Dynamic Testing of Lime-Tree (Tilia Europoea) and Pine (Pinaceae) for Wood Model Identification - MDPI

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Dynamic Testing of Lime-Tree (Tilia Europoea) and Pine (Pinaceae) for Wood Model Identification - MDPI
materials
Article
Dynamic Testing of Lime-Tree (Tilia Europoea) and
Pine (Pinaceae) for Wood Model Identification
Anatoly Bragov 1 , Leonid Igumnov 1,2, *, Francesco dell’Isola 1 , Alexander Konstantinov 1,2 ,
Andrey Lomunov 1 and Tatiana Iuzhina 1
 1   Research Institute for Mechanics, National Research Lobachevsky State University of Nizhny Novgorod,
     603950 Nizhny Novgorod, Russia; bragov@mech.unn.ru (A.B.); fdellisola@gmail.com (F.d.);
     constantinov.al@yandex.ru (A.K.); lomunov@mech.unn.ru (A.L.); yuzhina_tatiana@mech.unn.ru (T.I.)
 2   Research and Education Mathematical Center “Mathematics for Future Technologies”,
     603950 Nizhny Novgorod, Russia
 *   Correspondence: igumnov@mech.unn.ru; Tel.: +7-910-792-7826
                                                                                                   
 Received: 22 October 2020; Accepted: 19 November 2020; Published: 20 November 2020                

 Abstract: The paper presents the results of dynamic testing of two wood species: lime-tree
 (Tilia europoea) and pine (Pinaceae). The dynamic compressive tests were carried out using the
 traditional Kolsky method in compression tests. The Kolsky method was modified for testing the
 specimen in a rigid limiting holder. In the first case, stress–strain diagrams for uniaxial stress state
 were obtained, while in the second, for uniaxial deformation. To create the load a gas gun was
 used. According to the results of the experiments, dynamic stress–strain diagrams were obtained.
 The limiting strength and deformation characteristics were determined. The fracture energy of lime
 and pine depending on the type of test was also obtained. The strain rates and stress growth rates
 were determined. The influence of the cutting angle of the specimens relative to the grain was noted.
 Based on the results obtained, the necessary parameters of the wood model were determined and
 their adequacy was assessed by using a special verification experiment.

 Keywords: timber; natural composite; Kolsky method; deformation diagrams; wood species;
 energy absorption; wood model; verification

1. Introduction
      Wood is a complex natural composite. It is widely used as a material for damping intensive
dynamic loads of shock or explosive nature. In order to conduct reliable numerical analysis of the
designs of containers for transporting hazardous substances, using wood as shock damping components,
reliable mathematical models are required that take into account its complex multicomponent structure
of wood. The actively developing models of wood deformation and destruction can be used in various
design complexes to simulate the behavior of technically complex structures that incorporate wood
elements. However, the complex nature of wood means that not a single model can be used for all
purposes, thus different models must be used to solve various specific problems. In order to reliably
describe the behavior of wood in a dynamically loaded structure, its model should include a sufficiently
large set of parameters that take into account the deformation anisotropy and the dependence of the
strength properties on the strain rate, density, temperature and moisture content. For example, in the
manual for the LS-DYNA software package, the wood model No. 143 has 29 parameters: five modules
for transversely isotropic constitutive equations, six tensile strengths for yield criteria, four hardening
parameters to peak stresses, eight softening parameters after peak, and six parameters speed effect [1].
The LS-DYNA calculation complex library contains model parameters for only two wood species:
southern yellow pine and Douglas fir. This necessitates detailed studies of various wood species

Materials 2020, 13, 5261; doi:10.3390/ma13225261                             www.mdpi.com/journal/materials
Dynamic Testing of Lime-Tree (Tilia Europoea) and Pine (Pinaceae) for Wood Model Identification - MDPI
Materials 2020, 13, 5261                                                                                2 of 12

for various types of stress–strain states in a wide range of strain rates and temperatures, in order to
equip mathematical models of wood with parameters (identification) that can adequately describe the
behavior of the engineering structure containing wood components under shock wave loads.
      The first detailed review of using wood as an element of damping structures was given by
Johnson [2]. In the report, he noted that the dynamic properties of wood are not well understood.
In the past three decades, quite a lot of works have appeared that explored various aspects of the
high-speed deformation and destruction of wood, including the use of wood as a damping material in
containers for transportation of radioactive materials by air, road and rail transport [3]. A large amount
of research into the dynamic properties of wood was performed by Reid et al. [4–6]. In these works,
the dependences of destructive stress and energy absorption on the impact velocity were obtained.
      It was noted that dynamic destructive stresses are several times higher than static ones. The authors
also postulated that failure stresses of specimens fabricated along the grain are an order of magnitude
higher than that of the specimens cut transverse to the grain. The relationship between mechanical
parameters of selected wood species (Carya sp., Fagus sylvatica L., Acer platanoides L., Fraxinus excelsior L.,
Ulmus minor Mill.) and the grain orientation angle concern loading direction was investigated in [7].
It was observed that as the angle between fibers and loading direction increases whereas the mechanical
characteristics of all wood species decrease.
      In the works of Bragov et al., using the Kolsky method, dynamic diagrams of birch, aspen,
and sequoia were obtained at strain rates of ~103 s−1 with different direction of cutting specimens
relative to the direction of timber fibers [8,9]. The deformation diagrams of specimens under loading
along the grain are much higher than those under loading transverse to the grain. The limiting
deformative characteristics have the opposite direction.
      In recent years, interest in studying the effect of moisture, density and cutting angle on the
mechanical properties of wood has increased significantly. Adalian et al. [10] and Eisenacher et al. [11]
carried out a cycle of tests on wood in the range of strain rate from 10−3 to 103 s−1 . Wouts et al. [12],
Ha et al. [13,14] and Hao et al. [15] considered the damping ability of various biological materials
of plant origin from the point of view of improving artificial damping structures. Mach et al. [16]
calculated the hysteresis losses (dissipated energy) as the area bounded by the loading and unloading
curves, whereas stored energy (recoverable energy) is defined as the area under the unloading curve.
Thus, the total energy is calculated by summing the area of the hysteresis loss and the stored energy.
In the work of Novikov et al. [17], a large number of tests of sequoia, birch, aspen, and pine was
carried out at different cutting angles, temperatures ranged from −30 ◦ C to +65 ◦ C, and at the moisture
content of 5%, 20% and 30%. As a result, the dependence of strength on moisture and cutting angle
was determined.
      The mechanical properties of wood strongly depend on the place of growth, its age, the place of
cutting and the type of stress–strain state. Therefore, the results obtained by different authors may
differ significantly from each other. The purpose of this work is to conduct a detailed study of the
effect of strain rate and type of stress–strain state on the mechanical properties of wood as well as to
identify and verify the wood model.

2. Test Methods, Materials and Specimens
     For dynamic compressive tests of wood, the Kolsky method and split Hopkinson pressure bar
(SHPB) technology were used [18]. Figure 1 shows the installation diagram, as well as the main formulas
for determining the parametric dependencies of deformation, stress and strain rate of the sample under
compression. Two measuring bars were made of high-strength aluminum alloy and had a diameter of
20 mm and length of 1.5 m. During testing, a striker accelerated in the barrel of a gas gun impacts the
SHPB and excites an elastic compression wave in the loading measuring bar, which, upon reaching the
specimen, deforms it. The second (support) measuring bar acts as a dynamometer-waveguide and
allows you to register the transmitted strain pulse εT (t) and then to determine the process of stress
developing in the specimen. The pulse εR (t) reflected from the specimen in the loading bar makes it
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specimen, and its integration allows to determine the process of the specimen deformation
possible to determine the process of strain rate change in the specimen, and its integration allows to
development. Small-length foil strain gages were used for registration elastic strain pulses in the bars.
determine the process of the specimen deformation development. Small-length foil strain gages were
Based on these pulses, the parametric processes of stress, strain and strain rate over time are
used for registration elastic strain pulses in the bars. Based on these pulses, the parametric processes of
calculated using the formulae shown in the lower part of Figure 1. Then, excluding time as a
stress, strain and strain rate over time are calculated using the formulae shown in the lower part of
parameter, a dynamic stress–strain curve is constructed with the known law of variation of the strain
Figure 1. Then, excluding time as a parameter, a dynamic stress–strain curve is constructed with the
rate [19].
known law of variation of the strain rate [19].

                               Figure 1. Installation scheme and basic dependencies.
                               Figure 1. Installation scheme and basic dependencies.
     Dynamic tests were carried out with specimens of lime-tree (Tilia europoea) and pine (Pinaceae)
with aDynamic
       diametertests
                 of 20were   carried
                        mm and        out with
                                 a length  of 10specimens
                                                 mm, cut from of lime-tree
                                                                  solid wood(Tilia europoea)
                                                                               at an          0◦ and
                                                                                     angle ofand  pine ◦ relative
                                                                                                     90(Pinaceae)
with
to theaaxis
        diameter   of 20trunk.
            of the tree   mm andThe aflat
                                       length
                                          ends of the
                                                   10 mm,    cut from
                                                       samples          solid wood
                                                                  were carefully      at an angle before
                                                                                   hand-grinded    of 0° and  90°
                                                                                                         testing.
relative
The      to theparameters
     physical   axis of the of
                            tree trunk.
                               tested     The flatare
                                       materials   ends  of theinsamples
                                                      shown               were
                                                                  the Table  1. carefully hand-grinded before
testing. The physical parameters of tested materials are shown in the Table 1.
                                Table 1. The physical parameters of tested materials.
                                Table 1. The physical parameters of tested materials.
      Wood Species                           Lime-Tree                                         Pine
    Wood   Species
       Parameter            Along the GrainLime-Tree
                                               Transverse to the Grain     Along the Grain      Pine
                                                                                                Transverse to the Grain
      Parameter 3          Along the Grain    Transverse to the Grain      Along the Grain      Transverse to the Grain
     Density, g/cm             0.505 ± 0.02         0.512 ± 0.015            0.435 ± 0.01            0.484 ± 0.015
    Density, g/cm3           0.505 ± 0.02          0.512 ± 0.015             0.435 ± 0.01             0.484 ± 0.015
   Moisture content,%%
  Moisture content,              7.5 ± 0.2
                               7.5 ± 0.2               7.9±±0.3
                                                      7.9    0.3               6.8 ±± 0.3
                                                                               6.8    0.3                7.1±± 0.2
                                                                                                        7.1    0.2

      The total
     The   totalamount
                 amountofoftested
                              tested  samples
                                    samples  of of
                                                eacheach wood
                                                      wood       species
                                                              species     amounted
                                                                      amounted        50 pieces:
                                                                                  50 pieces:       40 pieces
                                                                                              40 pieces were were
                                                                                                              used
used
for    for mechanical
    mechanical          testing
                  testing and 10and  10 pieces
                                  pieces  were were
                                                used used    for subsequent
                                                       for subsequent   woodwood
                                                                               model model    verification.
                                                                                        verification.       In each
                                                                                                       In each  test
test mode   during   mechanical   testing (strain  rate and loading   direction), 4–5 experiments
mode during mechanical testing (strain rate and loading direction), 4–5 experiments were carried out, were  carried
out,results
the   the results  of which
            of which          were
                       were then     then averaged.
                                  averaged.             All the experiments
                                              All the experiments              were
                                                                      were carried  outcarried  out in conditions
                                                                                         in laboratory  laboratory
conditions
at           at room temperature
   room temperature      and 50% airand   50% air humidity.
                                       humidity.

3.
3. Experimental Results
     Using         abovemethods,
      Using the above     methods,the  thedynamic
                                            dynamic      tests
                                                      tests    of pine
                                                            of pine  andand   lime-tree
                                                                          lime-tree   werewere     carried
                                                                                             carried   out. Asout.a result,
                                                                                                                     As a
result,
their dynamic stress–strain curves, the ultimate strength and deformative characteristics of the
        their dynamic   stress–strain   curves,   the  ultimate  strength  and   deformative     characteristics    of the
specimens
specimens cut cutalong
                  alongand
                         andtransverse
                              transverse  toto
                                             thethe
                                                  grain  were
                                                     grain  wereobtained.  Dynamic
                                                                    obtained. Dynamic  strain  diagrams
                                                                                           strain   diagramsfor pine  and
                                                                                                                 for pine
lime-tree  underunder
and lime-tree      uniaxial stress stress
                         uniaxial   state are  presented
                                            state           in Figures
                                                   are presented         2 and 3. 2The
                                                                      in Figures     and figures
                                                                                            3. Theshow    the averaged
                                                                                                     figures   show the
stress–strain  curves  and  appropriate     strain  rate-strain   curves.  The  spread    of the  obtained
averaged stress–strain curves and appropriate strain rate-strain curves. The spread of the obtained           properties
was  no more
properties     than
             was  no6%.
                     moreIn than
                            all figures
                                   6%. Insolid  lines show
                                           all figures   solidthe  dependences
                                                               lines              of the true stress
                                                                      show the dependences             of the
                                                                                                   of the  truespecimen
                                                                                                                 stress of
Materials 2020, 13, 5261                                                                                                           4 of 12
Materials 2020, 13, 5261                                                                                                            4 of 12
Materials 2020, 13, 5261                                                                                                           4 of 12
 the specimen on its deformation σ~ε, and the dotted lines (in the lower part of the diagrams)
on its deformation σ~ε, and the dotted lines (in the lower part of the diagrams) correspond to the
the  specimen
 correspond  to on
                the its deformation
                    history            σ~ε,rate
                             of the strain   andchange
                                                  the dotted  lines
                                                       έ~ε (the     (in the lower
                                                                 appropriate axis ispart of right).
                                                                                     on the  the diagrams)
history of the strain rate change έ~ε (the appropriate axis is on the right).
correspond to the history of the strain rate change έ~ε (the appropriate axis is on the right).

                  Figure 2. Deformation diagrams of pine under loading along and across the grain.
                  Figure
                  Figure 2. Deformation diagrams
                         2. Deformation diagrams of
                                                 of pine
                                                    pine under
                                                         under loading
                                                               loading along
                                                                       along and
                                                                             and across
                                                                                 across the
                                                                                        the grain.
                                                                                            grain.

            Figure 3. Deformation diagrams of lime-tree under loading along and across the grain.
            Figure 3. Deformation diagrams of lime-tree under loading along and across the grain.
            Figure
      Two test     3. Deformation
               modes               diagrams
                      on strain rate        of lime-tree
                                     were chosen:  with under loading along
                                                         non-destructive andand across the results.
                                                                              destructive  grain. From the
      Twostress–strain
obtained     test modes on        strain rate
                               diagrams,          were chosen:
                                             it follows       that forwith
                                                                        bothnon-destructive
                                                                                wood species the    andspecimens
                                                                                                           destructive cutresults.
                                                                                                                            and loadedFrom
 the  Two   test
     obtained     modes      on
                  stress–strain  strain   rate
                                     diagrams,   were it   chosen:
                                                          follows    with
                                                                     that     non-destructive
                                                                             for  both    wood     and
                                                                                                  species
along the grain have the largest modulus of the load branch in the diagram, as well as ultimate stress    destructive
                                                                                                             the specimensresults.cutFrom
                                                                                                                                        and
the  obtained
 loaded
and      along
     energy      stress–strain       diagrams,       it  follows    that    for  both    wood    species
                  the grain have the largest modulus of the load branch in the diagram, as well as ultimate
               absorption.                                                                                  the  specimens       cut   and
loaded
 stress  along
        and      the
              energy
      Wood endurance    grain  have
                          absorption.
                               can be theindicated
                                           largest modulusin Figure of the    load branch
                                                                       4, where       diagramsin the
                                                                                                   ofdiagram,
                                                                                                        fivefold as   well asofultimate
                                                                                                                  loading          a pine
stress  and  energy      absorption.
specimen with its minor damages (curves 1–5) and a single independent loading of anotherofsimilar
      Wood      endurance       can   be  indicated         in Figure   4,    where    diagrams     of   fivefold  loading          a pine
      Wood
 specimenwith
specimen       endurance
             withitsitscomplete can  be
                          minor damages  indicated
                                                 (curves
                                    failure (curve         in  Figure
                                                              1–5)
                                                         6) are         4,   where
                                                                    and a single
                                                                 presented.            diagrams
                                                                                       independent
                                                                                 The diagrams       of  fivefold
                                                                                                         loadingon
                                                                                                   are located    loading
                                                                                                                   oftheanother of  a  pine
                                                                                                                                   similar
                                                                                                                           deformation
specimen
 specimen
axis        with
              withitsits
     conditionally        minor
                         in order damages
                            complete            (curves
                                          failure
                                    to make            (curve
                                                it easier     1–5)
                                                                 6)andareathe
                                                              to assess      single
                                                                                effectindependent
                                                                            presented.                  loadingare
                                                                                             The diagrams
                                                                                        of multiple    loading    of the
                                                                                                                 on    another
                                                                                                                        located    similar
                                                                                                                                   on the
                                                                                                                           steepness     of
specimen
 deformation
the           with
    load sections     its   complete
                 axisofconditionally     failure
                          the stress–strain in order  (curve
                                                curves.toThe     6)
                                                               make  are   presented.
                                                                      it easier
                                                                   average                  The
                                                                                    to assess
                                                                               strain             diagrams
                                                                                        rate at the  effectloads
                                                                                                repeated        are    located
                                                                                                             of multiple      loadingsthe
                                                                                                                   was ~600–800    on    on,
                                                                                                                                         −1
deformation
 the steepnessaxisof the conditionally
                            load sections  inoforder      to make it easier
                                                   the stress–strain       curves. to The
                                                                                       assess  the effect
                                                                                            average         ofrate
                                                                                                       strain   multiple     loading
                                                                                                                    at repeated          on
                                                                                                                                      loads
the
 wassteepness
      ~600–800of   s−1the  load
                       , and      sections
                              in the  case ofofspecimen
                                                  the stress–strain
                                                                failure, curves.
                                                                          the strain  The  average
                                                                                         rate         strain
                                                                                              was about       rates−1
                                                                                                            2200    at. One
                                                                                                                         repeated    loads
                                                                                                                              can clearly
was ~600–800 s−1, and in the case of specimen failure, the strain rate was about 2200 s−1. One can clearly
Materials 2020, 13, 5261                                                                                                    5 of 12
Materials 2020, 13, 5261                                                                                                    5 of 12
Materials 2020, 13, 5261                                                                                                    5 of 12
 see a decrease in the steepness of the load section of stress–strain curve during repeated loads by a
and in the case of specimen failure, the strain rate was about 2200 s−1 . One can clearly see a decrease
 factor
see     of 2–3, which
     a decrease  in the is associated
                         steepness      withload
                                     of the   partial destruction
                                                 section           of the specimen
                                                          of stress–strain         during
                                                                           curve during    each loading
                                                                                        repeated         and
                                                                                                  loads by a
in the steepness of the load section of stress–strain curve during repeated loads by a factor of 2–3,
 violation
factor      of the
        of 2–3,    flatness
                which       of its ends.
                        is associated   with partial destruction of the specimen during each loading and
which is associated with partial destruction of the specimen during each loading and violation of the
violation of the flatness of its ends.
flatness of its ends.

           Figure 4. An example of multiply repeated loading of the specimen with its minor damage.
           Figure 4. An example of multiply repeated loading of the specimen with its minor damage.
           Figure 4. An example of multiply repeated loading of the specimen with its minor damage.
      As an
      As  animportant
              importantcharacteristic
                        characteristicof of
                                         thethe  timber
                                             timber     damping
                                                     damping       capacity,
                                                               capacity,       the energy
                                                                         the energy          absorption
                                                                                       absorption  of the of  the
                                                                                                          tested
 tested
wood     wood
      Asspeciesspecies
          an important was  estimated
                        characteristic
                was estimated           under
                                        of the loading
                               under loading    timber   along
                                                        damping
                                                 along and      andcapacity,
                                                                     transverse
                                                            transverse  to thethe toenergy
                                                                                grain the
                                                                                       bygrain  by calculating
                                                                                             absorption
                                                                                           calculating    ofarea
                                                                                                        the  the
 the area
tested    under
        wood     the curve
               species was σ~ε  (Figure
                           estimated
under the curve σ~ε (Figure 5).          5).
                                       under   loading  along  and  transverse   to  the  grain by  calculating
the area under the curve σ~ε (Figure 5).

   a)                                                             b)
   a)                                                             b)
               Figure
               Figure 5. Energy absorption
                      5. Energy absorption of
                                           of the
                                              the tested
                                                  tested wood
                                                         wood species:
                                                              species: (a)
                                                                       (a) for
                                                                           for pine,
                                                                               pine, (b)
                                                                                     (b) for
                                                                                         for lime-tree.
                                                                                             lime-tree.
               Figure 5. Energy absorption of the tested wood species: (a) for pine, (b) for lime-tree.
      For both wood species, there is a significant excess of energy absorption by the specimens cut and
       For both wood species, there is a significant excess of energy absorption by the specimens cut
tested along the grain, compared to the specimens cut and tested transverse to the grain.
 and tested
      For both along
                   woodthespecies,
                             grain, compared
                                      there is ato    the specimens
                                                   significant    excesscutof and
                                                                              energy tested    transverse
                                                                                           absorption     bytothethespecimens
                                                                                                                     grain.      cut
      It is interesting to compare the results on the damping ability of wood-based materials obtained
       It is interesting
and tested     along the to    compare
                            grain, comparedthe results
                                                  to theon    the damping
                                                          specimens           ability
                                                                        cut and     testedof wood-based
                                                                                              transverse tomaterials
                                                                                                                the grain.obtained
by other researchers. In the work [12] the damping capacity of two types of deciduous and coniferous
 by other    researchers.toIncompare
      It is interesting         the workthe [12]  the damping
                                              results              capacity ability
                                                        on the damping        of two of   types   of deciduous
                                                                                             wood-based            and coniferous
                                                                                                              materials    obtained
wood: beech and spruce under loading in the longitudinal, tangential and radial directions were
 wood:
by  otherbeech     and spruce
            researchers.    In theunder
                                   work [12]loading    in the longitudinal,
                                                 the damping       capacity of two tangential
                                                                                         types ofand     radial directions
                                                                                                    deciduous                   were
                                                                                                                   and coniferous
compared. The highest specific energy absorbed was noted for specimens under longitudinal loading,
 compared.
wood:     beechTheandhighest
                        spruce specific      energyinabsorbed
                                  under loading                      was noted
                                                           the longitudinal,            for specimens
                                                                                  tangential                under
                                                                                                   and radial          longitudinal
                                                                                                                  directions   were
and the smallest—under tangential loading. This is traditional tendency for wood materials.
 loading, andThe
compared.         the highest
                      smallest—under
                                 specific tangential
                                             energy absorbedloading.was
                                                                      This noted
                                                                            is traditional       tendencyunder
                                                                                       for specimens         for wood     materials.
                                                                                                                      longitudinal
      While
       While    in  [14], the   damping      ability   of the   mesocarp     layer     in  durian     shell (tropical    fruit)
                                                                                                                          fruit) was
loading,    andinthe[14],  the damping tangential
                      smallest—under         ability of loading.
                                                            the mesocarp
                                                                     This islayer      in durian
                                                                               traditional            shell for
                                                                                                tendency     (tropical
                                                                                                                  wood materials.was
investigated
 investigated    and, as   aa result of
                                     of the  research, it    was  found the
                                                                          the inverse
                                                                                inverse effect:
                                                                                            effect: specific
                                                                                                     specific energy
                                                                                                               energy absorption
      While inand, [14],asthe result
                                damping  theability
                                             research,of itthe
                                                             was  found
                                                                mesocarp     layer in durian          shell (tropical absorption
                                                                                                                         fruit) was
 of the mesocarp
investigated     and,layer     underoflateral
                       as a result              loadingitis
                                        the research,          higher
                                                             was found than
                                                                         the that
                                                                               inverseunder     axial
                                                                                           effect:     one. This
                                                                                                    specific  energymayabsorption
                                                                                                                           be due to
of the mesocarp layer under lateral loading is higher than that under axial one. This may be due to
Materials 2020, 13, 5261                                                                                       6 of 12

of the mesocarp layer under lateral loading is higher than that under axial one. This may be due to
the fact that the durian shell does not have the same clearly pronounced fiber structure as in wood,
therefore the authors’ accentuation on the lower strength and damping ability of the material in the
axial direction of load application compared to lateral loading refers to the radial and tangential
strength of shell of this fruit.

4. Identification and Verification of the Wood Model
     To describe the behavior of wood under dynamic loads in the library of the LS-DYNA calculation
complex, there is model No. 143 MAT_WOOD. This is a model of a transversely isotropic material for
solid elements. It is possible to set material properties or use a predefined set of constants, but only for
two species of pine growing in the USA: southern yellow pine and Douglas fir.
     The primary features of the model are:
•     Transverse isotropy for the elastic constitutive equations (different properties are modeled parallel
      and perpendicular to the grain).
•     Yielding with associated plastic flow formulated with separate yield (failure) surfaces for the
      parallel- and perpendicular-to-the-grain modes.
•     Hardening in compression formulated with translating yield surfaces.
•     Post-peak softening formulated with separate damage models for the parallel and
      perpendicular-to-the-grain modes.
•     Strength enhancement at high strain rates.
     Model 143 for pine contains a predefined set of 29 parameters depending on moisture content and
temperature. According to the results of the pine tests, some parameters of this model were adjusted
for a particular batch of samples under study. These parameters are shown in Table 2.

                           Table 2. Main mechanical properties of pine for model identification.

                                             Designation                                            Value
                                                Density                                            450 kg/m3
                           Modulus of elasticity in the direction of the grain                 10,500 MPa
                   Flow stress during compression in the direction of the grain                     80 MPa
              The modulus of elasticity in the direction perpendicular to the grain                246 MPa
          Flow stress during compression in the direction perpendicular to the grain                10 MPa

     It should be noted that the elastic moduli of pine under loading along and across the grain
were obtained as a result of quasi-static tests, since the Kolsky method, in principle, does not allow
constructing a stress–strain curve in which the slope dσ/dε of the elastic loading section would be
equal to the static modulus of elasticity. Usually the steepness of this section is several times less than
the static Young’s modulus. The reasons for this are as follows:
-     The difference in the cross-sectional areas of the measuring bars and the sample (some part of
      the incident wave is reflected from the free surface around the sample), causing an apparent
      deformation of the sample,
-     The presence of gaps between the ends of the measuring bars and the sample (due to the
      non-parallelism of its ends and their roughness or insufficient “pressing” of the sample during
      the preparation of the test),
-     Dispersion during the propagation of waves in the bars (decrease in the steepness of the transmitted
      pulse during the propagation time to the recording strain gauge).
      In order to confirm the adequacy of the model parameters determined from experiments,
it is necessary to verify it, but in experiments other than those in which these parameters were
Materials 2020, 13, 5261                                                                                                              7 of 12

obtained.     For
Materials 2020,   13,this
                      5261purpose, we used a model experiment in full-scale and numerical implementation.                               7 of 12
The simulation of the indentation process was performed using the finite element method. The explicit
  Materials
performed
time        2020,
       integration 13, 5261
                using     the
                          schemeDynamics-2
                                       was used         for solving the equations of motion in time. Modeling 7was
                                                 ® software package [20]. The numerical experiment was simulated                           of 12
in  an  axisymmetric         formulation,
performed using the Dynamics-2 software         ®and    its design    corresponded       to  a  similar   natural   test.
                                                                 package [20]. The numerical experiment was simulated in
  performed
       To verify  usingthe  the   Dynamics-2
                              model      of and
                                                    ® software package [20]. The numerical experiment was simulated
                                              material      behavior,       we usedtoan      experimental       scheme for dynamic
an axisymmetric          formulation,               its design     corresponded          a similar    natural test.
  in an axisymmetric
indentation       by   using   formulation,
                                the   system     ofanda   its design
                                                         split          corresponded
                                                                Hopkinson       bar.  The  to  a similarprocedure
                                                                                            indicated      natural test.is schematically
      To verify the model of material behavior, we used an experimental scheme for dynamic                                     indentation
shown   To    verify    the    model       of  material       behavior,      we  used     an   experimental       scheme      forhead
                                                                                                                                    dynamic
by   usinginthe Figure
                    system 6. ofThe    sample
                                   a split          5 and abar.
                                              Hopkinson           removable      indenter
                                                                       The indicated           4 with ais hemispherical
                                                                                           procedure         schematically shown           are
                                                                                                                                             in
  indentation
sandwiched          by  using
                   between        the
                                the    system
                                     measuring     of  a
                                                      barssplit
                                                             2   Hopkinson
                                                                and  6. Upon     bar.
                                                                                impact The   indicated
                                                                                          loading     by   procedure
                                                                                                         the  striker  1,is
                                                                                                                          a  schematically
                                                                                                                            compression
Figure 6. The sample 5 and a removable indenter 4 with a hemispherical head are sandwiched between
  shown is
impulse     ingenerated
                  Figure 6. inThe        sample       5 duration
                                                          and a removable           indenteron   4 the
                                                                                                    with   a hemispherical         head      are
the  measuring        bars 2 andthe       bar 2 the
                                      6. Upon      impact     loadingof which     depends
                                                                         by the striker                 length
                                                                                           1, a compression      of the striker
                                                                                                                 impulse            and the
                                                                                                                              is generated
  sandwiched
amplitude           between       theofmeasuring        bars   2 and   6. Upon    impact loading by the the    striker   1, a compression
in  the bar 2on  thethe    speed
                       duration          the striker.
                                    of which      depends  In the   case
                                                                on the     of hemispherical
                                                                         length  of the strikerindenter,            contact
                                                                                                    and the amplitude        onarea    at the
                                                                                                                                 the speed
  impulse
initial       is
         moment   generated
                       of         in the
                           indentation     baris 2  the
                                                 very     duration
                                                           small,      of  which
                                                                    therefore,   thedepends
                                                                                       amplitudeon   the
                                                                                                      of length
                                                                                                          the     of  the
                                                                                                               reflected   striker
                                                                                                                            pulse     and
                                                                                                                                     is  verythe
of the striker. In the case of hemispherical indenter, the contact area at the initial moment of indentation
  amplitude and
significant,      on theso speed      of theisstriker.
                             the sample           loaded    In the case      of hemispherical       indenter, oftheadditional
                                                                                                                      contact area       at the
is very small, therefore,           the amplitude          of several    times.
                                                               the reflected     For reliable
                                                                                pulse              recording
                                                                                        is very significant,     and so the sample  loading   is
  initial
cycles, itmoment
             is necessaryof  indentation
                                 to increase   is   very    small,   therefore,
                                                  the lengthofofadditional         the
                                                                      the supporting    amplitude
                                                                                           bar         of  the
                                                                                                 in comparison  reflected    pulse
                                                                                                                     withtothe    lengthvery
                                                                                                                                       is    of
loaded    several     times. For      reliable recording                           loading    cycles,  it is necessary        increase     the
  significant,
the  loading       andasso    the sample        is loaded       several    times.cycles
                                                                                   For reliable     recording of additional loading
length   of thebar         much
                   supporting        as
                                     barrequired       to register
                                           in comparison         withloading
                                                                        the length        [21].loading
                                                                                      of the              bar as much as required to
  cycles, it is necessary to increase the length of the supporting bar in comparison with the length of
register loading cycles [21].
  the loading bar as much as required to register loading cycles [21].

                                    Figure 6. High speed indentation experiment scheme.
                                    Figure 6. High speed indentation experiment scheme.
         Using strain gauges 3,Figure  elastic6. strain
                                                 High speed
                                                         pulses indentation
                                                                    are recordedexperiment
                                                                                        in thescheme.
                                                                                                 measuring bars (Figure 7). The
         Usingpulses
 following       strainaregauges
                            indicated3, elastic    strain 1—incident
                                          by numbers:        pulses are recorded            in thepulse
                                                                             (loading) strain          measuring         bars (Figure
                                                                                                              εI(t), 2—reflected       pulse7).
          Using strain    gauges    R3, elasticby strain   pulses1—incident
                                                                     are recorded        in theI measuring          bars    (Figure
                                                                                                                        I (t),         7). The
 in the first loading cycle ε1 (t ) , 3—incident (loading) strain pulse ε 2 (t ) in the second
The     following    pulses  are  indicated          numbers:                         (loading)     strain   pulse    ε        2—reflected
                                                                                                                            loading cycle,
    following
pulse     in thepulses   are indicated
                  first loading    cycle εby R (numbers:
                                                t), 3—incident1—incident
                                                                     (loading) (loading)
                                                                                     strain strain
                                                                                              pulse pulse      εI(t),
                                                                                                       εI2 (t) in  the2—reflected
                                                                                                                          second loading pulse
                                                                           R                                                             T
 4—reflected
cycle,            strain
    in the4—reflected
                          pulse
           first loading strain
                                 in  the
                           cycle pulse
                                      R
                                             1
                                          second     loading
                                   ε1 (t ) ,in3—incident         cycle
                                                the second(loading)      ε 2
                                                                loading strain(t ) , 5—transmitted
                                                                           cycle εpulseR         I          pulse   (first
                                                                                               ε 2 (t ) in the second
                                                                                         (t), 5—transmitted                  cycle)
                                                                                                                      pulseloading     ε 1 (t )
                                                                                                                                (first cycle)
                                                                                                                                         cycle,
                                                      T
                                                                                       2
   T
ε, 14—reflected
    6—transmitted
     (t), 6—transmittedpulsepulse
                              (second
                    strain pulse
                                                    ε 2loading
                                          cycle)cycle)
                                   in(second
                                        the second
                                                        (tε)2.(t). cycle ε R (t ) , 5—transmitted pulse (first cycle) ε T (t )
                                                            T
                                                                               2                                                         1
                                                         T
 , 6—transmitted pulse (second cycle) ε (t ) .           2

      Figure 7. Typical waveform obtained in the experiment for high-speed indentation, taking into account
      Figure 7. Typical waveform obtained in the experiment for high-speed indentation, taking into
      additional cycles: upper beam—data from bar 2; lower beam—data from bar 6.
      account additional cycles: upper beam—data from bar 2; lower beam—data from bar 6.
       Figure 7. Typical waveform obtained in the experiment for high-speed indentation, taking into
      The loading of the SHPB system in the numerical experiment (Figure 8) is performed in the same
       account
      The       additional
          loading          cycles: system
                    of the SHPB    upper beam—data   from bar
                                          in the numerical    2; lower beam—data
                                                           experiment    (Figure 8)from   bar 6.
                                                                                    is performed    in the same
way as in the natural experiment—with the help of a striker having an initial velocity V 0 . In the
way as in the natural experiment—with the help of a striker having an initial velocity V0. In the
      The loading
calculation        ofthe
             process, theincident
                          SHPB system    in the numerical
                                   and reflected            experiment
                                                 strain pulses          (Figurein8)element
                                                                are calculated      is performed
                                                                                            2 and in
                                                                                                   thethe  same
                                                                                                        past—
 way  as  in the natural  experiment—with      the help  of  a striker having  an  initial
in element 6. The time dependences obtained during the simulation are compared with the    velocity  V 0. In the

 calculation process,
corresponding   valuesthe  incidentduring
                        recorded    and reflected  strain pulses are calculated in element 2 and the past—
                                          the experiment.
 in element 6. The time dependences obtained during the simulation are compared with the
 corresponding values recorded during the experiment.
Materials 2020, 13, 5261                                                                                                                      8 of 12

Materials 2020, 13, 5261                                                                                                                      8 of 12

calculation process, the incident and reflected strain pulses are calculated in element 2 and the past—in
element 6. The time dependences obtained during the simulation are compared with the corresponding
                          Figure 8. High speed indentation experiment simulation scheme.
 Materialsrecorded
values     2020, 13, 5261
                      during the experiment.                                                         8 of 12

      The indenter is made of high-strength tungsten–cobalt alloy and is modeled by a rigid non-
deformable material.
      To assess the processes occurring in the sample, data obtained from measuring bars is used. In
accordance with the Kolsky formulas, one can calculate the law of change of the indenter penetration
rate into the sample V(t) and the penetration resistance force F(t):
                               Figure 8. High speed
                                               V(t) =indentation
                                                       C1·(εI(t) + εexperiment
                                                                     R(t)) − C2·εsimulation
                                                                                 T(t)       scheme.
                               Figure 8. High speed   indentation   experiment    simulation scheme.
                                                                                                                                                  (1)
       The indenter is made of high-strength                      F(t) =tungsten–cobalt
                                                                             E2∙S2 εT(t).             alloy and is modeled by a rigid
        The indenter
non-deformable                 is made of high-strength tungsten–cobalt alloy and is modeled by a rigid non-
                           material.
here   εI(t), εR(t)
 deformable            and εT(t) denote the incident, reflected, and transmitted strain pulses in the measuring
                    material.
       To assess the processes occurring in the sample, data obtained from measuring bars is used.
bars, respectively,
        To assesswith    the Ethe
                                is the elastic
                              processes             modulus,the    and      C is thedata
                                                                                       bar obtained
                                                                                             velocity of      sound.    The subscripts       1 and In 2
In accordance                       Kolskyoccurring
                                               formulas, in   one can   sample,
                                                                            calculate    the law of change  from   measuring
                                                                                                                   of the indenter barspenetration
                                                                                                                                         is used.
refer   to
 accordance the   first   (loading)      and    second     (supporting)         measuring        bars.
rate  into the with sample  theV(t)
                                  Kolskyandformulas,
                                              the penetrationone can       calculateforce
                                                                      resistance        the lawF(t):of change of the indenter penetration
 rate When
       into the   modeling
                     sample V(t)   the and
                                         process    of dynamic resistance
                                               the penetration          indentation        intoF(t):
                                                                                        force     wood samples, the following scheme
was used: a sample and an indenter                  V(t) =  were
                                                               C1C·(εconsidered
                                                                       I (t) + εR (t))(Figure
                                                                                         − C 2·ε     9). The spatial discretization of the
                                                                                                ·εTT(t)
                                                                                                     (t)
                                                                   1·(εI(t) + εR(t)) − C2
indenter and the sample was doneV(t)                       by=using          a solid
                                                                 F(t) = E2 ·S2 ε (t). T three-dimensional            finite element with one        (1)
                                                                                                                                                   (1)
integration point. Due to the presence of symmetry,               F(t) = E2∙S    a 2quarter
                                                                                     ε (t). of the geometric model was considered.
                                                                                      T

On
here the I  planesR      of  symmetry,
                                 T             the  corresponding             boundary        conditions were pulses   specified:the at the nodes
 hereεεI(t),
           (t), εεR(t)  and εεT(t)
                    (t) and        (t) denote
                                        denote thethe incident,
                                                       incident, reflected,
                                                                     reflected, and  and transmitted
                                                                                            transmitted strain strain pulses in  in the measuring
                                                                                                                                         measuring
lying    on   the   plane     with     the  normal      in  the  direction        of the   oY   axis,    zero   velocities   in  the  oY direction2
bars,    respectively,EEisisthe
 bars,respectively,                  theelastic
                                           elasticmodulus,
                                                    modulus,and     andCCisisthe   thebar
                                                                                        barvelocity
                                                                                              velocityof   ofsound.
                                                                                                               sound.The Thesubscripts
                                                                                                                               subscripts11and  and 2
and
refer zerothe velocities      of rotation about          the oX and oZ axes            were set; at the nodes lying on the plane with
 referto to thefirst
                   first(loading)
                           (loading)and   andsecond
                                                 second(supporting)
                                                            (supporting)measuringmeasuringbars.   bars.
the normal
       When        in the direction          of the   oZ    axis, zero       velocitiesintoin   the oZ      direction
                                                                                                                    the and    zero velocities       of
        Whenmodeling
                   modelingthe      theprocess
                                          process  ofof
                                                      dynamic
                                                          dynamic   indentation
                                                                          indentation         wood
                                                                                            into   wood samples,
                                                                                                             samples,    following
                                                                                                                          the followingscheme    was
                                                                                                                                             scheme
rotation
used:        about
         a sample       the  oX
                          and anandand    oY
                                     indenter  axes  were     set.
                                                   were considered            (Figure (Figure
                                                                                         9). The spatial
 was used:        a sample                an indenter        were considered                          9). Thediscretization        of the indenter
                                                                                                                 spatial discretization         of the
and    Zero
      the        velocities
            sample        was   in theby
                                done      direction
                                             using    a  of thethree-dimensional
                                                         solid    oX axis were set at             the element
                                                                                              finite    nodes belonging
                                                                                                                   with   one    to the surface
                                                                                                                                integration          of
                                                                                                                                                point.
 indenter and the sample was done by using a solid three-dimensional finite element with                                                           one
the
Due  sample,       which
       to the presence        in  full-scale
                                of symmetry,     experiments
                                                    a quarter       rested      against
                                                                   of the geometric        the   transmitted       measuring       bar.
 integration       point. Due        to the presence        of symmetry,          a quartermodelof thewas       considered.
                                                                                                          geometric     modelOn   wasthe   planes of
                                                                                                                                        considered.
       The indenter
symmetry,                    was modeledboundary   by an absolutely           rigid  undeformable            body.   For thelying
                                                                                                                               indenter,    the law
 On the planes of symmetry, the corresponding boundary conditions were specified: at the plane
                  the    corresponding                          conditions         were    specified:       at the  nodes            on   the   nodes
of thethe
with       change
             normal    ininthethespeed      of itsofmovement
                                    direction        the   oY   axis, inzerothe velocities
                                                                                 axial direction
                                                                                               in  the   was
                                                                                                         oY     set. The and
                                                                                                              direction    timezerodependence
                                                                                                                                       velocities    of
                                                                                                                                                     of
 lying on the plane with the normal in the direction of the oY axis, zero velocities in the oY direction
indenter’s
rotation         axial
             about        velocity
                         the  oX    and foroZa particular
                                                axes   were    experiment
                                                               set;   at    the    was
                                                                                 nodes    calculated
                                                                                           lying     on    using
                                                                                                          the      the
                                                                                                               plane    Equation
                                                                                                                       with   the     (1)
                                                                                                                                    normal based
                                                                                                                                               in   on
                                                                                                                                                   the
 and zero velocities of rotation about the oX and oZ axes were set; at the nodes lying on the plane with
the  signals
direction      ofrecorded
                   the           in the
                          oZ axis,    zero measuring
                                              velocities    bars.
 the normal         in the    direction      of   the oZ in     thezero
                                                             axis,    oZ direction
                                                                              velocitiesand      zerooZ
                                                                                             in the      velocities
                                                                                                             direction of and
                                                                                                                          rotation
                                                                                                                                zeroabout     the oX
                                                                                                                                       velocities    of
and    The
      oY      “surface–surface”
            axes    were     set.           contact    interaction        was    set between        the   indenter    and   the   sample.
 rotation about the oX and oY axes were set.
        Zero velocities in the direction of the oX axis were set at the nodes belonging to the surface of
 the sample, which in full-scale experiments rested against the transmitted measuring bar.
        The indenter was modeled by an absolutely rigid undeformable body. For the indenter, the law
 of the change in the speed of its movement in the axial direction was set. The time dependence of
 indenter’s axial velocity for a particular experiment was calculated using the Equation (1) based on
 the signals recorded in the measuring bars.
        The “surface–surface” contact interaction was set between the indenter and the sample.

   a)                                                                            b)

        Figure 9.9.Geometric statement
                     Geometric         of the
                                statement  of problem of numerical
                                               the problem         simulation:
                                                           of numerical        (a) 3D configuration,
                                                                         simulation:                 (b) plane
                                                                                        (a) 3D configuration,
        configuration.
        (b) plane configuration.

      Zero velocities in the direction of the oX axis were set at the nodes belonging to the surface of the
sample, which in full-scale experiments rested against the transmitted measuring bar.
      The indenter was modeled by an absolutely rigid undeformable body. For the indenter, the law
of a)
   the change in the speed of its movement in the axial    b)direction was set. The time dependence of

        Figure 9. Geometric statement of the problem of numerical simulation: (a) 3D configuration, (b) plane
        configuration.
Materials 2020, 13, 5261                                                                                                           9 of 12

indenter’s axial velocity for a particular experiment was calculated using the Equation (1) based on the
signals recorded in the measuring bars.
  Materials 2020, 13, 5261                                                                                           9 of 12
     The “surface–surface” contact interaction was set between the indenter and the sample.
     InInnatural
            naturalexperiments
                       experiments on on the
                                          the indentation   thesamples
                                              indentation the    samplesofofpinepinewere
                                                                                      wereused
                                                                                            used ininthethe form
                                                                                                          form  of of  tablets
                                                                                                                   tablets
with
  with a length of 10 mm and a diameter of 20 mm. Some of the samples were cut in the directionof
     a  length    of  10 mm   and   a diameter    of 20 mm.   Some   of  the  samples   were  cut   in the  direction     ofthe
wood   grain,grain,
  the wood       whilewhile
                         another   partpart
                              another    of the  samples
                                              of the       waswas
                                                     samples    cutcut
                                                                    in in
                                                                        thethe
                                                                             perpendicular
                                                                                perpendiculartotothethegrain
                                                                                                         graindirection.
                                                                                                                direction.
     AsAs mentioned
             mentionedabove,above,ininthe
                                       the process
                                           process of dynamic
                                                        dynamicindentation,
                                                                  indentation,the  thesample
                                                                                       sample is is subjected
                                                                                                  subjected   to to multiple
                                                                                                                 multiple
loading
  loading ininthe
                theexperiment
                     experiment(see(seeFigure
                                        Figure 7), thus
                                                    thusundergoing
                                                          undergoingaacertain
                                                                           certaindeformation
                                                                                    deformation  in in  each
                                                                                                     each     loading
                                                                                                           loading       cycle.
                                                                                                                     cycle.
  High-speed
High-speed     filmfilm  recording
                      recording       of the
                                  of the      indentation
                                          indentation       process
                                                         process     makes
                                                                  makes        it possible
                                                                          it possible       to estimate
                                                                                       to estimate          a number
                                                                                                      a number            of
                                                                                                                  of loading
  loading
cycle and cycle     and indentation
             indentation      depth atdepth
                                          which at which  the destruction
                                                   the destruction   of theofmaterial
                                                                               the material  occurs.
                                                                                         occurs.        Figure
                                                                                                     Figure   1010shows
                                                                                                                    showsthe
  the frames
frames   of such of such   registration,
                    registration,    made made
                                            usingusing  a high-speed
                                                    a high-speed      camera
                                                                   camera    HSFCHSFC   Pro.
                                                                                     Pro.

                                Figure  10. High-speed
                                 Figure10.             registrationofofdynamic
                                            High-speed registration     dynamicindentation.
                                                                                 indentation.

       TheThe left  part
                 left     of of
                       part   thethe
                                   figure   corresponds
                                       figure  corresponds   to the  experiment
                                                                to the   experiment  with   thethe
                                                                                         with    sample    cutcut
                                                                                                      sample    in the    direction
                                                                                                                     in the          along
                                                                                                                             direction
thealong
     grain,    whereas       the   right  part   corresponds      to the  experiment        with   the
            the grain, whereas the right part corresponds to the experiment with the sample cut in the   sample    cut   in the  direction
transverse
   direction to      the grain.
                  transverse      to The   numbers
                                      the grain.    Theon    the left on
                                                          numbers      of the
                                                                           the high-speed        registration
                                                                                left of the high-speed            images indicate
                                                                                                               registration     imagesthe
number
   indicate  ofthe
                 loading
                      number cycles    (running
                                  of loading        number
                                                 cycles         of impulse
                                                          (running    numberinof  the  loadinginmeasuring
                                                                                     impulse         the loadingbar)      which one
                                                                                                                     measuring     bar)can
seewhich
     in Figure      7. It can   be  seen   in Figure    10  that the  samples    cutting    off parallel   to
             one can see in Figure 7. It can be seen in Figure 10 that the samples cutting off parallel to thethe  grain    remain   intact
throughout
   grain remain   theintact
                       experiment,
                               throughout whichtheisexperiment,
                                                     confirmed by      the final
                                                                    which         state of such
                                                                            is confirmed      by thesamples.     Samples
                                                                                                       final state  of such obtained
                                                                                                                              samples. by
cutting
   Samples in the    direction
                 obtained           perpendicular
                              by cutting                to the grain
                                            in the direction            retain their
                                                                 perpendicular          integrity
                                                                                    to the            duringtheir
                                                                                             grain retain      the integrity
                                                                                                                    first loading    cycle,
                                                                                                                                during
however,
   the first cracks
                loadingand cycle,gaps    between
                                     however,        the layers
                                                  cracks   and gapsof wood
                                                                       between appear     in theofsecond
                                                                                   the layers                cycle, which
                                                                                                      wood appear       in the grow
                                                                                                                                secondand
   cycle, which
progress              grow and loading
              in subsequent         progresscycles,
                                                in subsequent
                                                         leadingloading      cycles, leading
                                                                   to the separation       of theto sample
                                                                                                     the separation     of the sample
                                                                                                              into parts.
   intoIt parts.
          can be noted that for the same load amplitude, the samples obtained by cutting in the direction
          It canremain
of the fiber       be noted     that for
                            intact,       thethe
                                      while   same     load amplitude,
                                                   samples                 the samples
                                                               cut perpendicular           obtained
                                                                                       to the           by cutting
                                                                                                fiber exhibit         in the
                                                                                                                 failure      direction
                                                                                                                           already   in the
   of the   fiber
first loading cycle.remain     intact,   while   the  samples    cut perpendicular       to the   fiber  exhibit  failure   already   in
   the first loading cycle.
          A comparison of the shape of the imprint on the pine sample after the experiment on the
   dynamic indentation of a hemispherical indenter is shown in Figure 11.
Materials 2020, 13, 5261                                                                                   10 of 12

      A comparison of the shape of the imprint on the pine sample after the experiment on the dynamic
indentation
Materials 2020,
Materials        of 5261
          2020, 13,
                13, a hemispherical indenter is shown in Figure 11.
                    5261                                                                        10 of
                                                                                                10 of 12
                                                                                                      12

             a)                                                   b)

     Figure 11.
      Figure11.
     Figure     The shape
                 Theshape
             11.The       ofofthe
                     shapeof  the imprints
                               theimprints obtained
                                   imprintsobtained by
                                            obtainedby numerical
                                                     bynumerical modeling
                                                        numericalmodeling (a)
                                                                  modeling(a) and
                                                                           (a)and in
                                                                               andin the
                                                                                   inthe natural
                                                                                      thenatural test
                                                                                          naturaltest (b).
                                                                                                  test(b).
                                                                                                       (b).

     Figure 12 shows
     Figure     shows a comparison
                          comparison of the time dependences
                                                    dependences of the indentation resistance
                                                                                       resistance of pine
sample  recorded  in the experiments (solid colored lines) with the data obtained  by numerical
sample recorded in the experiments (solid colored lines) with the data obtained by numerical    modeling
(black dashed  lines) during dynamic   indentation  of hemispherical  indenter  into specimen  both
modeling (black dashed lines) during dynamic indentation of hemispherical indenter into specimen    along
and across
both along the
            andgrain.
                 across the grain.

               Figure 12.
               Figure     Comparison of
                      12. Comparison  of experimental
                                         experimental and
                                                       and calculated
                                                           calculated pulses
                                                                      pulses in
                                                                              in the
                                                                                 the supporting
                                                                                     supporting bar.
                                                                                                bar.
               Figure 12. Comparison of experimental  and calculated  pulses in the supporting  bar.

       It can be seen that the model used allows us to accurately reproduce the features of the deformation
      It can be seen that the model used allows us to accurately reproduce the features of the
 of real material, namely, the difference in its deformation behavior in different directions with respect
deformation of real material, namely, the difference in its deformation behavior in different directions
 to grain orientation.
with respect to grain orientation.
       The results obtained are in qualitative agreement with the data from previous studies of high
      The results obtained are in qualitative agreement with the data from previous studies of high
 strain rate behavior of wood [8,17]. Correction of some parameters of the MAT_WOOD model made it
strain rate behavior of wood [8,17]. Correction of some parameters of the MAT_WOOD model made
it possibletotodescribe
possible         describethe
                           thedeformation
                               deformationbehavior
                                             behaviorof of the
                                                            the studied
                                                                studied wood    species with
                                                                         wood species   with sufficient
                                                                                              sufficientaccuracy.
                                                                                                         accuracy.
A further increase in the quality of the mathematical model is possible by taking into account the effect
A further increase in the quality of the mathematical model is possible by taking into account the
 of the of
effect   strain rate inrate
            the strain  a wide
                            in arange
                                 wideof its change,
                                      range          as well as
                                             of its change,   as well
                                                                  taking
                                                                       asinto account
                                                                          taking      the fracture
                                                                                 into account      of the material.
                                                                                               the fracture of the
material. In addition, it is necessary to conduct more complex model experiments to verify the
fracture criteria, for example, high-speed penetration and perforation of wood plates.
Materials 2020, 13, 5261                                                                                         11 of 12

In addition, it is necessary to conduct more complex model experiments to verify the fracture criteria,
for example, high-speed penetration and perforation of wood plates.

5. Conclusions
     Dynamic tests of lime-tree and pine were conducted. There is a strong anisotropy of the properties
of the tested materials: the specimens exhibit the greatest strength under load applied along the
grain, while the lowest strength is observed under loading transverse to the grain. The load branch
module is non-linear and, as a rule, smaller than the unloading branch module (while maintaining the
specimen integrity). At the specimen cutting angle of 90◦ with respect to the direction of the fibers,
the stress–strain diagram after reaching a certain threshold stress value (about 8 MPa for lime-tree
and about 10 MPa for pine) is close to the ideal plastic diagram. At 0◦ cutting angle, the initial section
of the diagrams is close to linear. That is, an elastic deformation occurs. However, after reaching an
ultimate stress value (yield strength), the diagram becomes nonlinear with stress relaxation. Especially
such behavior is observed in the experiments in which the failure of specimens occurs.
     Using a modification of the SHPB method, experiments were performed on the dynamic
indentation of indenters with a hemispherical head into the samples parallel and perpendicular
to the direction of the fibers. Dependences of resistance to penetration on time are constructed. In the
direction of the fiber (along the grain), the resistance force was more than three-times greater than
in the transverse direction. The results of the natural experiment were compared with the results of
numerical modeling, in which the wood behavior was described by the MAT_WOOD model from
the LS-DYNA software, in which some of the parameters were obtained experimentally. A good
coincidence was observed.

Author Contributions: Conceptualization, A.B. and L.I.; data curation, T.I.; formal analysis, A.K.; funding
acquisition, L.I.; investigation, A.L.; methodology, A.K. and A.L.; project administration, A.B.; resources, L.I.;
software, A.K. and T.I.; supervision, F.d.; validation, F.d. and A.K.; visualization, A.K.; writing—original draft, A.L.;
writing—review and editing, A.B. All authors have read and agreed to the published version of the manuscript.
Funding: Experimental investigations of wood were performed with the financial support of the Ministry of
Science and Higher Education of the Russian Federation (task 0729-2020-0054). Numerical simulation of wood
behavior was supported by the grant of the Government of the Russian Federation (contract No.14.Y26.31.0031).
Conflicts of Interest: The authors declare no conflict of interest. The funders had no role in the design of the
study; in the collection, analyses, or interpretation of data; in the writing of the manuscript, or in the decision to
publish the results.

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