XIDer - an X-ray Integrating Detector - for the ESRF-EBS Upgrade David Schimansky

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XIDer - an X-ray Integrating Detector - for the ESRF-EBS Upgrade David Schimansky
XIDer – an X-ray Integrating Detector
    for the ESRF-EBS Upgrade
             David Schimansky

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XIDer - an X-ray Integrating Detector - for the ESRF-EBS Upgrade David Schimansky
Contents

   • About me

   • The European Synchrotron Radiation Facility (ESRF) & its upgrade
      program (EBS)

   • XIDer: A New Multi-Purpose Detector for Time-Resolved X-Ray
      Experiments at the ESRF
         • Requirements & Chosen Concept
         • My Job: Readout ASIC

   • Conclusion & Outlook
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   03.04.19 - HighRR BiWeekly Seminar      David Schimansky             1
XIDer - an X-ray Integrating Detector - for the ESRF-EBS Upgrade David Schimansky
About me

                                        • PhD student in Prof. Fischer‘s group LSuS @ ZITI

                                        • Studies (2011 – 2017):
                                            • B. Sc. and M. Sc. in Physics @ University of Heidelberg

                                            • Focus on particle, medical and detector physics as well as ASIC design

                                        • Work @ KIP in Prof. Schultz-Coulon‘s group F11 (2015 – 2018):
                                            • Bachelor and master thesis on ASIC characterisation and design

                                        • Work @ ZITI in Prof. Fischer‘s group LSuS (2018 – tbd):
                                            • PhD Thesis (May 2018 - tbd)

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   03.04.19 - HighRR BiWeekly Seminar                      David Schimansky                                            2
XIDer - an X-ray Integrating Detector - for the ESRF-EBS Upgrade David Schimansky
European Synchrotron
Radiation Facility (ESRF)
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03.04.19 - HighRR BiWeekly Seminar   David Schimansky   3
XIDer - an X-ray Integrating Detector - for the ESRF-EBS Upgrade David Schimansky
European Synchrotron Radiation Facility (ESRF)

                                         • Joint research facility in Grenoble, France (founded in 1988)

                                         • Funded by 22 countries (France, Germany, Italy, ..)

                                         • Electron synchrotron x-ray source (up to ~150keV)

                                         • First 3rd generation synchrotron (opened in 1994)

                                         • Circumference: 844m

                                         • 2000 publications per year

                                         • Advertises itself as „user facility“

                                         • Research topics (among others):
                                              • X-ray spectroscopy
                                              • X-ray tomography
                                              • X-ray diffraction                                          !"#$%&'()*&+"#(,-
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    03.04.19 - HighRR BiWeekly Seminar                    David Schimansky                                 4
XIDer - an X-ray Integrating Detector - for the ESRF-EBS Upgrade David Schimansky
Research at the ESRF

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    03.04.19 - HighRR BiWeekly Seminar   David Schimansky   5
XIDer - an X-ray Integrating Detector - for the ESRF-EBS Upgrade David Schimansky
Research at the ESRF

                                                                         Other: Training,
                                                   Surfaces &            feasibility tests,
                                                   Interfaces              proprietary          Chemistry
                                                                            research              12%
                                                      10%
                                                                                4%                 Electronic &
                                                                                                    Magnetic
                                              Soft Condensed                                        Properties
                                                   Matter                                              12%
                                                    10%
                                                                                                        Crystals
                                            Methods &                                                  &Ordered
                                         Instrumentation
                                                                                                       Structures
                                               2%                                                         10%
                                                    Medicine                                          Disordered
                                                      4%                                                Systems
                                                                                                          4%
                                         Macromolecular                                         Applied
                                         Crystallography             Environment &             Materials,
                                              15%                        Culture              Engineering
                                                                           7%                    10%
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                                                              Beamtime used at the ESRF (2010 data)                 '(0 !,.'%$&,/(

    03.04.19 - HighRR BiWeekly Seminar     David Schimansky                                                       6
XIDer - an X-ray Integrating Detector - for the ESRF-EBS Upgrade David Schimansky
and the phonon-related lattice dynamics in thermo-                               zinc antimonide (Zn-Sb) binary systems with their intricate phase
terials. In the following, we will briefly review the most                        diagram [11e18], clathrates [19e24] and filled skutterudites
    Synchrotron light sources around the world
ancements obtained using different synchrotron radia-
ques.
                                                                                 [22,25e27] featuring guest-framework characteristics, Zintl com-
                                                                                 pounds possessing large unit cells [28e31], half-Heusler alloys with

                                                                                                                                                              > 50 sources worldwide

                                                                                                                                                                                        !"#$%&'()*&+"#(,-
        Taken from „The complexity of thermoelectric materials: why we need powerful and brilliant synchrotron radiation sources?“ (W. Xu, Y. Liu, A. Marcelli, P.P. Shang, W.S. Liu,    '(0 !,.'%$&,/(
. World in
         map of the Today
           Materials main synchrotron  radiation
                          Physics, Volume        facilities in all continents. At present, SR facilities are not present only in Africa. SR, synchrotron radiation.
                                          6, 2018)

                  03.04.19 - HighRR BiWeekly Seminar                                                        David Schimansky                                                            7
XIDer - an X-ray Integrating Detector - for the ESRF-EBS Upgrade David Schimansky
and the phonon-related lattice dynamics in thermo-                               zinc antimonide (Zn-Sb) binary systems with their intricate phase
terials. In the following, we will briefly review the most                        diagram [11e18], clathrates [19e24] and filled skutterudites
    Synchrotron light sources around the world
ancements obtained using different synchrotron radia-
ques.
                                                                                 [22,25e27] featuring guest-framework characteristics, Zintl com-
                                                                                 pounds possessing large unit cells [28e31], half-Heusler alloys with

                                                                                                                                                              > 50 sources worldwide

                                                                                                                                                              High energy sources (6-8 GeV e-
                                                                                                                                                              in storage rings)

                                                                                                                                                              World‘s first 4th generation
                                                                                                                                                              synchrotrons (@ 3 GeV)

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        Taken from „The complexity of thermoelectric materials: why we need powerful and brilliant synchrotron radiation sources?“ (W. Xu, Y. Liu, A. Marcelli, P.P. Shang, W.S. Liu,         '(0 !,.'%$&,/(
. World in
         map of the Today
           Materials main synchrotron  radiation
                          Physics, Volume        facilities in all continents. At present, SR facilities are not present only in Africa. SR, synchrotron radiation.
                                          6, 2018)

                  03.04.19 - HighRR BiWeekly Seminar                                                        David Schimansky                                                                 8
XIDer - an X-ray Integrating Detector - for the ESRF-EBS Upgrade David Schimansky
ESRF Upgrade Program (Road to Fourth Generation)

                                         • Extremely-Brilliant Source (ESRF-EBS):
                                            • Storage ring upgrade program over the period 2015-2022

                                            • Improve energy efficiency (30% cost reduction)

                                            • Increase brilliance of x-ray beam

                                         • Detector Development Program (DDP):
                                            • Reach out to external laboratories

                                            • Build new detectors tailored to the upgraded source

                                            • R&D Phase from 2017 to 2021

                                            • Engineering Phase from 2020 to 2024
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    03.04.19 - HighRR BiWeekly Seminar               David Schimansky                                  9
ESRF Upgrade Program (Road to Fourth Generation)

                                         • Extremely-Brilliant Source (ESRF-EBS):
                                            • Storage ring upgrade program over the period 2015-2022

                                            • Improve energy efficiency (30% cost reduction)

                                            • Increase brilliance of x-ray beam

                                         • Detector Development Program (DDP):
                                            • Reach out to external laboratories

                                            • Build new detectors tailored to the upgraded source

                                            • R&D Phase from 2017 to 2021

                                            • Engineering Phase from 2020 to 2024
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    03.04.19 - HighRR BiWeekly Seminar               David Schimansky                                  10
Why SuS?

 Experience with similar setup: DSSC (DePFET Sensor with Signal Compression) @ European XFEL
                                                15 mm                    Full processing chain in every pixel
 • Low noise x-ray detector

 • Specs:
     • 0.5-6 keV
                                                                                                                204 µm
     • Single photon sensitivity          4096 Pixels
     • Dynamic range of >104 ph

     • Burst data rates of
                                           IO and Control
        150Gbps/chip
                                                                                       236 µm
 • SuS‘s job: Integration of readout ASIC parts, ASIC control block, ASIC readout, in-pixel RAM, ...

 • Fully assembled detector: 1MPix, 32 sensors, 256 ASICs                                                 !"#$%&'()*&+"#(,-
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     03.04.19 - HighRR BiWeekly Seminar          David Schimansky                                        11
XIDer: X-ray Integrating
Detector
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Project Outline

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                                                   XIDer:
    • 4-year funding: Shared 50/50 by ESRF and University of Heidelberg
                     • Two PhD students and half a postdoc in Heidelberg
                                     • One PhD student and staff @ ESRF
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    03.04.19 - HighRR BiWeekly Seminar              David Schimansky                       13
Detector Requirements

   Build detector for any kind of (time-resolved) x-ray diffraction experiment at the ESRF:

   • Energy range: 10-100keV

   • Different spatial resolutions: 100µm vs. 200µm pixel pitch (clusterable pixels)

                                                        %&
   • Dynamic range: Single Photons up to > 10$$
                                                       ''( )

   • Cope with different bunch filling modes for storage ring

   • Time-resolved ( >100k frames/s)

   • Flexible readout schemes (single frame, accumulated frames ..)

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   03.04.19 - HighRR BiWeekly Seminar       David Schimansky                                  14
Detector Requirements: Bunch modes

              Electron bunches
                                                                            Detector

                                                                   Signal
                                        Storage ring

                                                                                          t
                                                                              One orbit

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   03.04.19 - HighRR BiWeekly Seminar                  David Schimansky                       15
Detector Requirements: Bunch modes

              Electron bunches
                                                                            Detector

                                                                   Signal
                                        Storage ring

                                                                                          t
                                                                              One orbit

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   03.04.19 - HighRR BiWeekly Seminar                  David Schimansky                       16
Detector Requirements: Bunch modes/ Photon Fluxes
                                         Example cases of possible bunch modes

                                                                                              7/8 + 1 Bunch Mode
                       16 Bunch Mode
                     16 bunch mode                                                           7/8 +1 bunch mode
                                                                               868 bunches         1 bunch

        175 ns                                                                   2.45 μs        175 ns 175 ns
    1                                             16

                         One orbit
                             2.8 μs (2.8µs)                                            2.8 μs
                                                                                  One orbit  (2.8µs)

 • Pulsed illumination for time-resolved experiments                   • Quasi-continuous illumination for 7/8 of the orbital period

 • Single bunches have to be recorded and processed                    • Integrate many bunches into one image
                                                                                                  %&
 • Need single photon sensitivity                                      • Expected > 10$$
                                                                                                 ''()

                                                 Big dynamic range
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    03.04.19 - HighRR BiWeekly Seminar                      David Schimansky                                                 17
Detector Requirements: Frame Rates

                  See „Real-time direct and diffraction X-ray imaging of irregular silicon wafer breakage“
                  (A. Rack, M. Scheel, A. N. Danilewsky in IUCrJ, Volume 3, 2016)

    • Preliminary goal: >100k frames per second (e.g. Si fracture observed @ ~35kHz)

    • Main challenge: Data rates
          • Example: 900k pixels, 8 bit per pixel, 100kHz frame-rate ⇒ 90GB/s                                 !"#$%&'()*&+"#(,-
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    03.04.19 - HighRR BiWeekly Seminar                                  David Schimansky                     18
Preliminary Detector Concept

                                         2D hybrid integrating pixel detector

                                          Pixel 1       Pixel 2            Pixel 3   ...   HV (-)

                                            h+
                                            e-      Semiconductor sensor (CdTe)

                                                           Readout ASIC

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    03.04.19 - HighRR BiWeekly Seminar                  David Schimansky                            19
Preliminary Detector Concept

                                         2D hybrid integrating pixel detector

                                          Pixel 1       Pixel 2            Pixel 3   ...   HV (-)

                                            h+
   Designed in Grenoble                     e-      Semiconductor sensor (CdTe)

                      Our job                              Readout ASIC

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    03.04.19 - HighRR BiWeekly Seminar                  David Schimansky                            20
Preliminary Detector Concept: Floorplan

          100 µm                                          ...
                   Pixel
                                                                           ...

                                   (192 pixels)
                                    19.2 mm

                                                  ...
                   100 µm                               ASIC

                                                                                                (4 ASICs)
                                                                                                 ~77 mm
                                                                            Detector Module

                                                                 ...
                                                    12.8 mm
                                                  (128 pixels)

  • ~25k pixels per ASIC
                                                                                    ~115 mm
                                                                                    (9 ASICs)
  • 36 ASICs

  • ~900k pixel in total ≙ 90cm2 detector surface
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    03.04.19 - HighRR BiWeekly Seminar                           David Schimansky                           21
Picking the Sensor Material

                                                                   10-1   100   101    102      103   104   105    106      107 eV

                                                                   Infrared       Ultraviolet                X-rays

                                                                                                      10-100keV

   300µm Si ≈ 1-2% absorption            Thicknesses needed for 99% absorption
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    03.04.19 - HighRR BiWeekly Seminar    David Schimansky                                                        22
Readout ASIC
Brainstorming and first steps

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03.04.19 - HighRR BiWeekly Seminar   David Schimansky   23
ASIC: Essentials

                                         Channel

                                                         Signal
            Pixel                          Front-End                        Storage   Readout
                                                       Processing

                                                         Logic

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    03.04.19 - HighRR BiWeekly Seminar                   David Schimansky                       24
ASIC: Channel with Integrating Front-End
                                             Δ-)./ ~'()*
                                           ⇒ Δ-)./ ~!"#                             2
   !"# = ℎ&"#                                                                       1

   '()* ~!"#                        Isig                       Vint                 0010
                      Sensor                                                  ADC          Storage

    • Sensor generates charge signal when an incoming photon is absorbed

    • Charge sensitive amplifier integrates charge in capacitor: Vint ~ Qsig

    • Well known energy of x-ray photons allows calculating the amount of photons from the
       integrated charge by the CSA

    • However: Dynamic range is limited by depth of ADC (and supply voltage)                          !"#$%&'()*&+"#(,-
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    03.04.19 - HighRR BiWeekly Seminar                     David Schimansky                          25
ASIC: Integrating Front-End, ADC Saturation
                                           'ℎ
 Per 100x100µm2 pixel! 100Mcps ≙ 10%&
                                          ))* +

                                                         • Depending on the photon flux and amount of
                                                             bits, ADC saturates in a matter of µs
                                            11 bit
                                                                ⇒ not suited for long exposure times up to a
                                                                few ms in 7/8 bunch mode

                                            10 bit       • Possible solutions (among others):
                                                                • Digital Integration
                                            9 bit
                                                                • „Continuous Conversion“/Charge Removal
                                            8 bit

                                            7 bit
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     03.04.19 - HighRR BiWeekly Seminar              David Schimansky                                          26
ASIC: Integrating Front-End, Continuous Conversion

  FE without continuous conversion:
  • Sensor charge is collected and measured
                                                                 Sensor
    by CSA

                                                                          SA
                                                                          C
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    03.04.19 - HighRR BiWeekly Seminar        David Schimansky                 27
ASIC: Integrating Front-End, Continuous Conversion

  FE without continuous conversion:
  • Sensor charge is collected and measured
                                                                    Sensor
    by CSA
  • If bucket full (ADC saturates): Additional
    charge is lost

                                                                             SA
                                                                             C
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     03.04.19 - HighRR BiWeekly Seminar          David Schimansky                 28
ASIC: Integrating Front-End, Continuous Conversion

  Idea of continuous conversion:
  • CSA indicates if there is charge in the
                                                                 Sensor
    bucket
  • Use „spoons“ to empty charge bucket

                                                                          SA
                                                                          C
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     03.04.19 - HighRR BiWeekly Seminar       David Schimansky                 29
ASIC: Integrating Front-End, Continuous Conversion

  Idea of continuous conversion:
  • CSA indicates if there is charge in the
                                                                 Sensor
    bucket
  • Use „spoons“ to empty charge bucket

                                                                          SA
                                                                          C
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     03.04.19 - HighRR BiWeekly Seminar       David Schimansky                 30
ASIC: Integrating Front-End, Continuous Conversion

  Idea of continuous conversion:
  • CSA indicates if there is charge in the
                                                                 Sensor
    bucket
  • Use „spoons“ to empty charge bucket

                                                                          SA
                                                                          C
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     03.04.19 - HighRR BiWeekly Seminar       David Schimansky                 31
ASIC: Integrating Front-End, Continuous Conversion

  Idea of continuous conversion:
  • CSA indicates if there is charge in the
                                                                 Sensor
    bucket
  • Use „spoons“ to empty charge bucket
  • Remember amount of spoons needed

                                                                          SA
  • Calculate charge via spoon size and

                                                                          C
    amount => Conversion

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     03.04.19 - HighRR BiWeekly Seminar       David Schimansky                 32
ASIC: Integrating Front-End, Continuous Conversion

                     DigOut                 Counter
                      (=0)

                                         Charge Pump                                Comparator

                                                                  Vint ~ Qsig
                                   Signal
                                   peak

                                                                 Charge Sensitive
               Sensor
                                 Isig                               Amplifier
                                                                                       Vint
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    03.04.19 - HighRR BiWeekly Seminar                 David Schimansky                          33
ASIC: Integrating Front-End, Continuous Conversion

                     DigOut
                                            Counter
                      (=0)

                                         Charge Pump                                Comparator

                                                                  Vint ~ Qsig
                                   Signal
                                   peak

                                                                 Charge Sensitive
               Sensor
                                 Isig                               Amplifier
                                                                                       Vint
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    03.04.19 - HighRR BiWeekly Seminar                 David Schimansky                          34
ASIC: Integrating Front-End, Continuous Conversion

                                                               Comparator fires if Vint is
                                                                  above threshold and
                                                              activates charge pump and
                     DigOut                 Counter                     counter
                      (=0)
                                                                                                   Comparator
                                                                                                     applies
                                                                                                 threshold to Vint

                                         Charge Pump                                Comparator

                                                                  Vint ~ Qsig
                                   Signal
                                   peak

                                                                 Charge Sensitive
               Sensor
                                 Isig                               Amplifier
                                                                                       Vint
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    03.04.19 - HighRR BiWeekly Seminar                 David Schimansky                                     35
ASIC: Integrating Front-End, Continuous Conversion
                                              Counts injected
                                                                            Comparator fires if Vint is
                                             charge packages
                                                                               above threshold and
                                                                           activates charge pump and
                         DigOut                   Counter
                                                  Counter                            counter
                          (=1)
                                                                                                               Comparator
                                                                                                                 applies
                                                                                                             threshold to Vint

 Injects well defined                          Charge Pump
                                               Charge Pump                                      Comparator
                                                                                                Comparator
charge packages (e.g.
   ~ single photon)
                                                                               Vint ~ Qsig
                                       Signal                                                                 Vint is discharged
                                       peak                                                                    and falls below
                                                                                                                   threshold
                                                                             Charge Sensitive
                                                                             Charge Sensitive
                   Sensor
                                     Isig                                       Amplifier
                                                                                 Amplifier
                                                  Charge pump                                      VVint
                                                                                                      int
                                                 injects negative
                                                      signal                                                              !"#$%&'()*&+"#(,-
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        03.04.19 - HighRR BiWeekly Seminar                          David Schimansky                                    36
ASIC: Integrating Front-End, Continuous Conversion

                                                                                                    #$
                                         • Similar circuits reach counting rates up to 1010
                                                                                                  #%&'()*

                                            (see „High Dynamic Range X-Ray Detector Pixel Architectures
                                            Utilizing Charge Removal“ , IEEE Trans. Nucl. Sci, vol. 64, no. 4, April
                                            2017)

                                                                                                             #$
                                         • With 100µm pixels that is a manageable flux of 10+,
                                                                                                            --.*
                                                                    #$
                                           (requirement: > 10++           )
                                                                   --.*

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    03.04.19 - HighRR BiWeekly Seminar       David Schimansky                                                     37
ASIC: Integrating Front-End, First Prototype
                                          gain = 8
 charge
                                         à equal CPs
  input                                                        • 1st stage pumps 8 ph
                                                               • 2nd stage pumps 1 ph
                                                               • fpump ~ 100 MHz
                                                               à 1st stage: 100 ph in 175ns
                                                                               &'
                                                               à 10# − 10% &()*+,-

                                                                              serial
                                                                             digital
                                                                             output            !"#$%&'()*&+"#(,-
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    03.04.19 - HighRR BiWeekly Seminar      David Schimansky                                  38
ASIC – SUS65T1
First Submission Nov. 14, 2018

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03.04.19 - HighRR BiWeekly Seminar   David Schimansky   39
SUS65T1

   • SuS‘s first submission in the TSMC 65nm technology

   • Main goals:
         • Get to know the technology

         • Test prototype structures (bond pads, I/O circuits, synthesized digital blocks, JTAG, FE, ..)

         • Gain experience with sensor connection (bump bonding) and characterisation

   • Implemented blocks are not optimised for performance

   • The manufactured chip arrived a month ago

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   03.04.19 - HighRR BiWeekly Seminar              David Schimansky                                        40
SUS65T1: Block diagram
                                                          OUT_PX_MUX                              SUS65T1

            Pixel connection
                                                                                       FE1                  FE_Out[0]
                                         PixelBus
                               ...

                                                                                       FE2
                                                                                                            FE_Out[1]

                                                             MUX_ctrl    FE_ctrl       cnt_en

                                                             ControlBlock (JTAG,
                                              ...

                                 Other                      sequencer, serial data         DACs
                                                                   output)

                                               cmn_ctrl

                                     CommonPx             CLK TCK TDI TMS TDO    RUN MON_DIG                             !"#$%&'()*&+"#(,-
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                                                                            SER_OUT

   03.04.19 - HighRR BiWeekly Seminar                                   David Schimansky                                41
SUS65T1: Layout

                                                             Pixel bump bond
      I/O & power pads                                       matrix: 28 pads
                                                             (50x50µm2) for
                                                             100µm and
                                                             200µm pitch
                                                             configurations

                                                                   Pixel wire bonds: 28 pads
  Analogue output buffers                                          connected to the matrix
  to monitor one FE
                                                                 5 multiplexers + switches to
                                                                 common potential

                                                                  2 frontends + charge
                     other                                        injection circuits

                                                                  Control block: JTAG interface for
                                                                  slow control (MUX, DACs etc.) +
                                                                  sequencer for dynamic control
                                                                  of FEs + pixel logic

                                                              DACs
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     03.04.19 - HighRR BiWeekly Seminar   David Schimansky                                  42
SUS65T1: First Signs of Life

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    03.04.19 - HighRR BiWeekly Seminar   David Schimansky   43
SUS65T1: First Signs of Life

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    03.04.19 - HighRR BiWeekly Seminar   David Schimansky   44
SUS65T1: First Signs of Life

       keep CSA in permanent reset
           DDYN_RESET=1
                                             SUS65T1

                                     FE output buffer            Oscilloscope
                     -
                                                        FE_OUT
   VREF             +
   (via DAC)
  (DAC15)
                                       Buffer bias
                  Vc, Ilegs
               Frontend    , Itail
                         CSA             (DAC5)
                   (DAC4,10,11)

This first test shows qualitatively:
      • I/O pads work
      • JTAG slow control works
      • DACs work
      • Frontend amplifier works                                                            !"#$%&'()*&+"#(,-
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          03.04.19 - HighRR BiWeekly Seminar                            David Schimansky   45
Conclusion & Outlook
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03.04.19 - HighRR BiWeekly Seminar   David Schimansky   46
Conclusion

   • Project name: XIDer

   • General aim: Multi-purpose detector for time-resolved x-ray experiments at the ESRF

   • My job:
         • Design, characterisation & test of the readout ASIC

         • Verify feasibility

   • Parallel development of readout ASIC (in Heidelberg) and sensor (in Grenoble) has begun
         • ASIC with first prototype readout structures arrived a month ago and is currently under test
         • First sensor prototype structures for testing have recently arrived and are under test

   • First tests with ASIC show qualitative functionality of most of the prototype structures
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   03.04.19 - HighRR BiWeekly Seminar             David Schimansky                                        47
Outlook

   Next steps in the project:

   • Continue functional tests of prototype ASIC SUS65T1

   • Quantitative analysis of prototype frontend performance

   • Design of alternative readout architectures & improvements

   • Test different procedures of bump bonding the sensor to the ASIC

   • Sensor prototype characterisation

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Backup
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Backup
CdTe

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CdTe Crystals

                                   Taken from H. Shiraki et al „THM growth and characterization of 100 mm diameter CdTe single crystals“, IEEE Trans. Nucl. Sci, vol. 54, pp. 117-1723, 2009

          • 100mm diameter, 300mm length

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    03.04.19 - HighRR BiWeekly Seminar                                                   David Schimansky                                                                                      51
tion is the end result of the creation o
Cd(Zn)Te Polarisation                                                                                                                       electric field, and the method can be s
                                                                                                                                                "1! The amount of charge, denoted
                                                                                                                                            sary to collapse the electric field at a
                                                                                                                                            lated.
                                                                                                                                                "2! The time dependence, Q"T!, of
    Count rate collapses for high(a)Resulting
                                    photoncounts
                                              fluxes:
                                                  above threshold                                                                           charge density within the detector is c
                                                                                                                                                "3! Polarization results when the
                                                                                                                                            "i.e., steady state value! of the build
                                                                                                                                            exceeds that necessary to collapse th
                                                                                                                                            pinch point. Mathematically, thi
                                                                                                                                            limT→" Q"T! = Q*.
                                                                                                                                                The result of the third step, as we w
                                                                                                                                            functional dependence of the maximum
                                                                                                                                            critical flux #!*! on device design and

                                                                                                                                                              A. Necessary positive
                                                                                                                                               We begin by considering a photon
                                                                                                                                            flux #! describing the number of ph
                                                                                                                                            intersect the cathode surface of the d
                                                                                                                                            The source is assumed to be mono
                                                                                                                                            taken as the mean value of the x-ray
                                                                                                                                            and denoted by Ē!. The generation rat
                                                  Taken fromcounts
                                            (b)Measured         „Nature of polarization in wide-bandgap semiconductor detectors under
                                                                           above threshold                                                  within the detector, therefore, is ex
                                                  high-flux irradiation: Application to semi-insulating Cd Zn Te“ (D. S. Bale, C. Szeles,
                                                                                                                                            and has the form
                                                                                                           1-x   x
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                                             FIG. 5. "a! Simulated counts above a 25 keV threshold as the
                                         photon flux rate "x-ray tube current! is increased. "b! Measured                                                                     Ē! 1 −
    03.04.19 - HighRR BiWeekly Seminar
                                                                                                                                                                 $"Z!52= #!          e
                                         counts for 256 channelsDavid
                                                                   of aSchimansky
                                                                         polarizing detector as the photon flux                                                               %czt &
                                         rate "tube current! is increased.
Backup
Sensor-Prototype

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Sensor Prototype

                             4mm
                                                    For bump bonding on ASIC
                                   300µm
                                                    For bump bonding or gluing on interconnector
                                            100µm

 4mm
                                                    • 4x4 pixel test prototypes

                                                    • Three different pitches (100µm, 200µm, 300µm)
                                           200µm
                                                    • Different bond pad configurations (centered, cornered) for
                                                      bump bonding onto ASIC as well as interconnector

                                                    • Will be sent out for manufacturing soon
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    03.04.19 - HighRR BiWeekly Seminar              David Schimansky                                               54
Sensor Prototype: Possible ASIC Connections

                    Interconnector

                        Test ASIC

                                                                                       Test ASIC
                                           Test ASIC

                ⇒ Test ASIC needs a flexible bonding structure for its connection to the pixel matrix
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    03.04.19 - HighRR BiWeekly Seminar                    David Schimansky                              55
Backup
Synchrotrons

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Synchrotron Radiation Brilliance

                                                         photon flux
                                 SR Brilliance =
                                                      (ΔA) (ΔΩ) (Δλ/λ)

                                            source area                      spectral interval
                                                               solid angle

    • The figure of merit for a synchrotron‘s performance

    • High brilliance ≙ high flux of useful photons at the sample and detector

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    03.04.19 - HighRR BiWeekly Seminar                    David Schimansky                       57
Synchrotron Generations

                                                                         average                 Brilliance                        peak

                                                                                     photons/s/mm2/mrad2/0.1%BW
                                                                                                                                       1035
    •   1st   : Particle accelerators that generate                                          4th generation FELs

        synchrotron light as a parasitic effect                                                                                        1030
                                                                         1025
    • 2nd : Dedicated synchrotron light production                                                      planned

                                                                                                                      3rd generation
                                                                                                    current
                                                                         1020
    •   3rd   : Higher brilliance by introducing insertion
        devices (wigglers/undulators)                                                     dedicated
                                                                         1015           low emittance
                                                                                                                  2nd generation

    • 4th : Even higher brilliance and coherence                                        parasitic
                                                                                                         1st generation
                                                                           10
                                                                         10                           Synchrotron sources
                                                                                   X-ray tubes

                                                                         105
                                                                                1900 1920 1940 1960 1980 2000 2020 2040                        !"#$%&'()*&+"#(,-
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                                                                                                        Year

    03.04.19 - HighRR BiWeekly Seminar                David Schimansky                                                                        58
Backup
ESRF

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03.04.19 - HighRR BiWeekly Seminar   David Schimansky   59
Research at the ESRF

                                         • ~50 x-ray beam lines publicly available to external
                                           research groups as well as industry

                                         • Six major research groups maintain these beam
                                           lines and tailor them to specific areas of research:
                                              • Structure of materials
                                              • Structural biology

                                              • Electronic Structure, Magnetism and Dynamics
                                              • Matter at extremes
                                              • Complex systems & biomedical sciences
                                              • X-ray nanoprobes
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    03.04.19 - HighRR BiWeekly Seminar    David Schimansky                                     60
Research at the ESRF

                                                                 Structure of Materials:
                                                      1
                                                  ID3

                                                                      • Study composition, atomic structure and crystalline
                                                                         state of materials via diffraction and spectroscopy

                                                                      • Observe defects and traps in materials

                                                                      • Example: Formation of a crack in a silicon wafer
                                                                         observed with x-ray diffraction imaging (35kHz)
          ID
            22

                                                                                                                    See „Real-time direct and diffraction

                                                                                                                    Scheel, A. N. Danilewsky in IUCrJ,
                                                                                                                    X-ray imaging of irregular silicon
                                                                                                                    wafer breakage“ (A. Rack, M.
ID1
      9

                                                                                                                    Volume 3, 2016)
                                                          ID11

                                          5   A
                                      ID1                                                                                                                    !"#$%&'()*&+"#(,-
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                 03.04.19 - HighRR BiWeekly Seminar               David Schimansky                                                                          61
Research at the ESRF

                                               Matter at extremes
                                                   • Study behaviour of matter in extreme conditions with
               ID27

                                                     pressures beyond 200GPa and temperatures up to 5000K

                                                   • Example: Use diamond anvil cells and laser heating to
  ID24
     BM

                                                     emulate conditions in earth‘s core
        23

                                            ID
                                              06

             ID18

                                5   B
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       03.04.19 - HighRR BiWeekly Seminar          David Schimansky                                         62
Backup
Sensor

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03.04.19 - HighRR BiWeekly Seminar   David Schimansky   63
Sensor Material

                                                                                    10-1   100   101    102      103   104   105   106    107 eV
    • Energy range: 10-100keV
                                                                                    Infrared       Ultraviolet                X-rays

    • Usual aim: Build detector with high stopping power to absorb as                                                  10-100keV

       many photons as possible

                                                                             &'
    • Dominant process in our energy regime: Photo effect            "#$ ~    *
                                                                             ( )+

                 ⇒ The higher the energy, the less absorption (via p.e.)

                 ⇒ Use material with high Z (and high density)

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    03.04.19 - HighRR BiWeekly Seminar            David Schimansky                                                           64
Cd(Zn)Te Sensor

   • Tendency towards using Cd(Zn)Te due to:
         + High stopping power (Z, !) in desired energy region
         + Low noise @ room temperature due to band gap size (1.44eV compared to Germanium: 0.66eV)

   • However, Cd(Zn)Te entails many challenges:
         - Large crystals hard to produce
         - Hole trapping
         - Afterglow
         - Polarisation
         - Brittle
         - Sensitive to heat
         - Oxidizes in contact to air
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   03.04.19 - HighRR BiWeekly Seminar              David Schimansky                                   65
Backup
Frontend

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ASIC: Integrating Front-End, Digital Integration

                      ADC conversion + reset
                                                                • Split integration into sub intervals
          Integrate
                                                                • Summate sub images in storage

                                                                • Choice of integration window size
                                                                     depends on bunch structure, photon rate,
                            Exposure time
                                                                     conversion time, # ADC bits, ADU, DNL
                                                                     etc.
                           e.g. 100         +   100 = 200
Vint

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       03.04.19 - HighRR BiWeekly Seminar         David Schimansky                                       67
SUS65T1: Pixel Matrix Connection

                  Wire bonds
                                           ASIC            • 28 pads allow connecting sensors with
                      ...
                                                               100µm and 200µm pitch
       200µm            100µm
                                                           • Additional wire bond pads connected to
                                                               pixel matrix (not shown)

                                         ...

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    03.04.19 - HighRR BiWeekly Seminar            David Schimansky                                    68
SUS65T1: Pixel Matrix Connection

                  Wire bonds
                                           ASIC            • 28 pads allow connecting sensors with
                      ...
                                                               100µm and 200µm pitch
       200µm            100µm
                                                           • Additional wire bond pads connected to
                                                               pixel matrix (not shown)

                                         ...

                     100µm pitch                                                                       !"#$%&'()*&+"#(,-
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    03.04.19 - HighRR BiWeekly Seminar            David Schimansky                                    69
SUS65T1: Pixel Matrix Connection

                  Wire bonds
                                           ASIC            • 28 pads allow connecting sensors with
                      ...
                                                               100µm and 200µm pitch
       200µm            100µm
                                                           • Additional wire bond pads connected to
                                                               pixel matrix (not shown)

                                         ...

                     200µm pitch                                                                       !"#$%&'()*&+"#(,-
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    03.04.19 - HighRR BiWeekly Seminar            David Schimansky                                    70
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