Giulio Caracciolo, Riccardo Gubbiotti, Daniela Pozzi,
Claudia Roccia, Aldo Laganà
Department of Chemistry, Sapienza University of Rome ,Italy
P66 Capillary Electrophoretical Method for Plant Metabolomics: Rapid
Separation of Co-enzymes
Tomáš Křížek1, Pavel Coufal1, Zuzana Bosáková1, Jana Sobotníková1
1
Charles University in Prague, Faculty of Science, Department of Analytical
Chemistry, Prague, Czech Republic
P67 Purification and Investigation of Kinetic Properties of Dimethylarginine
Dimethylaminohydrolase Enzyme From Rat Kidney
Emel Caglar Yildiz1, Ismail Kurt1, M. Kemal Erbil1
1
Dept of Medicinal Biochemistry, Gulhane School of Medicine, Ankara, Turkey
P68 Comparative Efficiency of High Pressure Liquid Chromatography, Capillary
Zone Electrophoresis And Microcolumn Chromatography Techniques For
Quantification of HbA2 in The Screening of Beta-Thalassaemia
Ismail Kurt1, Emel Caglar Yıldız1, Adnan Hasimi2, M. Kemal Erbil1
1
Gulhane School of Medicine, Dept. of Medical Biochemistry, Ankara/TURKEY,
2
Deren Laboratories Group, Ankara, Turkey
33P69 High Sensitive and Easy-to-use High Throughput Method for LC-MS
Analysis of Aldehydes in Exhaled Breath Condensate
Marek Kuzma,1 Petr Kacer2, Kamila Syslova2, Věra Najmanova2, Zdena
Fenclova3, Jindriska Lebedova3, Daniela Pelclová3
1
Laboratory of Molecular Structure Characterization, Institute of Microbiology,
Prague; 2Department of Organic Technology, Institute of Chemical Technology,
Prague; 3Department of Occupational Medicine, 1st Medical Faculty, Charles
University, Prague, Czech Republic
P70 Glycoproteome Study of Barley Grain and Malt: Preliminary Insights
Markéta Laštovičková1, Dagmar Smětalová1,2 and Janette Bobáľová1
1
Institute of Analytical Chemistry, Academy of Sciences of the Czech Republic,
Brno; 2Brno University of Technology, Faculty of Chemistry, Brno, Czech
Republic
P71 Nano LC-MALDI/TOF/TOF Technology Applied to Differential Proteomic
Analysis of Murine Cardiac Tissues under Simulated Microgravity
Conditions.
Luciano Callipo1,Enrico Capobianco2, Lorenzo Citti3, , Silvia Rocchiccioli3,
Claudia Roccia1, Aldo Laganà1
1
Department of Chemistry, Sapienza University of Rome,Italy; 2CRS4
Bioinformatics Laboratory ,Polaris Science&Technology Park,Pula, Italy;
3
Clinical Physiology Institute-CNR, Pisa, Italy
P72 Immunomagnetic Probe for Detection of Biomarkers in Exhaled Breath
Condensate
Kamila Syslová1, Petr Kačer1, Marek Kuzma2, Štěpánka Vlčková3,Jindřiška
Lebedová3, Zdeňka Fenclová3 and Daniela Pelclová3
1
Department of Organic Technology, ICT-Prague, Prague; 2Laboratory of
Molecular Structure Characterization, Institute of Microbiology, Prague;
3
Department of Occupational Medicine, 1st Medical Faculty, Charles University,
Prague, Czech Republic
P73 Simultaneous Binding Assay of Microheterogenious Proteins by Capillary
Electrophoresis with Laser Induced Fluorescence Detection
Atsushi Taga1, Daiki Kanbayashi1, Nanae Umeda1, Shuji Kodama2, Atsushi Sato3,
Kentaro Suzuki3, Masakazu Izako3, and Reiko Sugiura1
1
School of Pharmaceutical Sciences, Kinki University, Osaka, Japan; 2Toyama
Institute of Health, Yoyama, Japan; 3GL Sciences inc., Hukushima, Japan
P74 The UPLC-PDA fingerprinting method for analysis of major extracellular
metabolites presented in fermentation broth of fungi of genus Geosmithia
Tereza Tylová1,2, Miroslav Kolařík1,3, Jana Olšovská1
1
Institute of Microbiology of the Academy of Sciences of the Czech Republic,
Prague 2; Czech Republic; 2Charles University, Faculty of Science, (Albertov 8),
Prague; 3Charles University, Faculty of Science, (Benátská 2), Prague, Czech
Republic
34P75 Unusual Application of Chirobiotic TAG Stationary Phase in Non-
Enantioselective Separations: a Case Study for the Quality/Purity Control of
Biotinylated Therapeutics
Elena Badaloni1, Walter Cabri1, Alessia Ciogli2, Ilaria D’Acquarica2, Roberto
Deias1, Francesco Gasparrini2, Fabrizio Giorgi1, Claudio Villani2
1
Analytical Development R&D Sigma-tau spa, Pomezia, Italy; 2Dipartimento di
Chimica e Tecnologie del Farmaco, Sapienza Università di Roma, Roma, Italy
P76 HPLC Enantioselective Analysis of Potential β-blocker Drugs and Kinetic
Study of In-vitro Decomposition in Serum
Katarína Hroboňová 1, Jozef Lehotay1, Ružena Čižmáriková2, Katarína Bruchatá2
1
Institute of Analytical Chemistry, Faculty of Chemical and Food Technology,
Slovak University of Technology; 2Department of Chemical Theory of Drugs,
Faculty of Pharmacy, Comenius University, Bratislava, Slovak Republic
P77 Enantioseparation of 1-Phenyl-1,2,3,4-tetrahydroisoquinoline on
Polysaccharide Based Chiral Stationary Phases
Helena Kažoka1, Oksana Rotkaja2, L. Varačeva1
1
Latvian Institute of Organic Synthesis; 2Latvian University, Rīga, Latvia
P78 An Overview of the Fabrication Methods & Applications of Carbon
Nanotube Membrane in Environmental Engineering
Seyed Ahmad Mirbagheri1, Amir Abedin Maghanaki2, Hamidreza Kamalan3,
Shima Hasheminasab4, Maryam Ouladi5
1
Civil Engineering Faculty, K. N. Toosi University of Technology, Tehran; 2Civil
Engineering Faculty, K. N. Toosi University of Technology, Tehran; 3Islamic Azad
University, Pardis Branch; 4Great Consulting Engineers, Tehran, 5Saipa
Industrial Group, Tehran, Iran
P79 Determination of UV Filters in Water Samples by SBSE-LD followed by
HPLC-DAD and Tandem Mass Spectrometry
Kieu T. N. Nguyen, Emanuele Magi, Carlo Scapolla, Marina Di Carro
University of Genoa, Department of Chemistry and Industrial Chemistry, Genova,
Italy
P80 Analysis of Metabolic Products of Fungi Growing in Air Conditioners by
HPLC-MS
Szabolcs B.Tóth1, Rita Jolankai2, József Szarvas1, Zoltán Murányi1
1
Eszterházy Károly College, Department of Chemistry,Eger,Hungary; 2University
of Pannonia, Georgikon Faculty of Agriculture, Keszthely, Hungary
Aula Marconi
17.30 – 18.30 Meeting of the CEGSS representatives
35Thursday, September 9
Aula Convegni
PARALLEL SESSION V
Chairpersons Francesco Dondi, Paola Dugo
8.30 – 9.00 Investigation of Some Natural Carbohydrates from Different Matrices by
KL15 Chromatographic Techniques
Virginia Coman1, Mihaela Vlassa1, Miuţa Filip1, Violeta Paşcalău1, Adela
Halmagyi2
1
Babeş-Bolyai University, Raluca Ripan Institute for Research in Chemistry;
2
Institute of Biological Researches, Cluj-Napoca, Romania
9.00 – 9.30 Evaluation of the Potential of Capillary Electrophoresis and Rewards of the
KL16 Coupling of CE and MS in Food Analysis
Claudio Corradini, Antonella Cavazza, Paola Salvadeo
Department of General and Inorganic Chemistry, Analytical Chemistry, Physical
Chemistry, University of Parma, Parma, Italy
9.30 – 9.50 Quantification of γ-Oryzanol in Crude Cereal Bran Oils and Commercial
L10 Products by a Rapid and Reliable NP-HPLC Method
Michele D’Ambrosio, Sandro Gadotti, Amedeo Luppi, Antonio Guerriero
Laboratorio di Chimica Bioorganica, Università degli Studi di Trento, Italy
9.50 – 10.10 Dionisus and Hera: Hunting for Traces of Proteinaceous Fining Agents in
L11 Wines
Alexander V. Kravchuk1, Angelo Cereda1, Alfonsina D’Amato2, Angela Bachi2,
Pier Giorgio Righetti
1
Department of Chemistry, Materials and Chemical Engineering “Giulio Natta”,
Politecnico di Milano; 2San Raffaele Scientific Institute, Milano, Italy
10.10 – 10.30 Rapid Procedures of Analysis of Triglycerides and Fatty Acids as Pentyl
L12 Esters and Phenethyl Esters in Alimentary Fats and Oils by High Resolution
Chromatographic Techniques
Daniele Naviglio, Veronica Fornaro, Antonello Santini
Department of Food Science, University of Naples Federico II, Portici (NA), Italy
10.30 – 11.00 COFFEE BREAK & EXHIBITION
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